Teledyne Analytical Instruments 9110E Manuals

Manuals and User Guides for Teledyne Analytical Instruments 9110E. We have 1 Teledyne Analytical Instruments 9110E manual available for free PDF download: Instruction Manual

Teledyne Analytical Instruments 9110E Instruction Manual (280 pages)

NITROGEN OXIDES ANALYZER

Brand: Teledyne Analytical Instruments | Category: Measuring Instruments | Size: 4 MB

Safety Messages
2
Table of Contents
3
List of Figures
9
User Notes
14
M9110E Documentation
15
Available Documentation
15
Manual Structure
15
How to Use this Instruction Manual
17
Specifications, Approvals and Warranty
19
M9110E Operating Specifications
19
Table 2-1: Model 9110E Basic Unit Specifications
19
EPA Equivalency Designation
20
CE Mark Compliance
21
Warranty
21
Getting Started
23
Unpacking and Initial Setup
23
Figure 3-1: Location of Shipping Screws and Power Configuration Plug
24
M9110E Layout
25
Figure 3-2: M9110E Layout
25
Figure 3-3: M9110E Rear Panel Layout
26
Figure 3-4: M9110E Front Panel Layout
26
Pneumatic Connections
27
Table 3-1: Inlet / Outlet Connector Nomenclature
27
Span Gas Defined
28
Figure 3-5: Basic Pneumatic Connections for Units Without Valve Options
28
Zero Gas Defined
29
Figure 3-6: Basic Pneumatic Connections for Units with Valve Options
30
Electrical Connections
31
Power Connection
31
Analog Output Connections
31
Figure 3-7: Analog Output Connector
31
Figure 3-8: Status Output Connector
32
Table 3-2: Analog Output Pin-Outs
32
Table 3-3: Status Output Signals
32
Figure 3-9: Control Input Connector
33
Table 3-4: Control Input Signals
33
Ethernet Connection and Configuration
34
Initial Operation
34
Startup
34
Warm-Up
35
Figure 3-10: Front Panel Display During Startup Sequence
35
Table 3-5: Front Panel Display During System Warm-Up
35
Warning Messages
36
Functional Check
37
Table 3-6: Possible Warning Messages at Start-Up
37
Figure 3-11: M9110E Pneumatic Diagram in Standard Configuration
39
Figure 3-12: M9110E Pneumatic Diagram with Options Installed
40
First Calibration
41
Basic Calibration Procedure
41
Interferences for no Measurements
44
Frequently Asked Questions & Glossary
45
Frequently Asked Questions
45
Glossary
46
User Notes
48
Optional Hardware and Software
49
External Pumps (Option 10)
49
Rack Mount Kits (Options 20-23)
49
Carrying Strap Handle (Option 29)
49
Current Loop Analog Outputs (Option 41)
50
Figure 5-1: M9110E with Carrying Strap Handle and Rack Mount Brackets
50
Particulate Filter Kit (Option 42A)
51
Calibration Valve Options
51
Zero/Span Valves (Option 50)
51
Figure 5-2: Current Loop Option Installed on the Motherboard
51
Internal Zero/Span (IZS) (Option 51)
52
Table 5-1: IZS or Z/S Valve States
52
IZS Permeation Tubes (Options 53 & 55)
53
Table 5-2: Available Permeation Source Options
53
Scrubbers and Expendables
54
Charcoal Scrubber (Option 64A)
54
Charcoal Refill Kit (Part# 00596)
54
Zero Air Scrubber (Option 64B)
54
Zero Air Scrubber Maintenance Kit (Option 43)
54
Table 5-3: Contents of Zero Air Scrubber Maintenance Kit
54
M9110E Expendables Kit (Option 42)
55
M9110E Spare Parts Kit (Option 43)
55
Communication Options
55
RS232 Modem Cables (Options 60 and 60A)
55
Multidrop (Option 62)
55
Ethernet (Option 63)
55
Sample Gas Conditioners (Options 86 & 88)
56
Figure 5-3: M9110E Ethernet Card and Rear Panel with Ethernet Installed
