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SI Analytics TITRONIC 300 Operating Manual

Piston burette
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Summary of Contents for SI Analytics TITRONIC 300

  • Page 2 Gebrauchsanleitung ....................Seite 3 ... 52 Wichtige Hinweise: Die Gebrauchsanleitung ist Bestandteil des Gerätes. Vor der ersten Inbetriebnahme bitte sorgfältig lesen, beachten und anschließend aufbewahren. Aus Sicherheitsgründen darf das Gerät ausschließlich für die beschriebenen Zwecke eingesetzt werden. Bitte beachten Sie auch die Gebrauchsanleitungen für eventuell anzuschließende Geräte.

  • Page 3: Table Of Contents

    TABLE OF CONTENT ® Technical Specifications of the TITRONIC 300 Piston Burette ......55 Summary ..........................55 ® Specifications Piston burette TITRONIC 300 ................ 56 Warning and safety information ....................58 Unpacking and First Operation ................59 Unpacking and First Operation of the Piston Burette .............. 59 Connection and installing of Piston Burette and magnetic stirrer TM 50 ........
  • Page 4 ® Maintenance and Care of the TITRONIC 300 Piston Burette ......102 Storage and transportation ................. 103 10 Recycling and Disposal ..................103 11 Index ........................104 Notes to the Manual The provided manual will allow you the proper and safe handling of the titration instruments. The pictogram has the following meaning: ...

  • Page 5: Technical Specifications Of The Titronic 300 Piston Burette

    ® Technical Specifications of the TITRONIC 300 Piston Burette Summary ® The TITRONIC 300 is a piston burette and suitable for the following applications:  Manual titration with or without calculation of the result  Dosage  ® It can be used as a dosing burette with the TitroLine 7750 Titrator ...

  • Page 6: Specifications Piston Burette Titronic ® 300

    1200, 2400, 4800, 9600, 19200 (Default 4800 baud) Address: adjustable, (0 to 15, default: 01) RS-232-1 for computer, input Daisy Chain  RS-232-2 devices of SI Analytics, titrator TitroLine 7750,    - Burettes TITRONIC 500, TITRONIC 110 plus, TITRONIC...
  • Page 7 Housing material: Polypropylene Front keyboard: Polyester Housing dimensions: 135 x 310 x 205 mm (w x h x d), height incl. cylinder, excluding stirrer Weight: ca. 2 kg for basic unit Ambient conditions: Ambient temperature: + 10 ... + 40 °C for operation and storage Humidity according to EN 61 010, Part 1: Max.

  • Page 8: Warning And Safety Information

    1.3 Warning and safety information  The Piston Burette TITRONIC 300 corresponds to protection class III. It was manufactured and tested according to DIN EN 61 010, Part 1, Protective Measures for electronic measurement devices and control devices s and has left the factory in an impeccable condition as concerns safety technology.

  • Page 9: Unpacking And First Operation

    Unpacking and First Operation 2.1 Unpacking and First Operation of the Piston Burette The piston burette itself as well as all related accessory and peripheral parts have been carefully checked at the factory to ensure their correct function and size. Please ensure that the small accessories are also removed in full from the packaging.

  • Page 10: Connecting The Piston Burette - Combination With Accessories And Additional Devices

    The burette TITRONIC® 300 offers the following interfaces: Two RS232 interfaces, 4-channel (Mini-DIN): 1) For connection of a weighing balance and other devices from von SI Analytics (burettes,etc.) 2) RS1 for connection to the PC 3) One USB-A (“Host“) interface for connecting USB devices such as a keyboard, printer, manual control...

  • Page 11: Setting The Language Of The Country

    2.4 Setting the Language of the Country The ex-factory default language setting is English. When the piston burette is switched on, the main menu will appear once the boot sequence is completed: Fig. 4 Using <MODE>, followed by <System settings> you navigate to the system settings. The very first menu is to be used for setting the language of the country: Fig.
  • Page 12 Fig. 7 The selected language will appear immediately. Pressing the <ESC> key twice will return the user to the main menu.

  • Page 13: Dosing Unit And Accessories

    2.5 Dosing unit and Accessories Fig. 8 TZ 2003 - drying tube TZ 3282 - dosing hose without dosing tip and holding bracket TZ 3802 - threaded cap with borehole GL 45, incl. adapter with 2 openings for drying tube and suction hose TZ 1748 - stand rod Z 305 - titration clamp...

