Buchi I-300 Pro Operation Manual
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Buchi I-300 Pro Operation Manual

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  • Page 1 Interface I-300 Pro Operation Manual...
  • Page 2 CH-9230 Flawil 1 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experi- ence, especially with respect to structure, illustrations and technical details. This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for com- petitive purposes, nor made available to third parties.

  • Page 3: Table Of Contents

    Scope of delivery .......................... 26 Technical data ...........................  26 3.8.1 Interface .......................... 26 3.8.2 Junction boxes ........................ 26 3.8.3 Ambient conditions.........................  27 3.8.4 Materials .......................... 27 Transport and storage ...................... 28 Transport ............................ 28 Storage ..............................  28 Operation Manual Interface I-300 Pro...
  • Page 4 Overview: setting up vacuum tubing connections.............. 37 Connecting AutoDest sensor to vapor temperature sensor (optional accessory)...... 39 Connecting foam sensor (optional accessory)...................  40 Connecting valve unit for external vacuum.................. 42 Operating I-300 and I-300 Pro in parallel...................  42 Operation.......................... 44 Navigating the menu..........................  44 6.1.1 Selecting menu items......................
  • Page 5 10.5.4 Device settings........................ 98 10.5.5 Error data .......................... 98 10.5.6 Maintenance data ........................ 98 10.5.7 System configuration data .....................  98 10.5.8 Distillation process data ...................... 98 10.5.9 Contact data...........................  98 10.5.10Location data .........................  98 Accessories ........................ 99 Operation Manual Interface I-300 Pro...

  • Page 6: About This Document

    This character indicates an instruction that must be carried out by the user. ð This character indicates the result of a correctly carried out instruction. Mark-up Explanation Window Software Windows are marked-up like this. Tabs are marked-up like this. 6/102 Operation Manual Interface I-300 Pro...

  • Page 7: Trademarks

    Signals are marked-up like this. Trademarks Product names and registered or unregistered trademarks that are used in this docu- ment are used only for identification and remain the property of the owner in each case. Operation Manual Interface I-300 Pro 7/102...

  • Page 8: Safety

    0 mbar to ambient atmospheric pressure. The measurement and regulation of the vacuum is performed by means of a VacuBox. The Interface I-300 Pro has been de- signed and built as an item of laboratory equipment and can be used in conjunction with the following devices: —...

  • Page 9: Residual Risks

    Technical modifications to the device or accessories should only be carried out with the prior written approval of BÜCHI Labortechnik AG and only by authorized BUCHI technicians. BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized modifications. Operation Manual Interface I-300 Pro...

  • Page 10: Product Description

    BÜCHI Labortechnik AG Product description Description of function The Interface I-300 Pro is designed for indicating, adjusting and controlling the com- plete distillation system. The Interface I-300 Pro settings enable precise specification of the individual process parameters. For example: — Rotation speed of the evaporating flask —...
  • Page 11 Rotavapor R-220 Pro", page 32. Information on Full display of figures and Display of figures and graphs display graphs on display of I-300 Pro. split between I-300 and R-220 Pro. Lift control Manual and programmed control Manual adjustment of lift posi- of lift position possible, see tion possible, see Chapter 6.10...

  • Page 12: Parameter Display With R-300 And R-220 Pro

    The parameters for the current distillation process are shown on the home screen of the Interface I-300 Pro. Depending on which Rotavapor the interface unit is con- nected to, different parameters may be shown. Below is a comparison of the R-300...
  • Page 13 — Lift position set by means of — Lift position set by means of Lift position "vertical adjustment handle" "vertical adjustment handle" — Lift position set by means of "Up" and "Down" buttons on home screen Operation Manual Interface I-300 Pro 13/102...

  • Page 14: Configuration

    3 | Product description BÜCHI Labortechnik AG Configuration 3.5.1 Front view Fig. 1: Front view of Interface I-300 Pro Touch-screen display Navigation control STOP button (emergency stop) 14/102 Operation Manual Interface I-300 Pro...

