PICARRO PI5310 Manuals

Manuals and User Guides for PICARRO PI5310. We have 2 PICARRO PI5310 manuals available for free PDF download: User Manual

PICARRO PI5310 User Manual (174 pages)

For N2O, CO, H2O

Brand: PICARRO | Category: Measuring Instruments | Size: 14 MB

Revision History
2
Table of Contents
4
List of Figures
9
List of Tables
12
Introduction
13
System Overview
13
Analyzer
13
Figure 1 - PI5310 Front/Back Panels
13
Front Panel Operating Status
14
A2000 Vacuum Pump
14
Analyzer Specifications
14
Figure 2 - LED Status Indicator
14
Figure 3 - A2000 Vacuum Pump - Side Views
14
Table 1 - PI5310 Specifications
14
Acronyms
16
Table 2 - Acronyms, Formulas, Units, and Symbols
16
Text Conventions
19
Safety
20
Warning Symbols
20
General Safety
21
CDRH Certification
21
CE Certification
21
Laser Safety
23
Figure 4 - Laser Safety Label - Affixed to Outside Cover of Analyzer
23
Figure 5 - Laser Safety Label - Affixed to Inside of Analyzer
24
Unpacking
25
Inspect the Shipping Containers
25
Unpack Components
25
Figure 6 - Shipping Container with Clamps Installed/Removed
25
Contents
26
Table 3 - Shipping Contents
26
Hardware Setup
29
Required Components and Tools
29
Installation Safety
29
Analyzer Preparation
32
Ventilation Considerations
32
Positioning
32
Set A2000 Pump Input Voltage
33
A2000 Pump and Gas Inlet Connections
33
Pump Connections
33
Figure 7 - Vacuum Pump Voltage Selection
33
Sample Gas Inlet Connections
34
Figure 8 - Analyzer Setup with A2000 Pump
34
Sample Gas Inlet Connection (SST Tubing)
35
Sample Gas Inlet Connection (PFA Tubing)
35
Figure 9 - Orientation of Inlet Nut and Ferrules (SST Tubing)
35
Figure 10 - Orientation of Inlet Nut and Ferrules (PFA Tubing)
35
Rack Mount Instructions
36
Rack Mount (Slide Rails)
36
Figure 11 - Inner Rail Slide Removal
37
Figure 12 - Attaching Inner Slide Rails to Analyzer
37
Figure 13 - Front Panel Restraint Installed
38
Figure 14 - Outer Rail Mounted to Rack
38
Rack Mount (Mount Kit)
39
Electrical Connections
40
Figure 15 - Front Panel Restraint Installed
40
Figure 16 - Rear Panel Diagram
41
Chiller Laser Cooling
42
Chiller Setup
42
Figure 17 - Reservoir Connections at Time of Shipment
43
Figure 18 - Reservoir Inspection
44
Figure 19 - Reservoir Coolant Level
44
Figure 20 - Reservoir Connected and Ready to Run
45
Figure 21 - Confirmation of Coolant Flow
45
Chiller Maintenance
46
Analyzer Basic Operation
48
Startup
48
Shutdown
49
Figure 22 - CRDS Data Viewer Screen
49
Figure 23 - Stop Data Acquisition Confirmation
50
Analyzer Restart after Electrical Power Outage
51
Picarro Launch Pad
51
Home Menu
51
Figure 24 - Picarro Launch Pad/Home Menu
52
Tools Menu
53
Figure 25 - Picarro Launch Pad/Tools Menu
53
Settings Menu (Setup Tools)
54
Administration Menu
54
Figure 26 - Transfer Files Dialog
54
Language Selector
55
Figure 27 - Picarro Launch Pad/Administration Menu
55
Zoom Level
56
Figure 28 - Language Selector
56
Figure 29 - Language Change Confirmation
56
Figure 30 - Picarro Launch Pad - Zoom Level
57
GUI Functions
58
GUI Overview
58
Figure 31 - CRDS Data Viewer GUI
58
Users, View, Tools, and Help Menus
59
User Menu
59
View Menu
59
Figure 32 - CRDS Toolbar Options
59
Tools Menu
60
Help Menu
60
Alarms Panel
60
Figure 33 - Configure Graph Window
60
Figure 34 - Alarm Panel
61
Digital Readouts
62
Figure 35 - Alarm Set Dialog
62
Instrument Status
63
Quit Button
63
Figure 36 - Digital Readouts Panel
63
Figure 37 - Instrument Status Panel
63
Figure 38 - CRDS Quit Button
63
Restart User Log(S) Button
64
Data Log Filename and Path
64
Data Window
64
Figure 39 - Restart User Logs Button
