Ankom XT15 Operator's Manual

Ankom XT15 Operator's Manual

Designed to extract crude (free) fat
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Operator's Manual
Rev F 5/9/17
2052 O'Neil Rd, Macedon NY 14502
Telephone: (315) 986-8090
Fax: (315) 986-8091
www.ankom.com

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Summary of Contents for Ankom XT15

  • Page 1 Operator’s Manual Rev F 5/9/17 2052 O’Neil Rd, Macedon NY 14502 Telephone: (315) 986-8090 Fax: (315) 986-8091 www.ankom.com...
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  • Page 3: Table Of Contents

    Instrument Installation ..............................9 Fat Extraction Calculations ............................10 Fat Extraction Support Items ............................10 Sample Preparation ..............................11 XT15 Fat Extraction step-by-step procedure using the ANKOM ..................17 Periodic Maintenance ..............................21 Troubleshooting & Replacement Parts ........................23 Diagnostics .................................. 24...
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  • Page 5: Introduction

    Use only ANKOM Technology filter bags (part # XT4) in your ANKOM Extraction System. Use of any other filter mechanism will void the warranty. Filter bags can be purchased from ANKOM Technology or from your local authorized ANKOM distributor. Operating Environment...
  • Page 6: Contact Information

    At ANKOM Technology we are committed to your total satisfaction and therefore always available to help you get the most from your ANKOM products. We are also very interested in any comments or suggestions you may have to help us improve.
  • Page 7: Instrument Description

    XT15 The quantitative isolation achieved by the filter bag permits the ANKOM Extraction System to automatically process samples in batches of up to 15. With the solvent reservoir filled, simply place filter bags with sample in the Extraction Vessel, lock the vessel in place, select the extraction time and temperature, and press “Start.”...
  • Page 8: Safety Precautions

    WARNING: Attempts to override safety features or to use this instrument in a manner not specified by ANKOM Technology voids the warranty and may result in serious injury or even death. This system is designed to meet and/or exceed the applicable standards of CE, CSA, NRTL and OSHA.
  • Page 9: Instrument Installation

    Operator’s Manual Instrument Installation Site Requirements XT15 To install and operate the ANKOM Extraction System you will need the following:  Adjustable wrench  Chilled or tap water supply not to exceed 23°C  Adequate power (see “Operating Environment” section) ...
  • Page 10: Fat Extraction Calculations

    Blank filter bag dry weight after hydrolysis Blank filter bag weight after extraction The Hydrolysis procedure can be found in the ANKOM HCl Operator's Manual. Fat Extraction Support Items The following support items are needed to perform the fat extraction procedure:...
  • Page 11: Sample Preparation

    (as shown to the right). If the seal is not strong, re-seal the bag. Repeat steps 1 – 7 for all filter bags that will be used in the ANKOM XT15 Extraction System.
  • Page 12 Operator’s Manual Sample Preparation Procedure for Crude Fat – To prepare meat samples with > 15% fat by weight or plant samples with > 20% fat by weight for fat extraction, follow the procedure detailed below. Using a Solvent Resistant Marker, number all of the weigh tins and empty filter bags you will use during the fat extraction procedure.
  • Page 13 (as shown to the right). If the seal is not strong, re-seal the bag. 12. Repeat steps 1 – 11 for all filter bags that will be used in the ANKOM XT15 Extraction System.
  • Page 14 (as shown to the right). If the seal is not strong, re-seal the bag. Repeat steps 1 – 8 for all filter bags that will be used in the ANKOM XT15 Extraction System.
  • Page 15 Operator’s Manual 10. Dry all samples at 102°C±2° for 3 hours to remove moisture prior to the extraction. 11. Remove the samples from the oven and place them in a Desiccant Pouch. 12. Allow the samples to cool to room temperature. This should take about 10 – 15 minutes.
  • Page 16 Operator’s Manual This page intentionally left blank pg. 16 Rev F 5/9/17...
  • Page 17: Fat Extraction Step-By-Step Procedure Using The Ankom Xt15