56
Table 5-4: Dryer and NH 3 Removal Options
56
Additional Manual (Option 70)
57
Extended Warranty (Options 92 & 93)
57
Operating Instructions
59
Overview of Operating Modes
59
Table 0-1: Analyzer Operating Modes
59
Sample Mode
60
Test Functions
60
Table 0-2: Test Functions Defined
61
Warning Messages
62
Calibration Functions
62
Table 0-3: List of Warning Messages Revision C.4
62
Calibration Mode
63
Setup Mode
63
Password (PASS)
63
Table 0-4: Password Levels
63
Configuration Information (CFG)
65
Clock (CLK)
65
Setup - Range Configuration (RNGE)
66
Figure 0-1: Analog Output Connector Key
66
Physical and Analog Output Ranges
67
Reporting Range Modes
67
Single Range Mode (SNGL)
68
Independent Range Mode (IND)
68
Auto Range Mode (AUTO)
70
Range Units
70
Dilution Ratio
71
Setup - Internal Variables (VARS)
73
Table 0-5: Variable Names (VARS) Revision C.4
73
Setup - Diagnostics (DIAG)
75
Table 0-6: M9110E Diagnostic (DIAG) Functions
75
Signal I/O
76
Analog Output Step Test
77
Analog I/O Configuration
78
Table 0-7: DIAG - Analog I/O Functions
78
Table 0-8: Analog Output Voltage Ranges
78
Analog Output Signal Type and Range Selection
79
Table 0-9: Analog Output Current Loop Range
79
Table 0-10: Analog Output Pin Assignments
79
Analog Output Calibration Mode
80
Manual Analog Output Calibration
82
Figure 0-2: Setup for Calibrating Analog Outputs
82
Table 0-11: Voltage Tolerances for Analog Output Calibration
82
Analog Output Offset Adjustment
83
Current Loop Output Adjustment
84
Figure 0-3: Setup for Calibrating Current Outputs
85
AIN Calibration
86
Test Channel Output
86
Table 0-12: Current Loop Output Calibration with Resistor
86
Table 0-13: Test Parameters Available for Analog Output A4
87
Optic Test
88
Electrical Test
88
Ozone Generator Override
89
Flow Calibration
90
Digital Inputs and Outputs
90
Status Outputs
90
Control Inputs
91
Figure 0-4: Status Output Connector
91
Table 0-14: Status Output Pin Assignments
91
Setup - Communication Ports (COMM)
92
Figure 0-5: Control Inputs with Local and External 5 V Power Supply
92
Table 0-15: Control Input Pin Assignments
92
Analyzer ID
93
COM Port Default Settings
93
COM Port Cable Connections
94
COM2 Configuration
94
DTE and DCE Communication
95
COM Port Communication Modes
95
Table 0-16: COM1 and COM2 DB-9 Pin Assignments
95
Table 0-17: COM Port Communication Modes
96
COM Port Baud Rate
98
COM Port Testing
98
Ethernet Port Configuration
99
Table 0-18: Ethernet Status Indicators
99
Hessen Mode Configuration
102
Setup - Data Acquisition System (DAS)
103
Table 0-19: Front Panel LED Status Indicators for Idas
103
Idas Structure
104
Idas Channels
104
Table 0-20: Idas Data Channel Properties
104
Idas Parameters
105
Table 0-21: Idas Data Parameter Functions
105
Idas Triggering Events
106
Configuring the Idas
106
Default M9110E Idas Configuration
106
Table 0-22: M9110E Default Idas Configuration, Revision C.7
107
Viewing Idas Data and Settings
108
Editing Idas Data Channels
109
Trigger Events
111
Editing Idas Parameters
112
Sample Period and Report Period
114
Number of Records
115
Report Function
116
Compact Report
117
Starting Date
117
Disabling/Enabling Data Channels
117
HOLDOFF Feature
118
Remote Idas Configuration
119
Figure 0-6: APICOM Graphical User Interface for Configuring the Idas
119