  • Page 15: Rear View

    BÜCHI Labortechnik AG Product description | 3 3.5.2 Rear view Fig. 2: Rear view of Interface I-300 Pro LAN port Slot for BUCHI SD card BUCHI standard communication port USB connection (not used) (COM) Locating lug for bracket MicroSD card (not used)

  • Page 16: Vacubox (Connections)

    NOTE Connecting VacuBox with R-220 Pro: If the Interface I-300 Pro and the VacuBox are operated in the Rotavapor R-220 Pro system, the following points should be noted: The external valves must always be connected to the Rotavapor R-220 Pro even if there is an alternative connection on the VacuBox.

  • Page 17: Legacybox (Connections)

    LegacyBox (connections) Connection of a LegacyBox is required whenever legacy BUCHI laboratory equip- ment is to be controlled via the Interface I-300 Pro. The LegacyBox is connected to the distillation system using a standard BUCHI communication cable and has other connection options such as an RS-485 communication port.
  • Page 18 0 – 10 V (max. 20 mA, min. 500 Ohm) Relay In Max. 30 V 2 A, electrically isolated Spare Spare Relay Out Max. 30 V 2 A, electrically isolated Shield Shield, connected to ground 18/102 Operation Manual Interface I-300 Pro...

  • Page 19: Display

    Function buttons (context-dependent) 10 Graph display area NOTE While distillation is in progress, the display is shown in inverse type. A progress bar for each process parameter shows the status on reaching the specified setting con- cerned. Operation Manual Interface I-300 Pro 19/102...

  • Page 20: Type Plate

    3 | Product description BÜCHI Labortechnik AG 3.5.6 Type plate The type plate is on the rear of the Interface I-300 Pro. BÜCHI Labortechnik AG CH-9230 Flawil/Switzerland Type: I-300 1000000000 Volt: 30 VDC Frequ.: Power: 3 W Built: 2014 Made in Switzerland Fig. 6: Type plate (example)

  • Page 21: Favorites Menu

    — [Wearing parts ] — [Startup info] 3.6.2 Favorites menu For creating favorites. See Chapter 6.8 "Creating favorites", page 75 3.6.3 Operating modes menu The Interface I-300 Pro distinguishes between the following operating modes for a distillation system: Operating Purpose Content mode [Manual] Carrying out distillation with manually set See Chapter 6.2.3 "Ex-...
  • Page 22 [Pressure hystere- Entry of pressure Entry of figure for the maximum allow- sis] able difference between the actual vac- uum and the specified figure before the vacuum pump switches on again. 22/102 Operation Manual Interface I-300 Pro...
  • Page 23 View Display of local time. Can be changed by means of the action [UTC offset]. Necessary for identification of recorded data. [eco mode] On/Off and entry of See Chapter 6.6 "Activating eco mode", figures page 73 Operation Manual Interface I-300 Pro 23/102...
  • Page 24 [Delete APP con- Confirmation ques- All connections settings entered for the nection] tion instrument are reset. BUCHI Cloud Services submenu The submenu [BUCHI Cloud Services] contains functions and views relating to cloud solutions. Action Option Explanation [System owner] Info Shows the details of the registered sys- tem owner.

  • Page 25: Libraries Menu

    Symbols on the status bar Symbol Status Manual distillation Distillation using a method Drying AutoDest distillation Distillation running The memory card has been inserted. Continuous pumping The instrument is connected to the BUCHI Cloud. Timed distillation Operation Manual Interface I-300 Pro 25/102...

  • Page 26: Scope Of Delivery

    Magnetic valve supply 24 V Power consumption Power connections / output volt- 30 VDC ± 5 % 30 VDC ± 5 % Hysteresis Automatic or 1 - 200 Automatic or 1 - 200 mbar mbar 26/102 Operation Manual Interface I-300 Pro...

