Pickering Laboratories PCX 5200 Manuals

Manuals and User Guides for Pickering Laboratories PCX 5200. We have 1 Pickering Laboratories PCX 5200 manual available for free PDF download: Operation Manual

Pickering Laboratories PCX 5200 Operation Manual

Pickering Laboratories PCX 5200 Operation Manual (76 pages)

Brand: Pickering Laboratories | Category: Laboratory Equipment | Size: 0 MB

Table of Contents

Table of Contents
3
Please Read
6
Symbols
6
Chapter 1 • Introduction

10
- Why Post-Coiumn Derivatization
  10
- How Does It Work
  10
- What Are the Requirements
  10
- Pickering PCX5200
  11
  - Reagent Delivery
    11
  - Column Protection
    11
  - Design of an HPLC
    13
  - A Simpler View of an HPLC
    14
  - Designing a Post-Column System
    14
Chapter 2 • PCX5200 System Components

16
- Getting to Know Your PCX5200
  16
  - Front Panels
    16
  - Internal
    18
  - Rear Panel
    19
  - Column Oven
    21
  - Reagent Reservoirs
    23
  - External Reagent Pressurization System
    24
  - Keypad and Liquid Crystal Display User Interface
    25
- Keypad Examples
  28
  - Loading a Preset
    28
  - Saving a Preset
    30
- Flow Diagrams
  33
  - PRESET Key
    33
  - PROG Key
    33
- Specifications
  35
  - Wetted Materials, PCX5200
    35
  - Pcx5200 Peek
    35
  - Ratings
    35
- RS232 Serial Port
  36
  - Downloading Firmware
    36
  - Radio Frequency
    36
Chapter 3 • Installation

38
- Unpacking
  38
- Site Requirements
  38
  - HPLC System Requirements
    38
  - Space Requirements
    39
  - Electrical Requirement
    39
  - Inert Gas
    39
  - Note about Fittings
    40
  - Inert Gas
    40
  - Reagent Reservoir Connections
    40
  - Pressure-Interlock Connections
    41
  - Injector Connections
    43
  - Detector Connections
    43
  - Guard & Analytical Column Installation
    44
  - Reagent Pump
    46
  - Priming the Reagent Pump
    46
  - System Testing & Verification
    46
- Shutdown
  47
  - Short-Term
    47
  - Medium-Term
    48
  - Long-Term
    49
Chapter 4 • Routine Maintenance & Troubleshooting

50
- Initial System Testing
  50
  - Test Chromatogram
    50
  - Paramater Log
    50
- Precautions & Problem Prevention
  51
  - Mobile Phase
    51
  - Back-Flow Prevention
    51
  - Reactor Precautions
    51
  - Electrical Precaution
    51
- Routine Maintenance
  52
  - Reagent Pump
    52
  - Pump Seal Replacement
    52
  - Check-Valves
    55
  - Cleaning Check-Valves
    55
  - Removing Check-Valves
    56
  - Installing New Check-Valves
    56
  - Rebuilding Check-Valves
    57
  - Pre-Column Filter
    58
  - Reagent Filter
    59
    
    Heated Reactor
    60
    
    Fuse
    61
  - Troubleshooting Guide
    61
    
    Advice
    61
    
    When Priming the Reagent Pump Is Difficult
    62
  - Interpretation of Pressures
    63
    
    Two-Reagent PCX5200
    63
    
    One-Reagent PCX5200
    63
  - Cleaning the Post-Column System
    64
    
    Fittings
    64
    
    External
    64
    
    Internal
    64
    
    Internal Spill
    64
  - PCX5200 Parameter Log
    66
  - Analytical Conditions
    67
  - Post-Column Band-Spreading Test
    68
Appendix A

66
Appendix B Spare Parts

70
References

71
Limited Warranty

73
Index

75

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