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Stanford Research Systems RGA300 Analyzer Manuals
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Stanford Research Systems RGA300 Analyzer manual available for free PDF download: Operating Manual And Programming Reference
Stanford Research Systems RGA300 Operating Manual And Programming Reference (362 pages)
Residual Gas Analyzer
Brand:
Stanford Research Systems
| Category:
Measuring Instruments
| Size: 3 MB
Table of Contents
Table of Contents
5
Specifications
14
Command List
16
1-1 Chapter 1 Getting Started
19
Chapter 1 Getting Started
19
Unpacking
20
Before You Open the Box
20
Checklist
20
Standard Equipment / Supplies
20
Accessories
20
Optional Equipment
20
Related Equipment
21
Installation
22
Introduction
22
Probe Installation
22
Hardware Requirements
23
Procedure
24
Electronics Control Unit Installation
26
Hardware Requirements
26
Procedure
28
RGA Windows Installation
29
Minimum System Requirements (Single Head Operation)
29
Procedure
29
Turning on the RGA
30
Running the SRS RGA System
31
Chapter 2 Rga General Operation
33
What Is an RGA
34
The SRS RGA
35
Basic Operating Modes of the SRS RGA
37
The SRS RGA as a Mass Spectrometer
37
The SRS RGA as a Single Gas Monitor
38
The SRS RGA as a Total Pressure Gauge
38
Residual Gas Analysis Basics
40
How Mass Spectra Are Interpreted
40
Partial Pressure Measurement
41
Partial Pressure Sensitivity Factors
43
Chapter 3 Rga Quadrupole Probe
47
Introduction
48
Ionizer
49
Description
49
Principle of Operation
49
Parameter Settings
50
Quadrupole Mass Filter
53
Description
53
Principle of Operation
54
Mass Range, Resolution and Throughput
55
Zero Blast Suppression
57
Ion Detector
58
Description
58
Faraday Cup Operation
59
Electron Multiplier Operation
59
Hardware Modifications
63
Repeller and Anode Grid Modifications
63
Repeller Removal
64
Operation Without a Filament
64
W Filament Replacement
64
RGA Cover Nipple Replacement
65
Chapter 4 Rga Electronics Control Unit
67
Introduction
68
Front Panel
69
Rear Panel
70
24VDC@2.5A Connector
70
Rs232/Dce/28.8K Connector
71
Locking Knobs
71
Power Entry Module (Option 02)
71
Led’'S
71
LED Functionality
72
STATUS (Green) Led's
72
ERROR (Red) Led's
73
ERROR (Red) Led’'S
73
Electrometer
74
Detection Limit Vs. Scan Rate
74
Adjusting the Zero of the Ion Detector
75
Mass Filter Power Supply
76
Maintenance and Service
77
5-1 Chapter 5 Rga Windows Software
79
Chapter 5 RGA Windows Software
79
Overview
81
Program Structure
81
RGA Files
81
RGA Files (.Rga)
81
RGA Scan Log Files (.Ana .Hst .Tbl)
81
RGA ASCII Data Files (.Asc)
82
RGA Graph Metafiles (.Wmf)
82
System Requirements
82
RGA ASCII Data Files (.Txt)
82
Getting Started
83
Starting the RGA Software
83
Connecting to a Head
83
Shutting down the RGA System
83
Features and Operation
85
The RGA Window
85
Multiple Head Operation
85
Display Modes
85
Analog (Mode Menu)
85
Histogram (Mode Menu)
86
P Vs T (Mode Menu)
87
Leak Test (Mode Menu)
88
Annunciator (Mode Menu)
88
Library (Mode Menu)
89
Data Acquisition
89
Scan Data Logging
89
Graph Management
90
Head Management
90
Sensitivity Factors
91
Spectrum Analysis
91
Background Data
91
RGA Head and Scan Parameters
92
Changing Scanning Parameters
92
Changing Head Parameters
92
Changing Scan Trigger Rates
93
Display Modes
94
Changing Display Modes
94
Running in Split Display Mode
94
Manual Scaling of Graphs
94
Using Scan Data as Background
95
General Utilities
96
Using the Data Cursors
96
Cursor Command
96
Cursor Properties Command
96
Scheduled Saving of Data
96
Logging Scans
96
Viewing Scans
96
Browsing through the Gas Library
97
Analyzing the Mass Spectrum
98
Spectrum Analysis Description
98
Analysis Procedure
98
Averaging Scan Spectrum
98
Pressure Reduction
99
Y-Axis Unit Change
99
Head Calibration and Security
100
Tuning the RGA Sensitivity
100
Adjusting the CEM Gain
100
Peak Tuning the RGA Head
101
Securing the RGA Head
102
RGA On-Line Help
103
Context Sensitive Help
103
Help Search
103
Help Index
103
Commonly Asked Questions
103
Sample Scans
103
Chapter 6 Programming the Rga Head
105
Introduction
108
The RGA COM Utility
109
LED Indicators
110
RS232 Interface
110
Command Syntax
111
Examples of Command Formats
111
Programming Tips
112
Communication Errors
113
Command Errors
113
Parameter Errors
113
Jumper Protection Violation
113
Troubleshooting the RGA Communications
115
Programming the RGA Head
116
Initializing the RGA Head
116
Programming the Ionizer
117
Programming the Detector
118
Setting up Analog Scans
120
Setting up Histogram Scans
122
Single Mass Measurements
124
Total Pressure Measurements
126
Storing Information in the RGA Head
127
Programming the Quadrupole Mass Filter
128
Error Checking the RGA
129
RGA Command Set
133
Initialization Commands
134
In0, In1, In2
134
Ionizer Control Commands
136
Dgparam, Param: 0 - 20
136
Eeparam, Param: 25 - 105
137
Flparam, Param: 0.00 - 3.50, *, ?
