WATERS CORPORATION TA Instruments DSC 2010 Manuals

WATERS CORPORATION TA Instruments DSC 2010 Manuals

Manuals and User Guides for WATERS CORPORATION TA Instruments DSC 2010. We have 1 WATERS CORPORATION TA Instruments DSC 2010 manual available for free PDF download: Operator's Manual

WATERS CORPORATION TA Instruments DSC 2010 Operator's Manual

WATERS CORPORATION TA Instruments DSC 2010 Operator's Manual (126 pages)

Differential Scanning Calorimeter

Brand: WATERS CORPORATION | Category: Measuring Instruments | Size: 2 MB

Table of Contents

Table of Contents
3
Notes, Cautions, and Warnings
9
Safety
10
Using this Manual
15
Introduction
19
Components
21
Introduction
21
The DSC 2010
21
The 2010 Instrument
22
2010 Instrument Keypad
23
2010 DSC Cell
25
POWER Switch
25
Accessories
26
Sample Encapsulating Press
26
Accessories for Subambient Operation
27
Lnca
27
Rcs
28
DSC Cooling Can
29
Specifications
30
Unpacking the 2010
35
Unpacking/Repacking the 2010
35
Repacking the 2010
38
Unpacking the DSC Cell
38
Inspecting the System
39
Installing the 2010 Instrument
39
Choosing a Location
40
Connecting Cables and Gas Lines
41
GPIB Cable
41
PURGE Line
44
Purge, Vacuum, and Cooling Gas Lines
44
COOLING GAS Line
45
VACUUM Line
45
Power Cable
47
Installations for Subambient Operation
48
Installing the DSC Cooling Can
49
Starting the 2010
52
Shutting down the 2010
53
CHAPTER 3: Running Experiments

55
- Overview
  57
- Before You Begin
  57
- Calibrating the DSC
  58
- Baseline Slope and Offset Calibration
  59
- Cell Constant Calibration
  60
- Temperature Calibration
  60
- Running a DSC Experiment
  61
- Experimental Procedure
  61
- Preparing Samples
  62
- Determining Sample Size
  62
- Physical Characteristics
  63
- Selecting Sample Pans
  63
- Sample Pan Material
  63
- Sample Pan Configuration
  65
- Nonhermetic Pans
  65
- Hermetic Pans
  65
- Open Pans
  66
- SFI Pans
  66
- Encapsulating the Sample
  66
- Preparing Nonhermetic Sample Pans
  67
- Preparing Hermetic Sample Pans
  70
- Setting up Accessories
  73
- Loading the Sample
  75
- Starting an Experiment
  77
- Stopping an Experiment
  77
- Subambient Experiments
  78
- DSC Cooling Can
  78
- Applications
  78
- Operation
  79
- Quench-Cooling between Runs
  79
- Starting a Run below Ambient Temperature
  80
- Programmed Cooling
  80
CHAPTER 4: Technical Reference

81
- Description of the DSC 2010
  83
- DSC Cell
  83
- Principles of Operation
  85
- Cell Block Heating
  85
- Sample and Reference Thermocouples
  86
- DSC Applications
  87
- Sample Types
  87
- Status Codes
  88
- Guidelines for Quantitative Studies
  92
- Specific Heat Experiments
  92
CHAPTER 5: Maintenance and Diagnostics

99
- Overview
  101
- Routine Maintenance
  102
- Inspection
  102
- Cleaning the Instrument Keypad
  102
- Cleaning a Contaminated Cell
  102
- Cleaning DSC Pans
  103
- Sample Encapsulating Press
  105
- Diagnosing Power Problems
  106
- Fuses
  106
- Power Failures
  107
- DSC 2010 Test Functions
  109
- 2010 Confidence Test
  109
- Replacement Parts
  111

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