Pickering Laboratories Pinnacle PCX Manuals

Manuals and User Guides for Pickering Laboratories Pinnacle PCX. We have 1 Pickering Laboratories Pinnacle PCX manual available for free PDF download: Operator's Manual

Pickering Laboratories Pinnacle PCX Operator's Manual

Pickering Laboratories Pinnacle PCX Operator's Manual (179 pages)

post-column derivatization instrument

Brand: Pickering Laboratories | Category: Analytical Instruments | Size: 2 MB

Table of Contents

Table of Contents
3
Read this
9
What Is Post-Column Derivatization?
17
Design of a HPLC System
18
Designing a Post-Column System
20
Design of the Pinnacle PCX
22
Background 6
23
Introduction
24
Check Valve
25
Reagent Pump
26
Reagent Valves
27
Fluidics Panel
29
Quick Change Reactor
30
Pump Compartment
31
Display Module
32
Electronics Compartment
33
Safety Features in the Pinnacle PCX
35
Standard Configurations of Pinnacle PCX
36
Site Requirements
38
Instrument Unpacking and Preparation
40
Gas Connections to Back Panel of Pinnacle PCX
41
Computer Connections
42
Pump and Autosampler Connections
44
Eluant Priming
46
Detector Connections
47
Reservoir Connections
48
Reagent Pump Preparation
49
Running a Chromatogram
50
Shutdown
51
Software Overview
53
Status Window
54
Menu Options/Functions
56
Configuring Your Pinnacle PCX
58
Log Files
59
Creating and Editing Sequences
62
Tutorials
63
Running Post-Column Analysis Using Pinnacle PCX
66
STOP/RESET Pinnacle PCX
69
Maintenance Suggestions
71
Operating Suggestions
72
Proper Shutdown Procedures
73
Basic Maintenance Procedures
76
Reagent Filter(S) Replacement
77
Ambient Reactor Replacement
78
Valve Maintenance
79
Pump Seal Replacement
82
Fuse Replacement
86
- Reagent Preparation 6
  90
- Reagent Preparation 6
  93
- Post-Column Conditions 6
  94
- Procedure 6
  95
- Sample Chromatograms and Gradient Programs 6
  96
- Precautions 6
  108
- Analytical Procedure 6
  113
- Precautions 6
  125
- Analytical and Post-Column Conditions 6
  127
- Sample Chromatograms 6
  132
- Precautions 6
  133
Contact Pickering Laboratories for Support
137
Instrument Parameter Log
138
Common System Problems
139
Common Chromatography Problems
140
Amino Acids
141
Carbamates
142
Glyphosate
143
Software Troubleshooting
144
Procedures
147
Installation/Operational Qualitication of the Pinnacle PCX
150
Installation/Operational Qualitication of the Pinnacle PCX Data Sheet
155
Performance Qualifications of the Pinnacle PCX Data Sheet
156
Sample Instrument Parameter Log
163
- Flow Diagram – Simplex
  164
- Flow Diagram – Duplex
  165
Parts List for Pinnacle PCX
166
Recommended Consumables and Spare Parts
169
Limited Warranty
172
References
173

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