Remote Operation of the Analyzer
120
Basic Operation
120
Terminal Operating Modes
120
Figure 0-7: Idas Configuration through a Terminal Emulation Program
120
Help Commands in Terminal Mode
121
Command Syntax
121
Table 0-23: Terminal Mode Software Commands
121
Data Types
122
Status Reporting
122
Table 0-24: Command Types
122
Remote Access by Modem
123
COM Port Password Security
124
APICOM Remote Control Program
125
Figure 0-8: APICOM Remote Control Program Interface
125
Additional Communications Documentation
126
Table 0-25: Serial Interface Documents
126
Calibration Procedures
127
Calibration Preparations
127
Required Equipment, Supplies, and Expendables
127
Zero Air
127
Span Gas Standards
127
Permeation Tubes
128
Calibration Gas Traceability
128
Data Recording Devices
128
Conversion Efficiency
128
Figure 7-1: Gas Supply Setup for Determination of no
129
Manual Calibration
130
Connect Zero Air and Span Gases to the Analyzer
131
Set Expected no and no
131
Span Gas Concentrations
131
Figure 7-2: Setup for Manual Calibration Without Z/S Valve or IZS Option
131
Perform Zero/Span Calibration
132
Calibration Checks
133
Calibration with Zero/Span Valves
133
Calibration with IZS Option
134
Figure 7-3: Pneumatic Connections for Manual Calibration Checks with IZS
135
Calibration Checks with IZS or Zero/Span Valves
137
Figure 7-4: Setup for Manual Calibration Check with Z/S Valve or IZS Option
137
Calibration with Independent or AUTO Ranges
138
Calibration in AUTO Range Mode
138
Independent Range Mode
139
Calibration with Remote Contact Closures
139
Automatic Calibration (Autocal)
140
Table 7-2: Autocal Modes
140
Table 7-3: Autocal Attribute Setup Parameters
140
Table 7-4: Example Auto-Cal Sequence
141
Calibration Quality Analysis
142
Table 7-5: Calibration Data Quality Evaluation
143
User Notes
144
Epa Protocol Calibration
145
Calibration of Equipment
145
Table 8-1: Activity Matrix for EPA Calibration Equipment and Supplies
146
Table 8-2: Activity Matrix for Calibration Procedure
146
Gas Phase Titration (GPT)
147
GPT Principle of Operation
147
GPT Calibrator Check Procedure
147
Example GPT Calculation
148
Multipoint Calibration Procedure
150
Zero Calibration
151
Span Calibration
151
Figure 8-1: GPT Calibration System
151
GPT no Calibration
152
Calibration Frequency
153
Other Quality Assurance Procedures
153
Summary of Quality Assurance Checks
154
Table 8-3: Definition of Level 1 and Level 2 Zero and Span Checks
154
Short Calibration Checks
155
Zero/Span Check Procedures
155
Table 8-4: Activity Matrix for Data Quality
155
Precision Check
156
Precision Check Procedure
156
Certification of Working Standards
156
Certification Procedures of Working Standards
157
Other Methods of Establishing Traceability
157
References
157
Instrument Maintenance
159
Maintenance Schedule
159
Table 9-1: M9110E Preventive Maintenance Schedule
159
Predictive Diagnostics
161
Maintenance Procedures
161
Table 9-2: Predictive Uses for Test Functions
161
Changing the Sample Particulate Filter
162
Figure 9-1: Sample Particulate Filter Assembly
162
Changing the O
163
Figure 9-2: Particle Filter on O
163
Changing the Ozone Filter Chemical
164
Figure 9-3: 04419 Ozone Filter Unit
164
Rebuilding the External Sample Pump
165
Changing the Pump and IZS Dust Filters
166
Changing the IZS Permeation Tube
