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Parr Instrument Company 6300 Operating Instructions Manual

Oxygen bomb calorimeter
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NO. 586M
Parr Instrument Company
6300
Oxygen Bomb Calorimeter
Operating Instruction Manual
For models produced after October 2010

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Summary of Contents for Parr Instrument Company 6300

  • Page 1 NO. 586M Parr Instrument Company 6300 Oxygen Bomb Calorimeter Operating Instruction Manual For models produced after October 2010...

  • Page 3: Table Of Contents

    — 43 Required Consumables, Utilities and Power ANAGEMENT Requirements — 13 Clearing Memory — 43 Installing the Calorimeter — 13 Removable SD Memory — 43 6300 Calorimeter External Plumbing — 17 HAPTER HAPTER & T — 45 AINTENANCE ROUBLESHOOTING — 21...
  • Page 4 PPENDIX Table D-1 — 81 OMMUNICATIONS NTERFACES 6300 Data File Naming Convention — 82 USB Port — 81 Table D-2 Balance and Port Input Driver Specifications — 81 6300 Calorimeter Run Data Template — 82 Mettler 011/012 Balance Interface — 81 Sartorius Balance Interface —...
  • Page 5 6300 Oxygen Bomb Calorimeter Cutaway Right — Figure F-4 6300 Oxygen Bomb Calorimeter Cutaway Left — Figure F-5 6300 Oxygen Bomb Calorimeter Cover Open — 108 Figure F-6 A1250DD2 Control Schematic — 109 Figure F-7 A1251DD Oxygen Solenoid Assembly — 110 Figure F-8 A1200DD Internal Plumbing Diagram —...
  • Page 6 ABLE OF ONTENTS This page left blank intentionally. P a r r I n s t r u m e n t C o m p a n y...

  • Page 7: Preface

    483M Introduction to Bomb Calorimetry This manual contains instructions for installing and operating the Parr 6300 Calorimeter. For ease of use, Additional instructions for the printer, cooler, and water the manual is divided into nine chapters. handling systems are found in the respective package and should be made a part of this book.

  • Page 8: Explanation Of Symbols

    This device contains components which may ignite calling Parr Instrument Company in order to determine which part(s) may be replaced or serviced. such material.

  • Page 9: General Specifications

    A, to review the menu functions used to modify Current: The total current drawn should not exceed the the program contained in the 6300 Calorimeter. A rating shown on the data plate on the calorimeter by review of the menus will provide a good idea of more than 10 percent.
  • Page 10 REFACE This page left blank intentionally. P a r r I n s t r u m e n t C o m p a n y...

  • Page 11: Hapter

    SOPERIBOL PERATION In the 6300 Oxygen Bomb Calorimeter most of the manual operations in conventional bomb calorimetry have been eliminated by a new technology centered In Isoperibol operation, the calorimeter jacket is held...

  • Page 12: Full Microprocessor Based Process Control

    • Enhanced testing and trouble shooting procedure. for all required data and control input and to: • The 6300 Calorimeter is equipped with a USB Generate all temperature readings in the connection plus an Ethernet port for direct calorimeter. •...

  • Page 13: Installation

    6300 NSTALLATION NSTALLING THE ALORIMETER HAPTER Each Parr 6300 Calorimeter was completely assembled NSTALLATION and thoroughly tested prior to shipment. The following stepwise procedure will guide the user through the installation process. EQUIRED ONSUMABLES TILITIES AND • Unpack the calorimeter and carefully check the...

  • Page 14: Swagelok Tube Fittings

    NSTALLATION printer and the connections at the rear of the NSTALLING THE ALORIMETER ONTINUED calorimeter. Install the printer ribbon and printer paper at this time. Apply power to the calorimeter • Make the connections to the oxygen supply at and turn on the printer. this time.

  • Page 15: General

    6300 NSTALLATION Fitting. Make sure that the tubing rests firmly on the shoulder of the fitting and that the nut is finger- Insert the tubing with pre-swaged ferrules into the tight. fitting body until the front ferrule seats. Before tightening the Swagelok nut, scribe the nut at Tighten the nut by hand.

  • Page 16: 6300 Calorimeter Back Panel

    NSTALLATION Figure 2-2 6300 Calorimeter Back Panel P a r r I n s t r u m e n t C o m p a n y...

