SI Analytics TitroLine 6000 Operating Instructions Manual
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SI Analytics TitroLine 6000 Operating Instructions Manual

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TitroLine® 6000/7000
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Summary of Contents for SI Analytics TitroLine 6000

  • Page 1 OPERATING INSTRUCTIONS TitroLine® 6000/7000 TITRATOR...
  • Page 2 Wichtige Hinweise: Important notes: Instructions importantes: Instrucciones importantes: Copyright...
  • Page 3 Technical Specifications of the Titrator TitroLine® 6000/7000 ......89 Unpacking and First Operation ................94 ® Working with the Titrator TitroLine 6000/7000 ..........107 Method Parameters ....................121 System settings ..................... 152...
  • Page 4 Data Communication via RS-232- and USB-B interface ........162 Connection of Analytical Balances and Printers ..........164 ® Maintenance and Care of the TitroLine 6000/7000 ..........168 Storage and transportation................... 169 10 Recycling and Disposal..................169 11 Index ........................170 Declaration of conformity last page of the document Notes to the Manual...
  • Page 5 Technical Specifications of the Titrator TitroLine® 6000/7000 1.1 Summary Solutions to be used: General provisions: Guarantee...
  • Page 6 ® 1.2 Specifications Titrator TitroLine 6000/7000 CE sign: Country of origin...
  • Page 7 Display: Power supply: RS-232-C Interface / none 4800 (0 to 15, default: 01) plus, universal USB Interface: Stirrer connection 12V DC out 500mA Housing material: Front keyboard: Housing dimensions: Weight: Ambient conditions:...
  • Page 8 Interchangeable units Dosing accuracy of the Titrator TitroLine 6000/7000 with WA interchangeable units:...
  • Page 9 Chapter 1 – Specifications Titrator TitroLine 6000/7000 1.3 Warning and safety information ® In the case of nonobservance of these provisions the titrator TitroLine 6000/7000 may constitute a danger: electrical accidents of persons or fire hazard. Moreover, in the case of unauthorised ®...
  • Page 10 Chapter 2 - Unpacking and first Operation 2 Unpacking and First Operation 2.1 Unpacking and First Operation of the titrator 2.2 Installing the Z 300 Rod Foot Plate (Optional)
  • Page 11 Chapter 2 - Unpacking and first Operation 2.3 Connection and installation of titrator and magnetic stirrer TM 235...
  • Page 12 Chapter 2 - Unpacking and first Operation 2.4 Connecting the Titrator - Combination with Accessories and Additional Devices ® 2.4.1 Back panel of the titrator TitroLine 6000/7000 ® 2.4.2 Connection ports of the TitroLine 6000/7000 2.4.3 Connecting a printer have to 2.4.4 Connecting a USB device (manual controller, keyboard, memory device, hub)
  • Page 13 Chapter 2 - Unpacking and first Operation 2.4.5 Connection of analytical balances ® 2.4.6 Connection of SI Analytics ID electrodes to TitroLine 7000 2.5 Setting the Language of the Country...
  • Page 14 Chapter 2 - Unpacking and first Operation...
  • Page 15 Chapter 2 - Unpacking and first Operation 2.6 Interchangeable unit WA 2.6.1 Installing the interchangeable unit...
  • Page 16 Chapter 2 - Unpacking and first Operation 2.7 Positioning and Replacing an Interchangeable Unit 2.7.1 Placing an interchangeable unit...
  • Page 17 Chapter 2 - Unpacking and first Operation 2.7.2 Removing an interchangeable unit ! Please note: Removing the interchangeable unit is only possible as long as the piston is in the lower position (zero position). Possibly, it may be necessary to press the <FILL> key first. ! 2.7.3 Programming the titration unit...
  • Page 18 Chapter 2 - Unpacking and first Operation...
  • Page 19 Chapter 2 - Unpacking and first Operation 2.8 Initial Filling or Rinsing of the Entire Interchangeable Unit...