  • Page 14: Initial Filling Or Rinsing Of The Dosing Unit

    2.6 Initial Filling or Rinsing of the Dosing unit The dosing unit and the tubes are already mounted and ready-to-use. After the reagent bottle is connected, the initial filling of the dosing unit can be performed. While performing the initial filling or washing program, an adequately sized waste bin has to be placed below the titration tip.
  • Page 15 Fig. 12 Fig. 13 Fig 14 Fig. 15 The rinsing program (Fig.12-15) can be canceled at all time with <STOP> and the continued with <START>. When the rinsing is finished, you can get back to the start menu by pushing 2 x<ESC>.

  • Page 16: Working With The Piston Burette Titronic® 300

    Working with the Piston burette TITRONIC® 300 3.1 Front Keyboard Fig. 16 Apart from alphanumeric input (a-z, A-Z, 0-9) and a few other functions, almost all functions can be performed using the front keyboard. <Mode>: Methods selection, rinsing, system settings, balance data <EDIT>: Changing the current method, new method, copy and delete method, standard methods <ESC>:...

  • Page 17: Manual Controller

    3.3 Manual controller The manual controller (Fig. 18) is needed for manual titration. It can also be used for starting dosage or other methods. Fig. 18 Mode Black key Grey Key Manual titration Start of titration, single-step and Filling continuous titration (please refer to Stop of titration including evaluation chapter 3.6.1, manual titration) Dosage through Dosage method...

  • Page 18: Menu Structure

    3.5 Menu Structure There are 4 selection menus:  Start or main menu  Method parameters  Method selection  System settings After power-up, the main menu is always the first menu to appear. The method displayed will always be the last method that was used (Fig.
  • Page 19 <MODE>/F6 will take you to the method selection menu (Fig. 21). Fig. 21 Existing methods can be selected by pressing the <↓> und <↑> keys and confirming the selection with <OK>/<ENTER>. Once the selection made, you will return to the main menu with the newly selected method. If no method is selected, <ESC>...

  • Page 20: Main Menu

    3.6 Main Menu After power-up, the main menu is always the first menu to appear. The method displayed will always be the last method that was used (Fig. 24). In the present case it was a titration method. Fig. 24 3.6.1 Manual Titration Manual titration is always performed using the manual controller.
  • Page 21 Fig. 27 The balance data can be input using the front keyboard or the external keyboard. Please confirm your selection using <OK>/<ENTER>. In the case of automatic takeover of the weighing-balance data, the sample weights will be read out of the balance data memory.

  • Page 22: Dosage

    Fig. 30 Stage 5 corresponds to maximum titration speed. Speed is reduced by 50% each time. Example: 20 dosing unit: Stage 5 40.00 ml/min Stage 4 20.00 ml/min Stage 3 10.00 ml/min Stage 2 5 ml/min Stage 1 2.5 ml/min As soon as manual titration is completed, press the <STOP/F2>...
  • Page 23 Fig. 33 Fig. 34 The dosed volume will be briefly displayed before the display returns to the main menu. The next dosage operation can be started immediately. Filling of the unit following dosage will not occur automatically, unless the maximum cylinder volume has been reached or the automatic filling option (“always") was activated.
  • Page 24 Fig. 36 Further dosages can be performed using <OK> or <ENTER.> Filling of the unit following dosage will not occur automatically here, unless the maximum cylinder volume has been reached. The unit can be filled at any time using <FILL>. <ESC> will take you back to the main menu.

  • Page 25: Method Parameters

    Method Parameters From the main menu shown in (Fig. 32), <EDIT> will take you to the method parameters: Fig. 37 4.1 Method editing and new method If you select <edit method> or <new method> you will be taken to the modification or new creation of a method. Selecting <new method>...

  • Page 26: Default Methods

    4.2 Default Methods ® The <Default methods> item of the TITRONIC 300 contains a series of ready-made standard methods which can be conveniently selected (Fig. 39). Fig. 39 Once the selection made, you are directly prompted for the input of the method name (Fig. 40). Fig.

  • Page 27: Delete Methods

    4.4 Delete Methods If this function is selected, you will be prompted to know whether the current method is actually to be deleted. You have to reply <Yes> in explicit terms and also confirm this reply with <OK>/<ENTER>. Fig. 42 4.5 Change Method Parameters The input or modification of the method name was already described in Chapters 4.1 and 4.3.

