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Thermo Scientific Sentinel PRO Manuals
Manuals and User Guides for Thermo Scientific Sentinel PRO. We have
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Thermo Scientific Sentinel PRO manual available for free PDF download: User Manual
Thermo Scientific Sentinel PRO User Manual (203 pages)
Mass Spectrometers
Brand:
Thermo Scientific
| Category:
Measuring Instruments
| Size: 4.9 MB
Table of Contents
Table of Contents
6
Chapter 1 Introduction
14
Chapter 2 Safety Information
16
Overview
16
Safety Conventions and Symbols
17
System Safety
18
Connecting the Instrument to the Electrical Supply
19
Repair & Maintenance
19
Changing the Rotary Pump Oil
19
Switching on the Rotary Pump
19
Rotary Pump Exhaust Outlet
20
Inlet System Exhaust
20
Gas Mixtures in the Inlet System
21
Protective Clothing
21
Hazardous Materials
21
Hazardous Area Systems
22
Fan Noise
22
Chapter 3 Site Requirements
24
Physical Installation
24
Cable Entries
25
Safe Area Systems
25
Hazardous Area Systems
25
Computer and Communications
25
Fibre Optic Communication
26
Hazardous Area Systems
26
Environment
27
General
27
Temperature
27
Humidity
27
Vibration
27
Particulate Contamination
27
Altitude
28
Inlet Gas Connections
28
Calibration Gases
28
Sample Gases
29
Exhaust Gas Connections
30
Power
31
Voltage and Frequency
31
Requirements
31
Over-Current Protection
33
Power Quality
33
Power Connection
33
Other Services
33
Safe Area Systems
33
Dry Gas Vent
33
Enclosure Purge
33
Hazardous Area Systems
34
Dry Gas Vent
34
Rotary Pump Purge
34
Compressed Air Requirements
35
Options
36
Pump Purge Gas
36
Rotary Oil Box Purge
36
Rotary Pump Ballast
36
Turbo Pump Bearing Purge
36
External I/O Unit
37
Chapter 4 Handling & Storage
38
Receiving the Instrument
38
Unpacking the Instrument
39
Storing the Instrument
39
Chapter 5 Installation & Interconnection
40
Introduction
40
Positioning the Instrument
40
Cable Connections
40
General Requirements
40
Safe Area Systems
40
Hazardous Area Systems
41
Power Connection
41
Safe Area Systems
41
Sentinel PRO Sample Pump Power Connection
43
Safe Area Systems
43
Hazardous Area Systems
43
Gas Connections
43
Computer System
44
Chapter 6 Commissioning
46
General
46
Procedure
46
Chapter 7 Startup & Shutdown
50
Startup
50
Procedure
50
Vacuum Gauge Trip Level
53
Checking Instrument Tuning and Mass Alignment
54
Emission
55
Peak Shape
55
Sensitivity
56
Detectors
57
Mass Alignment
57
Heaters
59
Shutdown
60
Introduction
60
Shutdown Procedure
60
Emergency Shutdown
61
Chapter 8 Status & Tuning Parameters
62
Instrument Status
62
Source Tab
63
Electron Energy
63
Emission
63
Filament Current
63
Filament Current Limit
63
Filament Integrity
64
In Current Limit
64
Ion Energy
64
Repeller Voltage
65
Source Current
65
Source Temperature
65
Trap Current
65
Analyser Tab
66
ASU Controller Status
66
Cabinet Temperature
66
Electronics Temperature
66
Magnet Controller Status
66
Mass Filter
67
Pressure Set Point
67
System Pressure
67
System Pressure Trip
68
Turbo Motor Current
68
Turbo Operating Hours
68
Turbo Speed
68
Turbo Speed Interlock
69
Vacuum
69
Vent Valve
69
Inlet
69
Pressure Raw
69
RMS Ambient Temperature
69
RMS Body Temp
69
RMS Controller Status
69
RMS Sample Flow Sensor
69
RMS Flow Zero
69
Sample Tube Temperature
70
Collector Tab
70
Faraday Deflector
70
Multiplier Deflector
70
Multiplier Voltage
70
Negative and Positive Quad Lens Voltages
70
Resolution
70
Power
71
Amplifier +24V
71
Analyser Supplies +24V
71
Instrument CPU 24V
71
Fan 24V
71
Inlet Probe Current
71
Magnet Supply Current
72
Magnet Sync AC
72
Power Controller Status
72
Turbo 24V
72
User IO 24V
72
Vent Valve 24V
72
Communications
72
Host Comms Quiet
72
User I/O 0 Comms Quiet
78
User I/O 1 Comms Quiet
78
User I/O 2 Comms Quiet
78