64
Figure 40 - Data Log Filename and Path Panel
64
Data Source and Data Key Pull down Menus
65
Figure 41 - Data Window Panel
65
Figure 42 - Data Source and Data Key Pull down Menus
65
6.10 Precision Pulldown Menu
66
6.11 Measurement Status Log
66
6.11.1 Common Status Log Messages
66
Figure 43 - Precision Pull-Down Pane
66
Figure 44 - Measurement Status Log
66
6.12 Reset Buffers Button
67
6.13 Graph Zooming and Panning
67
6.13.1 Zooming In/Out
67
Figure 45 - Data Graph Zoom Function
67
6.13.2 Lock/Unlock Time Axis
68
6.13.3 Panning
68
Figure 46 - Auto-Scale Buttons
68
User Management
69
Overview
69
Table 4 - User Accounts and Functions
69
Managing User Accounts
70
Figure 47 - User Management Window
70
Changing a User Password
71
Figure 48 - Change Password
71
Changing a User's Role
72
Figure 49 - Change Roles
72
Disabling a User Account
73
Adding a User
73
Figure 50 - Disable Users
73
Setting User Policies
74
Figure 51 - Add User
74
User Policy Descriptions
75
Figure 52 - User Policies Tab
75
Table 5 - User Policies
75
Viewing User History
76
Figure 53 - User History Tab
76
Viewing My Profile
77
Figure 54 - My Profile Tab
77
File Management
78
Data Archive
78
Data File Name
78
File Archiving
79
Figure 55 - Example Data File Name
79
Modbus Communication
81
Configuring Modbus Communication
81
Figure 56 - Settings/Modbus Configuration
81
Modbus Data Registers Overview and Setup
82
Figure 57 - Modbus Settings Window
82
Table 6 - MODBUS Register Types
82
Modbus TCP Setup Notes
83
Modbus RTU Setup Notes
83
Modbus Register Maps
83
Input Register Map
83
Table 7 - Input Registers
83
Discrete Input Register Map
86
Table 8 - Discrete Input Registers
86
Holding Register Map
88
Table 9 - Holding Registers
88
Coil Register Map
89
Table 10 - Coil Register Map
89
Troubleshooting
92
10.1 Power LED on Analyzer Does Not Illuminate
92
Sample Pressure Not Controlled to Appropriate Value for Concentration Measurements
92
Maintenance
93
11.1 Service Plans
93
11.2 Particulate Filter Replacement
93
11.2.1 Symptoms of a Clogged Filter
94
11.2.2 Solutions for Water Incursion
94
11.2.3 Required Parts and Tools
94
11.2.4 Pressure Inlet Port Particulate Filter Replacement
94
Figure 58 - Pressure Inlet Port
95
Figure 59 - Pressure Inlet Filter - Removed
95
Figure 60 - Removing Filter from Pressure Inlet Bulkhead
96
Figure 61 - Filter Removed from Pressure Inlet Bulkhead
96
11.2.5 CPU Fan
97
11.2.6 A2000 Pump Rebuild Kit
97
Figure 62 - Tightening the Filter Fittings
97
11.3 Cleaning and Decontamination
98
Transportation and Storage
99
12.1 Shutdown and Preparation
99
Figure 63 - Stop Data Acquisition/Shutdown
99
12.2 Packing
100
Figure 64 - Reduce Moisture Content/Shutdown
100
A Setup Tools and Communication
101
Analyzer Settings and Tools
101
Figure 65 - Analyzer Setup Tools
101
Serial Port
102
Figure 66 - Serial Port Settings
102
Port Manager
103
Command Interface - Specifying Digital Data Output
103
Figure 67 - Serial/Socket Port Manager Settings
103
Command Interface - Specifying Digital Data Output
104
Figure 68 - Command Interface Settings
104
Data Logger
105
Figure 69 - Data Streaming Settings
105
Figure 70 - Data Logger Setup Settings
106
Serial Communication
107
Remote Data Access
107
Ntp
108
Email
108
B Alarm Status
109
Table 11 - Alarm Status Bit Assignment
109
Table 12 - Alarm Status Definitions
109
C Data Log Columns
110
Table 13 - PI5310 Data Log Columns
110
D Enabling/Disabling Data Output
116
E Analog Current Signal Output
117
Connecting the 4-20Ma Signal Output
117
Figure 71 - 4-20 Ma Output with Terminal Connector