  • Page 28: Result (Only For Manual Titration)

    4.5.2 Result (only for manual Titration) The <Result> menu offers the following possible settings: Fig. 45 The Result text may contain up to 21 alphanumeric characters including special characters. Fig. 46 Please confirm your input with <OK</<ENTER>. 4.5.2.1 Formulae for manual titration On the Formula Selection submenu you can select the appropriate calculation formula: Fig.
  • Page 29 terms of ml. Reverse titration (examples. CSB, saponification number) (B*F3–ml*F1)*T*M/(W*F2) Formula for calculating the concentration of a sample taking into account a blank value, including a multiplicative factor. Reverse titration. (W*F2)/(ml-B)*M*F1) Formula for calculating a titer (T) of a titration solution.
  • Page 30 4.5.2.2 Sample weight and volume (sample quantity) Fig. 50 Fig. 51 The Sample Quantity (W) item is used to select whether one is wishing to use a sample weight or a sample volume for titration or solution preparation. You have the following options (Fig. 51): ...
  • Page 31 Once the selection made (e.g. %), the unit will also be displayed as piece of information on the display. Fig. 53 4.5.2.4 Decimal digits To conclude, it is possible to determine the number of decimal digits from 2-6. The standard setting is 2. 4.5.2.5 Global Memories If a titration result should be used again later, e.g.
  • Page 32 Fig. 56 MO1 can either be accepted or substituted by a designation of a blank value or a titer. Fig. 57 This value can be used with the formula. Fig. 58 The blank value, being titrated previously is always taken into account automatically. Fig.

  • Page 33: Dosing Parameters

    4.5.3 Dosing parameters Fig. 60 The dosing parameters (dosing speed, filling speed and max. dosing/titration volume) are determined for each method. This applies to both types of methods such as manual titration and dosage. Fig. 61 The dosing speed can be set as a function of the interchangeable unit in terms of ml/min from 0.1 to 100 ml/min. Dosing unit Max.

  • Page 34: Sample Identification

    4.5.4 Sample identification In the manual titration it is possible to input a sample identification. The possible input includes manual, automatic or no sample identification at all. Fig. 62 For the manual sample ID, a prompt for the sample ID will always be displayed at the start of the method (Cp. also chapter 3.6, Main menu).
  • Page 35 Fig. 65 Method type Short documentation Standard documentation GLP-Documentation Same as ‘Short Manual titration Method name, date, time, sample documentation’ + description, sample weight/sample volume, results and calculation plus method contents formula Dosing Only method printout, Method name, date, time, dosing parameters The documentation can also be stored in PDF and CSV-files on a connected USB stick.

  • Page 36: System Settings

    System Settings Fig. 66 From the main menu (Fig. 66), press <MODE> followed by <System settings> (or with the external keyboard connected, press F7) you get to the system settings: Fig. 67 Setting the national language was already described in Chapter 2.5. 5.1 Reagents/Dosing Unit In this menu you can set the size of the dosing unit (20 or 50 ml), perform an exchange of the dosing unit and enter reagents data, being stored during manual titration in the GLP documentation.
  • Page 37 Fig. 69 Chose <Dosing unit exchange>. Warning: The exchange of the dosing unit starts without any warning. Therefor please place the titration tip in a reagents bottle or beaker. The piston is moving up to 85%. Fig. 70 Then the system prompts to unlock the dosing unit. Fig.
  • Page 38 After the unit is unlocked, confirm with <OK>. The unit will move up the whole way. Fig. 72 Pull off the dosing unit and attach the new one just like it was before. The two struts of UV protection must comply with the mark on the housing (Fig.73).
  • Page 39 Fig. 75 After this procedure the dosing unit is moving back down again. Please lock the dosing unit. Abb. 76 The following reagents data can be chosen:  Unit size 20 or 50 ml (adjustable)  Reagent name: (default: blank) ...

  • Page 40: Global Memories

    Fig. 77 5.2 Global Memories Please refer to chapter 4.5.2.5. 5.3 RS232 Settings ® The <RS232 settings> item can be used to determine the device address of the TITRONIC 300 and set the parameters of the two RS232 interfaces separately: Fig.
  • Page 41 Fig. 80 The baud rate is preset to 4800. It may be set to 1200 – 19200: Fig. 81 The parity setting can be selected amongst <No>, <Even> and <Odd>. <No> is the standard setting. Fig. 82 You may select between 7 and 8 data bits. 8 bits is the standard setting. Fig.