  • Page 20 Chapter 2 - Unpacking and first Operation...
  • Page 21 Chapter 2 - Unpacking and first Operation 2.9 Replacing the Glass Cylinder and the PTFE Piston...
  • Page 22 Chapter 2 - Unpacking and first Operation Warning...
  • Page 23 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 ® 3 Working with the Titrator TitroLine 6000/7000 3.1 Front Keyboard <Mode>: <EDIT> <ESC>: <ESC <START> <FILL> Chapter 3.4, External PC Keyboard 3.2 Display...
  • Page 24 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.3 Manual controller “mouse“ 3.4 External PC Keyboard Keys Function <ESC <ESC...
  • Page 25 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.5 Menu Structure...
  • Page 26 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 27 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.6 Main Menu 3.6.1 Automatic Titration...
  • Page 28 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 29 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.6.2 Calibration (CAL menu)
  • Page 30 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 31 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 32 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.6.3 Manual Titration <START>/<F1> Chapter 3.6.1...
  • Page 33 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 Example: WA 20 interchangeable unit: 3.6.4 Dosage...
  • Page 34 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 35 ® Chapter 3 – Working with the titrator TitroLine 6000/7000...
  • Page 36 ® Chapter 3 – Working with the titrator TitroLine 6000/7000 3.6.5 Preparing Solutions...
  • Page 37 Chapter 4 Method Parameters 4 Method Parameters 4.1 Method editing and new method Chapter 4.5 4.2 Default methods...
  • Page 38 Chapter 4 Method Parameters Chapter 4.5 4.3 Copy Methods Chapter 4.5 4.4 Delete Methods <Yes>...
  • Page 39 Chapter 4 Method Parameters 4.5 Print method 4.6 Change Method Parameters Chapters 4.1 4.6.1 Method type...
  • Page 40 Chapter 4 Method Parameters 4.6.2 Titration mode 4.6.2.1 Linear titration 4.6.2.2 Dynamic titration...
  • Page 41 Chapter 4 Method Parameters 4.6.2.3 End-point titration 4.6.2.4 pH Stat Titration...
  • Page 42 Chapter 4 Method Parameters 4.6.3 Result...
  • Page 43 Chapter 4 Method Parameters only total consumption Formula“ Result text...
  • Page 44 Chapter 4 Method Parameters 4.6.3.1 Calculation Formula Formula selection...
  • Page 45 Chapter 4 Method Parameters Formula for linear and dynamic Formula for titrations to end- Additional information titration to EQ1 point (EP 1 and EP2)
  • Page 46 Chapter 4 Method Parameters Formela for linear and dynamic Hinweis titration to EQ2...
  • Page 47 Chapter 4 Method Parameters...
  • Page 48 Chapter 4 Method Parameters 4.6.3.2 Sample weight and volume (sample quantity)
  • Page 49 Chapter 4 Method Parameters Manual sample weight Automatic sample weight: Fixed sample weight Manual sample volume Fixed sample volume 4.6.3.3 Formula unit Unit...
  • Page 50 Chapter 4 Method Parameters 4.6.3.4 Formulae for the Preparation of Solutions W*(100-Fa-Fb)*Fc/Fd - W*(100-Fb) / (100*Fe) +Ff W*(100-Fa-Fb)*(Fd/Fg ) - W*(100-Fb) / (100*Fg) +Ff W*(100-Fa-Fb)*Fc / (100*Fd) Note on volume correction:...
  • Page 51 Chapter 4 Method Parameters 4.6.3.5 Decimal digits 4.6.3.6 Statistics...
  • Page 52 Chapter 4 Method Parameters 4.6.3.7 Global Memories <Enter/OK> <Ins> “M01” “blank value”...
  • Page 53 Chapter 4 Method Parameters 4.6.4 Titration parameters <Titration parameter>...
  • Page 54 Chapter 4 Method Parameters Generally applicable titration parameters <Measured value> <Measuring speed>...
  • Page 55 Chapter 4 Method Parameters norma ”user- defined”...