117
Table 14 - Signal Output Settings
117
Figure 72 - Removing the Terminal Connector
118
Figure 73 - Terminal Connector Retaining Screws
118
Data File Viewer
119
Quick Start Guide
119
Figure 74 - Batch Convert DAT to H5 - Navigation
119
Figure 75 - Selecting Variables for Concatenation
120
Figure 76 - Concatenated Output .H5 Filename
120
Data File Viewer Overview
121
Figure 77 - Time Series Selection Options
121
File Menu
122
Figure 78 - Picarro Data File Viewer - File and New Menus
122
Figure 79 - Select Variable Form
123
Figure 80 - Define Date Range Dialog
124
Figure 81 - File Structure of Data File Viewer
125
New - Time Series Plot
127
Figure 82 - Time Series Viewer
127
Time Series Viewer Menus
128
Save Configuration
128
Figure 83 - Time Series Viewer Menus
128
Figure 84 - Time Series Viewer - File Menu
128
Figure 85 - Time Series Viewer - Feature Capture
128
Take Screenshot
129
Time Series Viewer Analysis Menu
129
Figure 86 - Time Series Viewer - Analysis Menu
129
Time Series Viewer View Menu
130
Figure 87 - Histogram Window
130
The Time Series Viewer Canvas
131
Figure 88 - Time Series Viewer - View Menu
131
Figure 89 - Time Series Viewer Canvas
132
Figure 90 - Canvas Right-Click Pop-Up Menu
133
Figure 91 - Time Series Viewer Image Editor
133
Figure 92 - Time Series Viewer Dataset Options
134
Fitting Menu
135
Figure 93 - Correlation XY Plot
135
Analysis Menu
136
Figure 94 - Fitting Menu
136
Figure 95 - Analysis Menu
136
Figure 96 - Results of Quadratic Fitting
136
G Setting up Contained Exhaust Flow
137
Tools and Parts Required
137
Directions
137
Figure 97 - A2000 Pump Vacuum and Exhaust Ports
137
Figure 98 - Pump Noise Dampener Removal
138
Figure 99 - Pump Exhaust Line Adapter Fittings
138
H External Valve Sequencer
140
Introduction
140
A0311 16-Port Distribution Manifold
140
Compatibility
140
Function
140
A0311-S 16-Port Distribution Manifold (Silco)
141
Compatibility
141
Function
141
Figure 100 - A0311 - 16-Port Distribution Manifold
141
Figure 101 - A0311-S - 16-Port Sequencer - Fast Multiport Gas Sampler
141
Setting up Solenoid Valves
142
Setting up a Rotary Selector Valve
142
External Valve Sequencer Software Overview
142
Opening the Sequencer
142
Valve Sequencer UI Menus
143
Figure 102 - Launching the Valve Sequencer GUI
143
Figure 103 - Valve Sequencer UI Dropdown Menus
143
Figure 104 - External Valve Sequencer UI
144
Programming and Saving a Valve Sequence
145
Figure 105 - Example 15 Minute Sequence
146
Loading and Running a Saved Sequence
147
Loading a Saved Sequence
147
Running a Sequence
147
Skipping Steps or Advancing to a Particular Step
147
Stopping the Sequencer
147
Resetting Valves
148
Valve Sequencer Data Records
148
Figure 106 - Data Logger Service Mode
149
Scheduling a Sequence
150
I Introduction to Technology
151
Cavity Ring-Down Spectroscopy (CRDS)
151
Relating Ring-Down Time to Absorption Intensity
152
Figure 107 - Schematic of the Picarro CRDS Analyzer Cavity
152
Converting Absorption Intensity to Concentration
153
Figure 108 - Light Intensity as a Function of Time in a CRDS System
153
Spectral Precision and High Sensitivity Measurements
154
Figure 109 - Absorption Spectral Curve
154
JSDS for Koolance LIQ-702
156
Limited Warranty
172
Product Support
174

PICARRO PI5310 User Manual (161 pages)

Analyzer for N2O, CO, H2O

Brand: PICARRO | Category: Measuring Instruments | Size: 9 MB

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Measuring Instruments Laboratory Equipment Water Pump Digital Manifolds Samplers

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