166
Changing the External Zero Air Scrubber
167
Changing the no Converter
168
Figure 9-4: Zero Air Scrubber Assembly
168
Cleaning the Reaction Cell
169
Figure 9-5: no 2 Converter Assembly
169
Figure 9-6: Reaction Cell Assembly
170
Cleaning or Changing Critical Flow Orifices
171
Checking for Light Leaks
172
Figure 9-7: Critical Flow Orifice Assembly
172
Theory of Operation
173
Measurement Principle
173
Chemiluminescence
173
Figure 10-1: M9110E Sensitivity Spectrum
174
Nox
174
NO X and no 2 Determination
174
Chemiluminescence Detection
175
The Photo Multiplier Tube
175
Figure 10-2: no 2 Conversion Principle
175
Optical Filter
176
Auto Zero
176
Figure 10-3: Reaction Cell with PMT Tube
176
Measurement Interferences
177
Direct Interference
177
Third Body Quenching
177
Figure 10-4: Reaction Cell During the Autozero Cycle
177
Table 10-1: List of Interferents
178
Light Leaks
179
Pneumatic Operation
179
Pump and Exhaust Manifold
179
Sample Gas Flow
180
Figure 10-5: External Pump Pack
180
Sample Particulate Filter
181
Table 10-2: M9110E Valve Cycle Phases
181
Ozone Gas Air Flow
182
Generator
182
Figure 10-6: Ozone Generator Principle
182
Perma Pure Dryer
183
Figure 10-7: Semi-Permeable Membrane Drying Process
183
Ozone Supply Air Filter
184
Figure 10-8: M9110E Perma Pure Dryer
184
Ozone Scrubber
185
Flow Rate Control - Critical Flow Orifices
185
Figure 10-9: Flow Control Assembly & Critical Flow Orifice
186
Table 10-3: M9110E Gas Flow Rates
186
Pneumatic Sensors
187
Vacuum Manifold
187
Sample Pressure Sensor
188
Vacuum Pressure Sensor
188
O 3 Supply Air Flow Sensor
188
Figure 10-10: Vacuum Manifold, Standard Configuration
188
Dilution Manifold
189
Electronic Operation
189
Figure 10-11: Dilution Manifold
189
Cpu
190
Figure 10-12: M9110E Electronic Block Diagram
190
Disk on Chip
191
Figure 10-13: M9110E CPU Board Annotated
191
Flash Chip
192
Sensor Module, Reaction Cell & PMT
192
Reaction Cell Heating Circuit
192
Photo Multiplier Tube (PMT)
192
PMT Cooling System
193
TEC Control Board
193
Figure 10-14: Schematic of Basic PMT Design and Functionality
193
PMT Preamplifier
194
Pneumatic Sensor Board
195
Figure 10-15: PMT Preamp Block Diagram
195
Relay Board
196
Heater Control
196
Valve Control
196
Status Leds
196
Motherboard
197
A to D Conversion
197
Sensor Inputs
197
Thermistor Interface
198
Analog Outputs
198
External Digital I/O
199
I 2 C Data Bus
199
Power-Up Circuit
199
Power Supply/ Circuit Breaker
199
Communications Interface
200
Figure 10-16: Power Distribution Block Diagram
200
Front Panel
201
Display
201
Figure 10-17: M9110E Electronic Interface Block Diagram
201
Keypad
202
Front Panel States Led's
202
Display / Keyboard Interface Electronics
202
Table 10-4: Front Panel Status Led's
202
Software Operation
203
Adaptive Filter
203
Figure 10-18: Keyboard and Display Interface Block Diagram
203
Calibration - Slope and Offset
204
Figure 10-19: Schematic of Basic Software Operation
204
Temperature/Pressure Compensation (TPC)
205
Converter Efficiency Compensation
206
Internal Data Acquisition System (Idas)
206
Troubleshooting & Repair
207
General Troubleshooting
207
Warning Messages
208
Fault Diagnosis with Test Functions
208
Figure 11-1: Viewing and Clearing Warning Messages
208
Using the Diagnostic Signal I/O Function
209
Table 11-1: Test Functions - Possible Causes for Out-Of-Range Values