  • Page 27: Ambient Conditions

    50 % at 40 °C The laboratory equipment described in this document may only be used in indoor ar- eas. 3.8.4 Materials Component Material Pressure foil Polyester Casing Vent tube connection Pressure sensor Al₂O₃ 96% Operation Manual Interface I-300 Pro 27/102...

  • Page 28: Transport And Storage

    Make sure that the ambient conditions are complied with (see Chapter 3.8 "Tech- nical data", page 26). Wherever possible, store the device in its original packaging. After storage, check the device for damage and replace if necessary. 28/102 Operation Manual Interface I-300 Pro...

  • Page 29: Installation

    BÜCHI Labortechnik AG Installation | 5 Installation Fitting the Interface I-300/I-300 Pro The Interface I-300/I-300 Pro can be mounted on one of the following BUCHI labora- tory devices: — Rotavapor R-300 — Vacuum Pump V-300 — Rotavapor R-220 Pro Alternatively, the Interface I-300/I-300 Pro can be mounted separately on a laboratory stand, see Chapter 5.1.4 "Mounting interface unit on laboratory stand (optional acces-...
  • Page 30 Connect the communication cable to the COM port on the rear of the interface unit. Position the interface unit (3) on the holder and fix it in place using the knurled- head screw (1) supplied. When doing so, make sure that the communication cable is not trapped. 30/102 Operation Manual Interface I-300 Pro...

  • Page 31: Fitting Interface Unit On Vacuum Pump V-300

    Tools required: — Torx key Tx30 The Interface I-300 Pro can be mounted on the top of the Vacuum Pump V-300 using a holder. Remove the rubber plug (4) from the top panel of the vacuum pump. Use a screw- driver if necessary.

  • Page 32: Mounting Interface Unit On Rotavapor R-220 Pro

    BÜCHI Labortechnik AG 5.1.3 Mounting interface unit on Rotavapor R-220 Pro The Interface I-300 Pro is fitted directly adjacent to the display of the Rotavapor R-220 Pro. Remove the cover to the left of the Rotavapor display. (Behind the cover you will see a communication cable with a standard BUCHI communication connection and a LAN cable.)

  • Page 33: Mounting Interface Unit On Laboratory Stand (Optional Accessory)

    Fixing screws for interface unit Lug on front plate The Interface I-300 Pro can also be mounted directly onto a plastered or tiled wall or a laboratory fume hood with the aid of a wall bracket. Operation Manual Interface I-300 Pro...

  • Page 34: Connecting The Interface I-300/I-300 Pro

    Connecting the Interface I-300/I-300 Pro The Interface I-300/I-300 Pro can be connected either to an individual BUCHI labora- tory device or to a complete distillation system. Fig. 12: Interface unit, VacuBox, Rotavapor, vacuum pump and recirculating chiller...

  • Page 35: Connecting Communication Cables To Interface Unit

    The following port has to be enabled in the firewall settings on the internet gate- way: — TCP (HTTPS) traffics through remote port 443 In order to use the BUCHI Cloud a DNS server must be configured on the instru- ment. NOTE If there is no DNS server available enter the IP address for the BUCHI Cloud connec- tion manually.

  • Page 36: Overview: Setting Up Communication Connections (Com)

    BÜCHI Labortechnik AG Activate the function [DHCP]. ð The unit is now ready. Enabling BUCHI Cloud access Enable access to BUCHI Cloud in order to use the BUCHI Monitor App. Navigation path ➔ ➔ Settings ➔ Network ➔ BUCHI Cloud Navigate to the action [[BUCHI Cloud]] via the navigation path.

  • Page 37: Overview: Setting Up Vacuum Tubing Connections

    5.2.5 Overview: setting up vacuum tubing connections The vacuum tubing connections in a typical BUCHI distillation system lead from the Rotavapor R-300 via a Woulff bottle to the Vacuum Pump V-300/V-600. The vacuum is measured by means of the VacuBox, which is also connected to the Woulff bottle.
  • Page 38 Woulff bottle marked CONTR (5) and the VacuBox (6). The pressure is measured in the VacuBox. The current working pressure can be indi- cated and controlled by means of the Interface I-300/I-300 Pro. NOTE The VacuBox and Woulff bottle can be mounted either on the Rotavapor R-300 or the Vacuum Pump V-300/V-600.