    Operator’s Manual XT15 Fat Extraction step-by-step procedure using the ANKOM To perform fat extraction on prepared samples, follow the procedure detailed below. Turn the instrument power ON. PET Ether The Display will briefly show the software version number followed <ENTER>...
  • Page 18 Operator’s Manual 3. Insert Filter Bags into the instrument. Press down the Safety Valve Handle to release the Safety Valve Pin and rotate the Main Handle upward until it stops. Use the Extraction Vessel Handle to pull the Extraction Vessel out.
  • Page 19 Operator’s Manual Slide the Extraction Vessel into the instrument ensuring the Extraction Vessel O-ring stays in place. Pull the Main Handle downward, closing and locking the Extraction Vessel in place. You will hear a click noise when the Safety Valve Pin locks in place.
  • Page 20 Remove the filter bags from the Bag Holder. Dry the samples for 15 – 30 minutes in the oven at 102 ± 2°C or in the ANKOM Dryer set at the factory setting of 110°C. Remove the samples from the oven or dryer and place them in a Desiccant Pouch.
  • Page 21: Periodic Maintenance

    Extraction Vessel. The vessel can most easily be cleaned by using a drill with a long shafted stiff wire brush (ANKOM part # X107). This treatment will remove a lot of the black coating that accumulates on the bottom of the vessel.
  • Page 22 3. Use compressed air to blow backwards through the filter (blow opposite the arrow on the filter). If the filter is clogged, replace it with ANKOM part # X97. 4. Reconnect the filter and fittings. 5. Turn on the water and check for leaks.
  • Page 23: Troubleshooting & Replacement Parts

    Operator’s Manual Troubleshooting & Replacement Parts The ANKOM technology web site has the most current troubleshooting and replacement parts information. XT15 Therefore, if you have any questions about the operation of your ANKOM Extraction System, or if you need replacement parts, please visit our web site at www.ankom.com.
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  • Page 25: Diagnostics

    Operator’s Manual Diagnostics XT15 To help solve problems that may occur while running the ANKOM Extractor, the following computer controlled Diagnostics are available and accessible through the Display and Keypad. Toggle Outputs (Q0 Heater Relay and Q1 - Q7 valves)
  • Page 26 Operator’s Manual Press the ENTER button on the Keypad to turn ON the heater relay Heater (Q0) (Q0). The screen to the right will be displayed. ENTER to toggle Press the ENTER button on the Keypad to turn OFF the heater Heater (Q0) relay (Q0).
  • Page 27 When the instrument has not been run for more than two hours, the temperature should read the ambient temperature of the room. If the temperature reading does not show ambient temperature when the instrument is cool, contact ANKOM Technology. When the Level Sensor in the instrument Vessel is not covered by liquid, the Level Sensor should read 10.00v.
  • Page 28 Press the ENTER button on the Keypad. The screen to the right ETS relay - ON will be displayed showing the state of the ETS relay. If the ETS relay is "OFF", contact ANKOM Technology. Press the STOP button on the Keypad to go back to the Inputs Inputs <ENTER>...
  • Page 29: Appendix A - Electrical Diagram

    Operator’s Manual Appendix A – Electrical Diagram (pg. 1 of 3) Rev F 5/9/17 pg. 29...
  • Page 30 Operator’s Manual Appendix A – Electrical Diagram (pg. 2 of 3) pg. 30 Rev F 5/9/17...
  • Page 31 Operator’s Manual Appendix A – Electrical Diagram (pg. 3 of 3) Rev F 5/9/17 pg. 31...
  • Page 32 Automation saves time and money! ANKOM Technology is an international company with products that include… TDF Dietary Fiber Analyzer  Automates AOAC 991.43/AACC 32.07.01  IDF/SDF and TDF values  Faster, Technician-free Filtering  Computer controlled operation  Reduced per assay costs A2000 Fiber Analyzer ...

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