209
Status Led's
210
Motherboard Status Indicator (Watchdog)
210
Figure 11-2: Switching Signal I/O Functions
210
CPU Status Indicator
211
Relay Board and Status Leds
211
Figure 11-3: Motherboard Watchdog Status Indicator
211
Figure 11-4: Relay Board PCA
212
Gas Flow Problems
213
Table 11-2: Relay Board Status Leds
213
Zero or Low Flow Problems
214
Sample Flow Is Zero or Low
214
Ozone Flow Is Zero or Low
215
High Flow
216
Sample Flow Is Zero or Low but Analyzer Reports Correct Flow
216
Calibration Problems
216
Negative Concentrations
216
No Response
217
Unstable Zero and Span
218
Inability to Span - no SPAN Key
218
Inability to Zero - no ZERO Key
219
Non-Linear Response
219
Discrepancy between Analog Output and Display
220
Discrepancy between no and no Slopes
220
Discrepancy between no and NOX
220
Other Performance Problems
220
Excessive Noise
220
Slow Response
221
Auto-Zero Warnings
221
Subsystem Checkout
222
Simple Vacuum Leak and Pump Check
222
Detailed Pressure Leak Check
222
Performing a Sample Flow Check
223
AC Power Configuration
224
DC Power Supply
224
Table 11-3: DC Power Test Point and Wiring Color Code
224
I 2 C Bus
225
Keyboard / Display Interface
225
Table 11-4: DC Power Supply Acceptable Levels
225
Relay Board
226
Motherboard
226
A/D Functions
226
Analog Output Voltages
226
Table 11-5: Relay Board Control Devices
226
Status Outputs
227
Control Inputs
227
Table 11-6: Analog Output Test Function - Nominal Values
227
Table 11-7: Status Outputs Check
227
Cpu
228
Communication
228
General RS-232 Troubleshooting
228
Modem or Terminal Operation
229
PMT Sensor
229
PMT Preamplifier Board
229
High Voltage Power Supply
230
Pneumatic Sensor Assembly
230
Reaction Cell Pressure
231
Sample Pressure
231
Figure 11-5: Pressure / Flow Sensor Assembly
231
Ozone Flow
232
Converter
232
O 3 Generator
233
IZS Option
233
Box Temperature
234
PMT Temperature
234
Repair Procedures
234
Disk-On-Chip Replacement
235
Flash Chip Replacement or Upgrade
235
O 3 Generator Replacement
236
Sample and Ozone Dryer Replacement
236
PMT Sensor Hardware Calibration
237
Figure 11-6: Pre-Amplifier Board Layout
238
Replacing the PMT, HVPS or TEC
239
Figure 11-7: M9110E Sensor Assembly
239
Technical Assistance
240
User Notes
242
Appendix A: Software Documentation
243
Figure A-1: Basic Sample Display Menu
244
APPENDIX A-1: M9110E Software Menu Trees and Index, Revision C.8
244
Appendix
244
Figure A-2: Sample Display Menu - Units with Z/S Valve or IZS Option Installed
245
Figure A-3: Primary Setup Menu (Except Idas)
246
Figure A-4: Secondary Setup Menu (COMM & VARS)
247
Figure A-5: Secondary Setup Menu (DIAG)
248
Figure A-6: Internal Data Acquisition (Idas) Menu
249
Appendix
250
Setup Variables for Serial I/O, Revision C.8
250
Appendix
259
Warnings and Test Measurements, Revision C.8
259
Appendix
261
M9110E Signal I/O Definitions, Revision C.8
261
APPENDIX A-6: Terminal Command Designators, Revision C.8
266
User Notes
268
Appendix B: Spare Parts and Expendables
269
Intentionally Blank
274
Appendix C: Warranty/Repair Questionnaire Model 9110E
277
Appendix D: Diagrams and Schematics
279

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Teledyne Analytical Instruments 9110E Instruction Manual (280 pages)

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