  • Page 39: Connecting Autodest Sensor To Vapor Temperature Sensor (Optional Accessory)

    Communication connection between Coolant outlet on condenser AutoDest sensor and VacuBox NOTE There are two arrows stamped on the AutoDest sensor indicating the direction of flow for the coolant. The coolant tubing should be connected accordingly. Operation Manual Interface I-300 Pro 39/102...

  • Page 40: Connecting Foam Sensor (Optional Accessory)

    The communication cable from the foam sensor is connected to the Vac- uBox, see Chapter 3.5.3 "VacuBox (connections)", page 16. NOTICE Risk of heat damage to electronic components Only use the foam sensor at vapor temperatures up to 85 °C. 40/102 Operation Manual Interface I-300 Pro...
  • Page 41 When inserting the foam sensor, make sure that the sensor rod passes centrally through the components. The tip of the foam sensor should be positioned approx. 4 to 5 cm below the ground neck of the evaporating flask. Operation Manual Interface I-300 Pro 41/102...

  • Page 42: Connecting Valve Unit For External Vacuum

    Rotavapor R-220 Pro. Connecting valve unit for external vacuum The Interface I-300 Pro can be used together with the VacuBox to control an external vacuum. For precise control of the vacuum, the use of a Woulff bottle is also recom- mended.
  • Page 43 Installation | 5 If a mobile connection (see Chapter 5.2.2 "Establishing LAN connection", page 35) is desired when the I-300 and I-300 Pro are operating in parallel, the LAN cable must only be connected to one of the interface units, preferably the I-300 Pro.

  • Page 44: Operation

    BÜCHI Labortechnik AG Operation Navigating the menu The I-300 Pro offers the fundamental option of navigating the menu either by using the function buttons and the navigation control or by means of the touch-screen func- tionality of the display. The touch-screen functions can be operated using laboratory gloves. Liquids on the screen do not pose a problem either and do not impair functionality in any way.

  • Page 45: Entering Parameter Settings

    The Interface I-300 Pro offers the facility for manually setting various parameters. The parameters are shown on the home screen of the Interface I-300 Pro. The individual parameters are selected by rotating the navigation control or tapping the item directly on the screen.
  • Page 46 In that case, a scroll bar appears on the screen. To scroll down to a parameter, turn the navigation control or slowly swipe the screen upwards with your finger. 46/102 Operation Manual Interface I-300 Pro...

  • Page 47: Changing Settings

    To save the new option for the setting, press the navigation control to choose SAVE or tap SAVE directly on the screen. Performing distillation The Interface I-300 Pro offers the following operating modes for carrying out distilla- tion: Operation Manual Interface I-300 Pro...

  • Page 48: Overview: Typical Distillation Sequence

    Set the required pressure and start the vacuum pump. Rotavapor Immerse the evaporating flask in the heating bath. Rotavapor Increase rotation to the desired speed. Stopping distillation Step Component Action Vacuum pump/Valve unit Stop pressure regulation. 48/102 Operation Manual Interface I-300 Pro...

  • Page 49: Basic Functions

    To evacuate the system to the specified vacuum again after venting, press the function button HOLD OFF. Venting after completion of distillation If venting has not been pre-programmed on the interface unit, the system can be fully vented manually after completion of the distillation process. Operation Manual Interface I-300 Pro 49/102...