Chapter 9 Fault Diagnosis
78
Alarm Conditions
78
Leak Detection
79
Mass Spectrometer Faults
80
No Peaks
80
Poor Sensitivity
81
Poor Stability on Startup
81
Poor Results Following Calibration
82
Ion Source and Magnet Pole Pieces Assembly
83
Filament Failure
83
Chapter 10 Maintenance
86
Maintenance Schedule
86
Procedures
86
Rotary Pump Oil Level
86
Cleaning the Cooling Fans
87
Lubricating the Turbo Molecular Pump
88
Dismantling and Cleaning Procedures
88
Filament
88
Ion Source
90
Magnet Pole Piece Assembly
93
Fuses
95
Appendix A Hazardous Area Operation
98
Introduction
98
Installation
99
General Hazardous Area Work
100
Commissioning and Maintenance
100
Routine Checks
101
Hazardous Area - General
101
Area Classification
101
Gas Classification
102
Methods of Protection
102
Purge/Pressurisation
103
Flameproof (Europe) or Explosion Proof (North America
103
Increased Safety
104
Non-Electrical
104
Purge Operation
105
Purge Overview
105
Purge Operation Requirements
106
Parameter Measurement
107
Sample Containment System
108
Definition and Description
108
Parameters
108
Leakage Handling
108
Inspection and Testing
110
Enclosure Leak Testing
111
Purge Operation and Testing
112
All System Types
112
ATEX, Iecex and X-Purge Systems
112
Z-Purge Systems
113
Other Hazardous Area Considerations
113
Temperature
113
Over-Temperature Protection
113
Batteries
114
Dry Gas Vent
114
Rotary Vacuum Pump
115
General
115
Thermal Trip
115
Purge
115
Calibration Panels
116
Air Conditioner
117
Remote / Dual RMS
117
RMS and Instrument in Hazardous Area
117
RMS in Hazardous Area and Instrument in Safe Area
117
Sample Pump (Sentinel PRO Applications
118
Fibre Optic Communications
118
Service Replacement Items
118
Troubleshooting
120
Standards Conformance
122
Introduction to the Prima PRO Hardware
130
Main Components
130
Principle of Operation
131
Vacuum System
133
Ion Source
134
Filaments
136
Mass Analyser
138
Collector
138
Ion Detection
139
MCP Detector Assembly
139
MCP Operation
140
Faraday Detector
142
Introduction of a Gas Sample
142
Mass Spectrometer Parameters
144
Sensitivity
144
Resolution
144
Cracking Patterns
146
Ion Types
146
Molecular Ion
146
Isotope Ions
146
Fragment Ions
147
Multiple-Charged Ions
147
Rearrangement and Recombination Peaks
147
Definitions
148
Appendix C Technical Description: Inlet
150
Rapid Multi-Stream Sampler (RMS
150
Introduction
150
Safety
150
Inlet Specification
151
Inlet Operation
152
General Description
152
Connection to the Mass Spectrometer
153
Seals
153
Inlet Selection
154
Calibration Gas Control
154
Gas Connection
155
Exhaust Connection
156
Heating
157
Main Body Heater
157
Sample Tube Heater
157
Flow Sensor
160
Digital Inputs
160
Vginet
160
Inlet Testing
161
Functional Testing
161
Cross Port Leakage
163
External Leakage
164
Maintenance
164
Routine Maintenance
165
Sample Tube Removal
168
Inlet Ports
170
Cleaning Procedure
170
Inlet Options
171
Remote Mounting
171
Dual RMS
172
Solenoid Inlet
176
Introduction
176
Inlet Operation
177
Valve Operation
179
Capillary Connection
179
Heating
180
Inlet Controller
180
General
180
Valve Drives
181
Manifold Heater
181
Microcapillary Block Heater
181
Flow Sensor
181
Digital Inputs
181
Vginet
182
Testing
182
Capillary Testing
182
Valve Function
183
Cross Seat Leakage
183
External Leakage
184
Maintenance
185
Calibration Inlet
185
Sample Inlet
187
Cleaning Procedure
188
Appendix D Local I/O
190
Introduction
190
Serial I/O
190
Serial Link Type Selection
190
Indicators
191
Fibre Optic Serial Connection
191
Supplying Power to the External I/O Circuit
193
Indicators
193
Analogue I/O
194
Appendix E Air Conditioner
196
Normal Operation
196
Fault Conditions
197
Fault Diagnosis
198
Appendix F Regulatory
200
Fcc
200
Weee
201
China Rohs
202
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