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TORION T-9
PerkinElmer TORION T-9 Gas Chromatograph Manuals
Manuals and User Guides for PerkinElmer TORION T-9 Gas Chromatograph. We have
1
PerkinElmer TORION T-9 Gas Chromatograph manual available for free PDF download: User Manual
PerkinElmer TORION T-9 User Manual (276 pages)
Gas Chromatograph/Mass Spectrometer (GC/MS)
Brand:
PerkinElmer
| Category:
Laboratory Equipment
| Size: 34.96 MB
Table of Contents
Table of Contents
5
1 Introduction
11
Overview
12
Conventions Used in this Manual
12
About Notes, Cautions, and Warnings
12
2 Safety Practices
15
Overview
16
Precautions for the Instrument
17
Precautions for Customers
19
Safe Handling of Gas Cylinders
19
General Operating Conditions
20
Environmental Conditions
21
Electrical Safety
22
Electrical Requirements
23
The AC Line Cord
23
Electromagnetic Compatibility (EMC)
25
Europe
25
South Korea
25
United States (FCC)
25
Pollution Degree
25
Installation Category
25
Warning Labels
26
Warning Signs on the Instrument
28
WEEE Instructions for Perkinelmer Products
29
Decontamination
30
Cleaning the Instrument
30
3 System Overview
31
What Is Solid Phase Microextraction (SPME)
32
What Is the Torion T-9 GC/MS
33
About the Power Supply and Battery
34
What Is the Custodion SPME Syringe
35
What Is Low Thermal Mass (LTM) Gas Chromatography
36
What Is Toroidal Ion Trap Mass Spectrometry (TMS)
38
4 Basic Custodion Operations
41
Prepare the Custodion SPME Syringe for Sampling
42
Using the Custodion
43
Sample Headspace Vapors from Liquid or Solid Samples
43
Sample Gases
44
Sample Liquids
44
Sample Solids
45
Sample Unknown Liquids and Solids
45
Performing an Injection with the Custodion Syringe
48
5 Basic Operation
49
Overview
50
Startup
51
Running with External Power and Carrier Gas
51
Home Screen
54
Using the Custodion Syringe
55
Performing a System Blank Run
60
System Blank
60
SPME Blank
64
Performance Validation
67
Sample Concentration
73
Sample Analysis
75
Using Alerts for Hazardous Compounds
80
Viewing Spectra of a Specific Scan
80
Review the Results of an Analysis
86
Viewing the Results on the Torion T-9 GC/MS System
86
Previous Results
86
Quantitative Analysis
89
Exporting Files
91
Advanced Menu
94
Procedure
94
Activating a Procedure
94
Ending a Procedure
95
Selecting a Different Procedure
96
Status/Diagnostics
97
Gas Chromatography Tab
97
Mass Spectrometry Tab
97
Versions Tab
98
Status Tab
98
Edit Tab
99
Current Problems Tab
102
Performance Validation
102
Manage Files
103
Methods
104
System Settings
107
Setting the Date and Time
107
Password
108
Network Connection
108
Network Settings on the Instrument
109
Power Management
110
Shutdown
112
Turning off the System
112
Exiting the Software
113
6 Software
117
Software Programs
118
Chromion
118
Tightvnc Viewer
118
Nist
118
Chromion Installation and Operation
119
Chromion Main Screen
120
Connecting Chromion to a Networked Instrument
122
Chromion Menu Bar
128
File Menu
128
Edit Menu
129
Preferences
129
Decimal Display
129
Data Review Tab
129
Real Time Plots Tab
133
File Manager Tab
133
NIST Tab
137
Target Library
138
Hazard Levels
138
Method Menu
141
Creating a New Method
142
Load and Delete Methods
144
Importing a Method
145
Saving a Method
146
Save Method as
146
Rename Method
146
Export Method
147
Send Method to Instrument
147
Help Menu
149
Gas Chromatograph
150
Gas Chromatograph Mini Toolbar
151
GC Settings Tab
152
Heaters
152
Column
152
Split Injection
153
Sample Introduction
154
Readbacks
154
Solvent Delay
154
Retention Time Calibrations Tab
155
Target Library Editor
157
Target Library Editor Mini Toolbar
157
Target List Setup Tab
161
Mass List
161
Deconvolution Parameters Tab (Target Library Editor)
166
Deconvolution Parameters Mini Toolbar
166
Target List Search
167
Unknown Identification
168
Unknown Libraries
169
Quant Overrides Tab
170
Quant Concentrations Tab
171
Quant Files Tab
173
Quant Review Tab
174
Groups Tab
175
Performance Validation
179
Performance Validation Mini Toolbar
179
Performance Validation and Calibration Tab
181
Mass Item Table
181
Tests Section
183
Deconvolution Parameters Tab (Performance Validation)
184
Performance Validation Settings Tab
184
Mass Range Tab
184
Tools
185
Data Review
185
Data Review Mini Toolbar
185
Setting the Cursor Mode
193
Additional Functionality Icons
195
Data Review Menu Items
201
Deconvolution Window
205
Spectra Graphs/Charts
209
Add Peak to Library
209
Peak Details
210
Library Search
212
Nist
213
Mass Spectrometer
216
Mass Spectrometer Mini Toolbar
216
MS Parameters Tab
218
MS Calibrations Tab
220
File Manager
221
File Manager Mini Toolbar
221
Computer Section - Right Click Functionality
222
SD Card Section - Right Click Functionality
224
Supported File Types
226
Library Editor
227
Library Editor Mini Toolbar
228
Real Time Plots
235
Real Time Plots Mini Toolbar
235
TIC Graph Tab
236
Spectra Graph Tab
237
Data Logger Tab
237
Logging
238
Edit Data Logger Item List
238
Clear Chart
240
Desorption
241
Desorption Mini Toolbar
242
Log Data Tab
244
Batch Processing
246
Batch Processing Mini Toolbar
246
Reports
248
Reports Mini Toolbar
248
Creating a Report
248
Header Information
250
Report Data
250
Tightvnc Viewer
255
Nist
256
7 Advanced Operations
257
Loading Operational Settings When Running an Analysis
258
Reset and Restart Buttons on the Instrument
258
Deleting Sample Data from the SD Card
259
8 Maintenance
261
GC Injection Port Maintenance
262
Accessing the GC Injection Port
262
Septum Replacement
262
Injection Liner and Seal Cleaning or Replacement
263
How to "Bake Out" the GC Injection Port and Column
264
Changing the Battery
265
Changing the Carrier Gas Cartridge
266
Removing/Replacing the SD Card
267
9 Troubleshooting
269
Troubleshooting Guide
270
Torion T-9 GC/MS will Not Turn on
270
Torion T-9 GC/MS will Not Turn off
270
Torion T-9 GC/MS Cannot Maintain Vacuum
270
GC Baseline Is Noisy, or Drifts Upward
270
GC Peaks Are Asymmetric
271
GC Peaks Are Eluting Late
272
Acquired Mass Spectra Are Noisy
273
Results Are Not Reproducible
274
There Is no Instrument Signal
274
Acquired Mass Spectra Are Not Correct
274
SPME Fiber Came off Inside the GC Inlet
275
Torion T-9 GC/MS Fails to Identify a Compound
275
Torion T-9 GC/MS Falsely Identified a Compound
275
Torion T-9 GC/MS Fails to Reach Set Temperatures
275
Torion T-9 GC/MS Is Unable to Run on Battery Power
276
Torion T-9 GC/MS Suddenly Powers down
276
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