  • Page 50: Executing Manual Mode

    In [Manual] operating mode (manual distillation), the distillation process can be con- trolled by manually setting the individual process parameters. CAUTION Risk of personal injury and property damage from unexpected equip- ment behavior Always carefully check the pre-programmed settings before every distillation process. 50/102 Operation Manual Interface I-300 Pro...
  • Page 51 Heating Bath B-301/B-305 for heating bath temperature — Actual reading and specified setting Recirculating Chiller F-3xx for cooling temperature — Actual reading for vapor temperature AutoDest sensor or vapor temperature sensor — Actual reading for lift Operation Manual Interface I-300 Pro 51/102...
  • Page 52 To abort the cooling process prematurely, press the function button STOP. Editing parameters during manual distillation There is the facility for changing individual parameter settings while distillation is in progress. Precondition: R Distillation process has been started. 52/102 Operation Manual Interface I-300 Pro...

  • Page 53: Executing Timer Mode

    In [Timer] mode, a distillation process with a predefined duration is started. CAUTION Risk of personal injury and property damage from unexpected equip- ment behavior Always carefully check the pre-programmed settings before every distillation process. Navigation path ➔ Operating modes ➔ Timer Operation Manual Interface I-300 Pro 53/102...
  • Page 54 — Actual reading for vapor temperature AutoDest sensor or vapor temperature sensor — Actual reading and specified setting for duration of distillation (timer) — Actual reading for lift Starting timer-controlled distillation Precondition: 54/102 Operation Manual Interface I-300 Pro...
  • Page 55 There is the facility for changing the timer setting and other parameters while timer- controlled distillation is in progress. Precondition: R Timer-controlled distillation process has been started. Fig. 34: Editing parameters while distillation is in progress Operation Manual Interface I-300 Pro 55/102...
  • Page 56 There is the facility for stopping distillation before the set time has elapsed. To stop the timer-controlled distillation process prematurely, press the function button STOP. ð On completion of timer-controlled distillation, the display shows the following infor- mation: 56/102 Operation Manual Interface I-300 Pro...

  • Page 57: Executing Continuous Pumping Mode

    NOTE In [Continuous pumping] mode, the settings for manual or timer-controlled distillation are ignored. Navigation path ➔ Operating modes ➔ Continuous pumping [Continuous pumping] Operating modes Fig. 37: Selecting the option on the menu Operation Manual Interface I-300 Pro 57/102...
  • Page 58 To edit individual process parameters while drying is in progress, select and edit the parameter concerned in each case. To stop the drying process, press the function button STOP. In this operating mode, the following parameters and readings are available: 58/102 Operation Manual Interface I-300 Pro...

  • Page 59: Executing Autodest Mode

    Navigation ➔ Operating modes ➔ AutoDest [AutoDest] Operating modes Fig. 40: Selecting the option on the menu Precondition: R An AutoDest sensor has been installed and calibrated, see Chapter 7.7 "Calibrat- ing AutoDest sensor", page 80. Operation Manual Interface I-300 Pro 59/102...
  • Page 60 Recirculating Chiller F-3xx for cooling temperature — Actual reading for vapor temperature AutoDest sensor — Actual reading for lift Starting automatic distillation Precondition: R Process parameters have been set. Press the function button START. 60/102 Operation Manual Interface I-300 Pro...

  • Page 61: Executing Drying Mode

    In [Drying] mode, the remaining product in the evaporating flask is gently dried after completion of a distillation process. For this purpose, the evaporating flask on the Ro- tavapor R-300 rotates in alternating directions at defined intervals (e.g. 5 seconds). Navigation path ➔ Operating modes ➔ Drying Operation Manual Interface I-300 Pro 61/102...
  • Page 62 VacuBox (e.g. with Vacuum Pump V-300/V-600) — Actual reading for current pressure in distillation system — Actual reading and specified setting Rotavapor R-300 for rotation speed (evaporating flask) — Specified setting for rotation interval 62/102 Operation Manual Interface I-300 Pro...