  • Page 56 Chapter 4 Method Parameters <Initial waiting time> Dynamic control...
  • Page 57 Chapter 4 Method Parameters Attenuation setting...
  • Page 58 Chapter 4 Method Parameters Linear titration Titration direction increase decrease increase decrease Pretitration <Pretitration>...
  • Page 59 Chapter 4 Method Parameters Titration end End value slope value Maximum titration volume...
  • Page 60 Chapter 4 Method Parameters maximum titration volume...
  • Page 61 Chapter 4 Method Parameters 4.6.5 ‘End-point titration’ and ‘dead-stop titration’ titration parameters Dead-Stop Titration and Polarisation voltage...
  • Page 62 Chapter 4 Method Parameters ® 4.6.6 Titration parameter pH Stat Titration (only TitroLine 7000)
  • Page 63 Chapter 4 Method Parameters Important: Determination of Enzyme Activity...
  • Page 64 Chapter 4 Method Parameters...
  • Page 65 Chapter 4 Method Parameters 4.6.7 Dosing parameter Interchangeable unit Max. dosing speed [ml/min]...
  • Page 66 Chapter 4 Method Parameters 4.6.8 Sample identification...
  • Page 67 Chapter 4 Method Parameters 4.6.9 Documentation Method type Short documentation Standard GLP-Documentation documentation...
  • Page 68 Chapter 5 - System Settings 5 System settings Chapter 2.5 5.1 Calibration settings...
  • Page 69 Chapter 5 - System Settings...
  • Page 70 Chapter 5 - System Settings 5.2 Interchangeable Unit - Reagents...
  • Page 71 Chapter 5 - System Settings...
  • Page 72 Chapter 5 - System Settings 5.3 RS232 Settings...
  • Page 73 Chapter 5 - System Settings...
  • Page 74 Chapter 5 - System Settings 5.4 Date and Time 5.5 Password 5.6 RESET Please note: connected USB storage medium (this will be possible with a higher update!).
  • Page 75 Chapter 5 - System Settings 5.7 Printer 5.8 Device Information 5.9 System Tone...
  • Page 76 Chapter 5 - System Settings 5.10 Software Update...
  • Page 77 Chapter 5 - System Settings Important:...
  • Page 78 Chapter 6 Data Communication via RS-232 and USB-B interface 6 Data Communication via RS-232- and USB-B interface 6.1 General Information PIN-No. Meaning / Description 6.2 Chaining multiple devices —“Daisy Chain Concept“ Chapter 5.3 6.3 Instruction Set for RS-Communication Every...
  • Page 79 Chapter 6 Data Communication via RS-232 and USB-B interface Command Description Reply “text...
  • Page 80 Chapter 7 – Connection of Analytical Balances and Printers 7 Connection of Analytical Balances and Printers Connection of Analytical Balances 7.1.1 Balance TZ-Number...
  • Page 81 Chapter 7 – Connection of Analytical Balances and Printers 7.2 Balance data editor <F5/balance symbol >...
  • Page 82 Chapter 7 – Connection of Analytical Balances and Printers 7.3 Connection of Printers ® Connection of Autosampler (only TitroLine 7000 7.4.1 Connection of sample changer TW alpha plus TZ 3087...
  • Page 83 Chapter 7 – Connection of Analytical Balances and Printers 7.4.2 Connection of sample changer TW 7400 TZ 3987 ® 7.5 Using software TitriSoft (only TitroLine 7000) 7.5.1 General 7.5.2 TitriSoft 3.0 7.5.3 TitriSoft 2.75...
  • Page 84 Chapter 8 – Maintenance and Care ® 8 Maintenance and Care of the TitroLine 6000/7000 Heavy strain: Normal strain: Interrupted use...
  • Page 85 Kapitel 8 Lagerung und Transport Kapitel 7 Wartung und Pflege des Titrators Kapitel 7 Wartung und Pflege des Titrators Chapter 9 – Storage and Transportation Please note: Storage and transportation 10 Recycling and Disposal Please note:...
  • Page 86 Chapter 11 – Index 11 Index...
  • Page 88 ® Typ / type / type / tipo TitroLine 6000/7000 Bescheinigung des Herstellers Supplier’s Certificate Certificat du fournisseur Certificado del fabricante SI Analytics GmbH...

This manual is also suitable for:

Titroline 7000

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