138
Ieparam, Param: 0,1
140
Vfparam, Param: 0 - 150
140
Detection Control Commands
142
Hvparam, Param: 0 - 2490
144
Nfparam, Param: 0 - 7
146
Scan and Measurement Commands
148
Hsparam, Param:0 - 255
149
Mfparam, Param: 1 - M_MAX
151
Miparam, Param: 1 - M_MAX
151
Mrparam, Param:0 - M_MAX
152
Saparam, Param: 10 - 25
154
Sc[Param], Param: 0 - 255
155
Tp?, Tp0, Tp1
156
Parameter Storage Commands
159
Mgparam, Param: 0.0000 - 2000.0000
159
Mvparam, Param: 0 - 2490
159
Spparam, Param:0.0000 - 10.0000
160
Stparam, Param:0.0000 - 100.0000
160
Mass Filter Control Commands
162
Mlparam, Param: 0.0000 - M_MAX
162
Error Reporting Commands
163
Tuning Commands
167
Diparam, Param: 0 - 255
167
Dsparam, Param: -0.8500 - +0.8500
168
Riparam, Param: -86.0000 - +86.0000, *, ?, None
169
Rsparam, Param: 600.0000 - 1600.0000, *, ?, None
171
Error Byte Definitions
173
Chapter 7 Rga Tuning
177
Introduction
178
Tuning Options
179
Peak Tuning Procedure
180
Introduction
180
General Procedure
181
Peak Position Tuning Algorithms
182
Peak Width Tuning Algorithms
184
Temperature Effects on the Mass Scale Calibration
185
Sensitivity Tuning Procedure
187
Electron Multiplier Tuning Procedure
190
Chapter 8 Rga Maintenance
191
Warnings
193
Probe Bakeout
195
Procedure
196
Ionizer Degas
197
Ionizer Replacement
198
Equipment
198
Procedure
198
Filament Replacement
201
Handling and Care of the Filament
201
Equipment
201
Procedure
201
CDEM Handling and Care
204
Handling and Mounting
204
Operating Pressure
204
Operating Temperature
204
Bakeout Temperature
204
Operating Voltage
204
Initial Pump-Down
204
Contamination
204
Storage
205
CDEM Pre-Conditioning
206
CDEM Refreshment
207
Materials
207
Procedure
207
CDEM Replacement
208
Equipment
208
Procedure
208
Quadrupole Filter Cleaning
211
Equipment
211
Procedure
212
SRS Probe Refurbishing Service
215
Chapter 9 Rga Troubleshooting
217
Warnings
218
Internal Error Detection in the SRS RGA
219
Basic Troubleshooting
221
Built-In Hardware Checks
226
24V DC Power Supply
226
Electrometer
226
Quadrupole Mass Filter RF P/S
227
Filament’'S Background Protection Mode
228
Chapter 10 Rga Circuit Description
229
Overview of the RGA
231
Circuit Description
232
General Description
232
Circuit Boards
233
Description of Schematics
234
Microprocessor
234
Digital I/O Ports
234
The LED Port
235
The MPX Port
235
The MISC Port
235
Clocks
235
RS232 Interface
236
Schematic Name: QMSE_T2
236
I/V Calibration
236
A/D Conversion
236
Power-Up Conditioning
237
DC Control Voltages
237
RF Amplitude Detection
237
RF Amplitude Control
238
Foldback Current Limiting
238
Schematic Name: QMSE_B1
239
Mass Filter RF Supply
239
DC Potentials
240
Schematic Name: QMSE_B2
240
Filament Heater Supply
240
Bias Regulators
241
Schematic Name: QMSE_B3
242
Power Supplies
242
Schematic Name: QMSE_V1
242
Signal Conditioning
242
Schematic Name: QMSE_V2
243
Electron Multiplier High Voltage Power Supply
243
Chapter 11 RGA Probe Assembly
245
Feedthru Flange Connectors Schematic
245
O100MAX Maximum Insertion Nipple Drawing
245
Leak Testing
258
RGA Probe Assembly Schematic
245
Appendix C Do I Need a Ppm100 Partial Pressure Monitor for My Srs Rga?
269
Introduction
270
What Is the PPM100 Controller
271
How Does the PPM100 Interface to the SRS RGA
272
Leak Test Analysis
273
Partial Pressure Monitor and Control
273
What Does the PPM100 Controller Do
273
Mass Spec Display
274
Analog I/O Ports
275
RGA Control
275
Capacitance Manometer Readings (CM1-4)
276
Data Logging (Charts and Tables)
276
Computer Interfaces (RS-232, GPIB and USB)
278
Vacuum Process Control
278
Internet Access
279
Who Should Consider the PPM100
281
Do I Still Need RGA Windows
284
PPM100 Specifications
285
Vacuum References
320
Residual Gas Analysis
321
Vacuum Technology Books
321
High Pressure Sampling / D
328
Quantitative Measurements with
328
Vacuum System Contamination
334
Vacuum Pumps
337
Pirani/Thermocouple Gauges
345
Rotor Gauge
345
Esorption
347
Publications
349
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