  • Page 63: Executing Methods Mode

    — Clean system — Fit receiving flask — Fit dry receiving flask — Replenish solvent — Transfer contents to drying flask — Fit dry evaporating flask The subsequent step has to be started manually. Operation Manual Interface I-300 Pro 63/102...
  • Page 64 Fig. 45: Selecting the option on the menu Navigate to the Operating modes menu and select the menu item [Methods], see Chapter 6.1 "Navigating the menu", page 44. Fig. 46: Creating a new method To create a new method, press NEW. 64/102 Operation Manual Interface I-300 Pro...
  • Page 65 Any of the settings for a method can be edited at any time, e.g. number of steps, as- signed functions, etc. NOTE Drying not available with R-220 Pro: The option "Drying" is not available if the Interface I-300 Pro is operated with the Ro- tavapor R-220 Pro. Operation Manual Interface I-300 Pro 65/102...
  • Page 66 The specified settings are displayed across all programmed steps. Select a method and press START to start the distillation process immediately. Fig. 50: Display while method is running ð The display shows the home screen in inverse type. 66/102 Operation Manual Interface I-300 Pro...

  • Page 67: Displaying Reading Graphs

    Displaying reading graphs The Interface I-300 Pro offers the facility for displaying graphs of process data read- ings while distillation is in progress. You can individually select which process param- eters are to be shown as graphs.

  • Page 68: Recording Process Data

    Recording process data The Interface I-300 Pro offers the facility for saving process data from a distillation process to an SD card. The following process data is recorded: —...

  • Page 69: Inserting An Sd Card

    Slot BUCHI SD card The BUCHI SD card is inserted in the slot in the interface unit as shown. When do- ing so, make sure that the bevelled corner of the SD card is at the top right. ð The display shows the symbol for SD card inserted on the status bar.

  • Page 70: Activating Recording

    Solvent library The Interface I-300 Pro has an internal solvent library. Stored in that library are the most common solvents together with an algorithm in each case. Based on the chemi- cal properties of the solvent, the algorithm calculates and dynamically sets the ideal vacuum according to the current readings for heating bath and coolant temperature.
  • Page 71 Enter the specified settings for heating bath and coolant temperature if necessary. Fig. 57: Selecting "Set" temperature for heating bath when using equipment of a different make Operation Manual Interface I-300 Pro 71/102...

  • Page 72: Creating Your Own Solvent Library

    You can also create your own solvent library in which you can enter details of up to 60 of your own solvents. Navigation ➔ Tools ➔ Own solvent library Navigate to the "Tools" screen and select the menu item "Own solvent library", see Chapter 6.1 "Navigating the menu", page 44. 72/102 Operation Manual Interface I-300 Pro...

  • Page 73: Activating Eco Mode

    Chapter 6.8 "Creating favorites", page 75. Activating eco mode The Interface I-300 Pro offers an "eco mode" option for saving energy if the distillation system remains inactive for a predefined period of time. In eco mode, the distillation system shuts down the activity of the heating bath and recirculating chiller after a de- fined delay period so that: —...

  • Page 74: Setting Hysteresis

    The hysteresis setting is only relevant if the distillation system is not being operated with a BUCHI Vacuum Pump V-300 but with a different make of pump or with a labo- ratory vacuum supply, and is controlled by means of a valve.

  • Page 75: Creating Favorites

    Enter the desired figure for the maximum vacuum deviation from the specified set- ting. Creating favorites The Interface I-300 Pro offers the facility for saving individual functions and settings as favorites (bookmarks). Fig. 62: Submenu "Favorites" Clicking on any of the saved favorites takes you directly to the screen concerned.

  • Page 76: Activating Come Here Function

    Navigation path ➔ Precondition: R Monitoring services have been installed and set up. For details see "BUCHI Cloud and Monitoring Services Quick Guide " or https://www.buchi.com/en/buchi-cloud . Navigate to the Start screen and select the function button [Come here], see Nav- igating the menu.

  • Page 77: Cleaning And Servicing

    Any servicing and repair work which involves opening up the casing may only be car- ried out by BUCHI service technicians. Use only genuine BUCHI consumables and spare parts in order to ensure correct operation of the device and preserve the warranty.

  • Page 78: Opening Leak Test History

    Typically, an airtight system should have a leakage rate of less than 5 mbar/min. Opening leak test history Use the function Test results to view details of leak tests previously carried out. Navigation path ➜ Configuration➜ Maintenance ➜ Test results 78/102 Operation Manual Interface I-300 Pro...

