Parr Instrument Company 6300 Manuals

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Parr Instrument Company 6300 Operating Instructions Manual

Parr Instrument Company 6300 Operating Instructions Manual (130 pages)

Oxygen Bomb Calorimeter

Brand: Parr Instrument Company | Category: Measuring Instruments | Size: 2.92 MB

Table of Contents

Table of Contents
3
Preface

7
- Scope
  7
- Explanation of Symbols
  8
- Intended Usage
  8
- Fuse
  8
- General Specifications
  9
- Environmental Conditions
  9
- Getting Started
  9
Hapter

11
Concept of Operation

11
Chapter 2 Installation

13
- Required Consumables, Utilities and Power Requirements
  13
- Installing the Calorimeter
  13
  - Swagelok Tube Fittings
    14
  - General
    15
  - 6300 Calorimeter Back Panel
    16
- 6300 Calorimeter External Plumbing
  17
- Standard
  19
Hapter

21
Instrument Description

21
- Types of Controls
  21
- Menu Keys
  21
- Control Keys
  21
Hapter

23
Program Installation & Control

23
- Software Installation
  23
- Default Settings
  23
- Revising Default Settings
  23
  - 6300 Factory Default Settings
    24
  - Figure
    24
- Bombs
  24
- Network Data
  25
Hapter

27
Operating Instructions

27
- To Begin a Test
  27
- Operating the Oxygen Bomb
  27
- Figure 5-1 Fill Flow Diagram
  28
- Allowable Sample Size
  29
- Attaching the Cotton Thread
  29
  - Cotton Thread Assembly
    29
  - Pre-Period/Post-Period
    30
- Closing the Bomb
  31
- Fill Cycle
  31
- Pre-Period
  31
- Bomb Firing
  31
  - Rinse & Cool Flow Diagram
    32
- Post-Period
  33
- Cool/Rinse
  33
- Drain
  33
- Figure 5-5 Drain Flow Diagram
  34
- Samples
  35
- Combustion Aids
  35
- Oxygen Charging Pressure
  35
- Combustion Capsules
  35
- Foodstuffs and Cellulosic Materials
  36
- Coarse Samples
  36
- Corrosive Samples
  36
- Explosives and High Energy Fuels
  36
- Volatile Sample Holders
  36
- Poor Combustion
  37
  - Combustion Capsule with Adhesive Tape Seal
    37
Hapter

39
- Reports
  
  39
  - Entering Corrections and Obtaining the Final Report
    39
  - Manual Entry
    39
  - Fixed Corrections
    39
  - Acid and Sulfur
    39
Hapter

41
Reporting Instructions

42
- Report Generation
  42
- Net Heat of Combustion
  42
Chapter 8 File Management

43
- Clearing Memory
  43
- Removable SD Memory
  43
Chapter Maintenance

45
- Troubleshooting
  
  45
Appendix A Menu Operating Instructions

53
- Main Menu
  53
- Calorimeter Operation Menu
  53
Ppendix

53
- Temperature Vs. Time Plot
  54
- Temperature Plot Setup Menu
  54
- Operating Controls Menu
  55
- Data Entry Controls Menu
  59
Appendixa

53
Appendix B Calculations

60
- Run Data File Manager
  67
- Diagnostics Menu
  70
- Calculating the Heat of Combustion
  71
- Fuse Correction
  71
- General Calculations
  71
- Standardizing the
  71
- Thermochemical Corrections
  71
- Acid and Sulfur Corrections
  73
- ASTM Treatment for Acid and Sulfur
  74
- Table
  74
  - Settings for ISO & BSI Methods
    74
- Conversion to Net Heat of Combustion
  75
- ISO Calculations
  75
- Spiking Samples
  75
Appendix C

77
Appendixc C Standardization

77
Appendix D Communications Interfaces

81
- USB Port
  81
- Balance and Port Input Driver Specifications
  81
- Sartorius Balance Interface
  81
- Connection
  81
- Table
  81
- Generic Interface
  82
  - 6300 Data File Naming Convention
    82
  - 6300 Calorimeter Run Data Template
    82
- Ethernet Interface
  83
- Samba Server Feature (Optional)
  84
- Bar Code Port
  92
- Network Data Services
  92
Appendixd

81
Appendix E Technical Service

93
- Return for Repair
  93
Ppendix

93
Appendix F Drawings

96
- A1250DD2 Controller Assembly
  96
- A1251DD Oxygen Solenoid Assembly
  96
- A1252DD Water Solenoid Assembly
  96
- A1257DD Water Regulator Assembly
  97
- A1258DD Temperature Control Assembly
  97
- A1260DD Water Level Assembly
  97
- A1264DD Air Can Assembly
  98
- A1265DD Bucket and Stirrer Tube Assembly
  99
  - Parts Diagram for the 1136 and 1136CL Oxygen
    102
- Parts Diagram for the 1138 and 1138CL Oxygen
  104
- 6300 Oxygen Bomb Calorimeter Cutaway Right
  106
- Figure F
  106
- 6300 Oxygen Bomb Calorimeter Cutaway Left
  107
- 6300 Oxygen Bomb Calorimeter Cover Open
  108
- A1250DD2 Control Schematic
  109
- A1251DD Oxygen Solenoid Assembly
  110
- A1200DD Internal Plumbing Diagram
  111
- A1252DD Water Solenoid Assembly
  112
- A1416DD Bomb Wash Pump Assembly and Fittings
  113
- A1254DD Circulatory Pump Assembly
  114
- A1255DD Bucket Stirrer Assembly
  115
- A1256DD Water Assembly Tank
  116
- A1257DD Water Regulator Assembly
  117
- A1258DD Temperature Control Assembly
  118
- Cover Contact Pin Assembly
  119
- Stirrer Motor and Mount
  120
- A1260DD Water Level Control Assembly
  121
- A1265DD Bucket Assembly
  122
- 6300 Air Can Assembly
  123
  - A1450DD Bomb Head Assembly (1)
    124
  - A1450DD Bomb Head Assembly (2)
    125
Appendix G Bomb Rinse Container Assembly

127
- Overview
  127
- Concept of Operation
  127
  - Bombs
    128
- Vessel Rinse Container
  128
- Figure G
  128
Appendixg

127

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