  • Page 42: Connection Of Printers

    The stop bits can be set to 1, 1,5 and 2. The default setting is 1. Abb. 84 Selecting <Reset RS Parameters> will reset the RS232 parameters to the factory settings. Connection of Printers The results and methods can be printed on the following media: ...

  • Page 43: Reset

    Fig. 86 5.6 RESET RESET will reset all settings to the factory setting. Please note: All methods will also be deleted. So please print the methods or export/copy them to a connected USB storage medium (refer to chap. 5.9). The RESET has to be confirmed separately once again: Fig.

  • Page 44: System Sounds

    5.8 System Sounds The system tone can be switched on and off. Fig. 89 5.9 Data exchange All methods with all parameter settings and global memories can be stored and restored on a connected USB- memory. It is also possible to transfer the settings from one titrator to another one. The backup will be started with Settings backup: Abb.

  • Page 45: Software Update

    Die Sicherungsdatei bekommt einen Zeitstempel. Die Sicherungsdatei auswählen und sofort werden die Einstellungen übertragen bzw. wieder hergestellt: Abb. 92 Abb. 93 5.10 Software Update Fig. 94 An update of the device software requires a USB stick containing a new version. For this operation, the two files that are needed have to be located in the root directory of the USB stick:...
  • Page 46 Plug the USB stick into a free USB-A port, wait for some seconds, and then select the Software Update function. The valid software updates will be shown on the display. In the present case this is Version „14_29“ from week 29, year 2014.
  • Page 47 Fig. 98 Upon completion of the update (approx. 2-3 minutes), the device will shut down the software completely and proceed to a new start. Please note: During the update, the device must not be switched off. Important: In the course of an update, the methods will not be deleted! You can continue to use them. If no valid update file is stored on the USB stick, the following message will appear: Fig.

  • Page 48: Connection Of Analytical Balances

    Connection of Analytical Balances As it often happens that the sample is weighed in on an analytical balance, it makes sense to connect this ® ® balance to the TITRONIC 300. To connect the balance to the TITRONIC 300, the balance must have a RS- 232-C-interface and the connection cable must be configured accordingly.
  • Page 49 Fig.100 The balance data can be edited one by one. Following a change, a star will appear opposite the weighed-in quantity: Fig. 101 Weights may be deleted or added individually. It is also possible to delete all weights at one stroke. Fig.

  • Page 50: Data Communication Via Rs-232- And Usb-B Interface

    PC. Then the USB-B interface takes over the function of the RS232-1 interface. Please contact SI Analytics for acquiring the software. The address always consists of two characters: e.g. address 1 of the two ASCII- characters <0> and <1>. The addresses can be set from 00 to 15, i.e.

  • Page 51: Instruction Set For Rs-Communication

    (short report) aaLI output method content aaLO output documentation (as configured) aaRH request of identification aaIdent: TITRONIC 300 aa“last command“ aaRC send last command aaRS report status aaStatus:“text possible answers are: „STATUS:READY“ for ready „STATUS:dosing“ dosing „STATUS:filling“...
  • Page 52 ® Maintenance and Care of the TITRONIC 300 Piston Burette The preservation of the proper functioning of the piston burette requires testing and maintenance work to be performed on a regular basis. Regular inspections are essential prerequisites for the correctness of the volume and the proper functioning of the piston burette.
  • Page 53 Please note: The main printed board carries a lithium battery. Batteries should not to be disposed of with the normal domestic waste. They will be taken back and recycled or disposed of properly by the manufacturer at no cost. Should you have any questions regarding disposal, please contact SI Analytics.
  • Page 54 Index analytical balance 60 manual controller 67 Balance data editor 98 manual controller TZ 3880 60 Care 102 Manual Titration 70 change method parameters 77 max. dosing/titration volume 83 Connection of Analytical Balances 98 method name 75 Connection of Printers 92 method parameters 75 copy methods 76 new method 75...
  • Page 56 Xylem Analytics Germany Sales GmbH & Co.KG SI Analytics Gebäude G12, Tor Rheinallee 145 55122 Mainz Germany Tel. +49.(0)6131.66.5042 Fax. +49.(0)6131.66.5105 E-Mail: Service-Instruments.si-analytics@xyleminc.com SI Analytics is a trademark of Xylem Inc. or one of its subsidiaries. © 2016 Xylem, Inc. Version 160824 US...

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