  • Page 79: Fitting Gl14 Cap Nut With Tube Seal

    Seals are wearing parts. They have to be regularly inspected, cleaned and, if neces- sary, replaced. The life of a seal depends on how much it is used and how well it is looked after. Operation Manual Interface I-300 Pro 79/102...

  • Page 80: Checking Vacuum Seal

    ➜ Configuration ➜ System information ➜ AutoDest sensor Place the AutoDest sensor in a homogeneous water bath. Navigate to the System information sub-screen and select the menu item [Au- toDest sensor], see Chapter 6.1 "Navigating the menu", page 44. 80/102 Operation Manual Interface I-300 Pro...

  • Page 81: Calibrating The Pressure Sensor

    Press the navigation control to choose OK and confirm the calibration offset. Calibrating the pressure sensor The pressure sensor is calibrated at the factory by BUCHI prior to delivery. However, it can be recalibrated with the aid of an external reference pressure gauge at any time.

  • Page 82: Offset Calibration

    Navigate to the "Service" screen and select the menu item "Pressure offset", see Chapter 6.1 "Navigating the menu", page 44. Fig. 69: Menu item "Pressure offset" Enter the pressure measured by the reference sensor. ð The measured readings will then automatically be adjusted by the specified offset. 82/102 Operation Manual Interface I-300 Pro...

  • Page 83: Simple Calibration

    Repeat the process for all subsequent stages. To skip a stage, press the function button SKIP. ð After the last stage, the calibration settings are saved. To return to the menu, press the function button ESC or OK. Operation Manual Interface I-300 Pro 83/102...

  • Page 84: Loading Factory Calibration

    Rotavapor® Open Interface enables you to obtain an overall view of the status and communication of third party equipment with the device. NOTE Use of the function is at your own risk. For information about programming see https://www.buchi.com/en/content/buchi- cloud-services NOTE The password for Rotavapor ® Open Interface is displayed only once.
  • Page 85 Navigate to the Rotavapor Open Interface sub-screen and select the option [Yes], see Chapter 6.1 "Navigating the menu", page 44. Confirm the action when asked. ð The interface shows the password Restart the interface. ð The Rotavapor ® Open interface unit is set up. Operation Manual Interface I-300 Pro 85/102...

  • Page 86: Help With Faults

    The addresses of the official BUCHI Customer Service offices can be found on the BUCHI website at: www.buchi.com. If you have any questions regarding technical is- sues or faults, please contact those offices.

  • Page 87: Esupport

    — supply of spare parts — repairs — technical advice eSupport eSupport enables you to send a service ticket directly to a BUCHI technical engineer. Navigation path ➔Configuration ➔BUCHI Cloud Services Precondition: R The BUCHI Cloud Services have been installed and set up. For details see "BUCHI Cloud and Monitoring Services Quick Guide "...

  • Page 88: Taking Out Of Service And Disposal

    BÜCHI Labortechnik AG Taking out of service and disposal Taking out of service Switch off the Interface I-300 Pro and disconnect it from the mains power supply. Remove all tubing and communication cables from the device. Disposal The operator is responsible for proper disposal of the Interface.

  • Page 89: Appendix

    Isopentanol 88.1 0.809 Methylethylketone 72.1 0.805 Methanol 32.0 1227 0.791 Dichlormethane 84.9 1.327 Pentane 72.1 0.626 n-propanol 60.1 0.804 Pentachloroethane 202.3 1.680 1,1,2,2-tetra- 167.9 1.595 chloroethane Tetrachloromethane CCl 153.8 1.594 1,1,1-trichloroethane C 133.4 1.339 Operation Manual Interface I-300 Pro 89/102...

  • Page 90: Spare Parts And Accessories

    – 10.2 Spare parts and accessories Use only genuine BUCHI consumables and spare parts in order to ensure correct, safe and reliable operation of the system. NOTE Any modifications of spare parts or assemblies are only allowed with the prior written permission of BUCHI.
  • Page 91 Interface I-300 / I-300 Pro. Holder. To fix interface on lab stand 11059021 To fix Interface I-300 / I-300 Pro, VacuBox and Legacy- Box on lab stand, Rotavapor® R-21x or Vacuum Pump V-7xx. Incl. support, fixing clamp. Holder, set. To fix Interface and Woulff bottle on...
  • Page 92 Vapor temperature sensor. Incl. cap nut, seal 11060707 GL14 Measures the vapor temperature inside the system. Meant to be used with the Interface I-300 / I-300 Pro. Woulff bottle. 125 mL, P+G, incl. holder 11059905 For trapping particles and droplets and for pressure equalization.

  • Page 93: Wearing Parts

    Tubing. FEP, Ø6/8 mm, transparent, 40 mm 11059909 Connection tubing Woulff bottle. 10.2.3 Spare parts Further spare parts Order no. Image Holder. For valve unit/Woulff bottle 11059908 To fasten valve unit or Woulff bottle. Operation Manual Interface I-300 Pro 93/102...

  • Page 94: Health And Safety Approval

    I-300/I-300 Pro and Recirculating Chiller F-305/ F-308/F-314. VacuBox. Incl. support set 11060914 Communication interface between Rotavapor® R-300 and Interface I-300/I-300 Pro or Vacuum Pump V-300/ V-600 and Interface I-300/ I-300 Pro. Support foam sensor, Incl. clamping nut, support 11059024 ring...
  • Page 95 — we have taken all measures necessary to prevent potential hazards in respect of the products returned. Company name or stamp: Place, date: Name (block letters), position (block letters): Signature: Operation Manual Interface I-300 Pro 95/102...

  • Page 96: Handling Data

    The following communication details relate to Version 1.0 of the interface. Information is subject to amendment in respect of extent and content. NOTE External control of the equipment via the BUCHI Cloud is not implemented. Data transmission via the LAN interface to the server Category...

  • Page 97: Counter Data

    — Duty hours of instruments in the system — Max. readings for temperature and current 10.5.2 Data configuration settings Destination host connect.buchi.com Destination port Protocol HTTPS (TLS 1.2) Certificates RSA 2048 bit, SHA-256 Server location Ireland (Operator: Amazon Web Services) Operation Manual Interface I-300 Pro 97/102...

  • Page 98: Device Settings

    — E-mail address — Phone number — Company — Data protection and policy agreement for user — Agreement regarding the sending of marketing material 10.5.10 Location data — The coordinates of the mobile device. 98/102 Operation Manual Interface I-300 Pro...

  • Page 99: Accessories

    Vacuum is adjusted according to cooling capacity of condenser. Meant to be used with the Interface I-300 / I-300 Pro and glass assembly V, HP or S. Communication cable. BUCHI COM, 0.3 m, 6p 11058705 Enables connection between Rotavapor®...
  • Page 100 Interface I-300 / I-300 Pro. Holder. To fix interface on lab stand 11059021 To fix Interface I-300 / I-300 Pro, VacuBox and Legacy- Box on lab stand, Rotavapor® R-21x or Vacuum Pump V-7xx. Incl. support, fixing clamp. Holder, set. To fix Interface and Woulff bottle on...
  • Page 101 Vapor temperature sensor. Incl. cap nut, seal 11060707 GL14 Measures the vapor temperature inside the system. Meant to be used with the Interface I-300 / I-300 Pro. Woulff bottle. 125 mL, P+G, incl. holder 11059905 For trapping particles and droplets and for pressure equalization.
  • Page 102 T +971 4 313 2860 T +52 55 9001 5386 F +66 2 862 08 54 F +971 4 313 2861 latinoamerica@buchi.com bacc@buchi.com middleeast@buchi.com www.buchi.com/es-es www.buchi.com/th-th www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...

This manual is also suitable for:

I-300Interface i-300 pro

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