  • Page 17: 6300 Calorimeter External Plumbing

    6300 NSTALLATION 6300 C ALORIMETER XTERNAL LUMBING Figure 2-3 Closed Loop Confi guration with 6520A O2 Regulator DI Water ~Room Temp 5-10 °C Rinse Collection 6520A Water Recircualtion System Figure 2-4 Closed Loop Confi guration with 1564 O2 Regulator DI Water ~Room Temp 5-10 °C...
  • Page 18 NSTALLATION 6300 C ALORIMETER XTERNAL LUMBING ONTINUED Figure 2-5 Open Loop Confi guration with 1552 O2 Regulator Tap Water · <25 °C DI Water · <85 ppm ~Room Temp · <60 psig 1552 Water Cooler Rinse Collection Drain Figure 2-6 Open Loop Confi...

  • Page 19: Standard

    6300 NSTALLATION ENTER to store the default sample mass of 1 gram. NSTALLING THE ALORIMETER ONTINUED This test should go through Fill, Pre-period, Post- period and Cool/Rinse Cycles without error. The • calorimeter is now ready to be standardized. After the calorimeter displays the main menu, press the Calorimeter Operation button.
  • Page 20 NSTALLATION This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 21: Hapter

    6300 NSTRUMENT ESCRIPTION Some keys lead to multiple choices. Always clear HAPTER the current value before entering a new value. Once entered the screen will revert to the previous menu NSTRUMENT ESCRIPTION and the new value will be displayed in the lower right corner of the key.
  • Page 22 NSTRUMENT ESCRIPTION This page left blank intentionally. P a r r I n s t r u m e n t C o m p a n y...

  • Page 23: Hapter

    • Establish the operating parameters to be stored as The program in the 6300 Calorimeter can be extensively the user default settings. modified to tailor the unit to a wide variety of operating conditions, reporting units, laboratory techniques, •...

  • Page 24: Figure

    & C ROGRAM NSTALLATION ONTROL Figure 4-1 6300 Factory Default Settings Calorimeter Operations User Function Setup Cold Restart Operating Mode Determination Bomb Installed/EE 1/940.0 User/Factory Settings Heater and Pump User Setup ID 63-1138 Reload Factory Default Settings Operating Controls Reload User Default Settings...

  • Page 25: Network Data

    6300 & C ROGRAM NSTALLATION ONTROL Factory Default Settings Continued Acid Multiplier 0.0709 Automatic Reporting Sulfur Value is Percent Auto Report Destination Printer Sulfur Multiplier 0.6238 Individual Printed Reports Fuse Multiplier Edit Final Reports Use Offset Correction (ISO) Recalculate Final Reports...
  • Page 26 & C ROGRAM NSTALLATION ONTROL This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 27: Hapter

    6300 PERATING NSTRUCTIONS PERATING THE XYGEN HAPTER Combustion with oxygen in a sealed bomb is a very PERATING NSTRUCTIONS effective and reliable method for releasing all heat energy obtainable from a sample, and for preparing hydrocarbon compounds and carbonaceous materials EGIN A for analysis.

  • Page 28: Figure 5-1 Fill Flow Diagram

    PERATING NSTRUCTIONS Figure 5-1 Fill Flow Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 29: Allowable Sample Size

    6300 PERATING NSTRUCTIONS Figure 5-2 LLOWABLE AMPLE Cotton Thread Assembly To stay within safe limits, the bomb should never be charged with a sample which will release more than 8000 calories when burned in oxygen. The initial oxygen pressure is set at 30 atmospheres (450 psig).

  • Page 30: Pre-Period/Post-Period

    PERATING NSTRUCTIONS WARNING - DO NOT OVERFILL THE BOMB The safety relief valve on the regulator should protect the system from an over fi ll. If for any reason, the bomb should accidentally be charged to more than 600 psig (40 atm), do not fi re the bomb. The danger- ous pressures which might develop under such conditions could damage the bomb and injure the operator.

  • Page 31: Closing The Bomb

    6300 PERATING NSTRUCTIONS at the top of the bomb closes and isolates the bomb LOSING THE from the oxygen filling line. Care must be taken not to disturb the sample when The controller monitors the operating temperature moving the bomb head from the support stand to the until it confirms that the initial equilibrium has been bomb cylinder in the calorimeter.

  • Page 32: Rinse & Cool Flow Diagram

    PERATING NSTRUCTIONS Figure 5-4 Rinse & Cool Flow Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 33: Post-Period

    6300 PERATING NSTRUCTIONS ERIOD RAIN After fi ring is confi rmed, the post-period begins (see At the completion of the bomb rinse sequence, the Figure 5-3). drain sequence begins (see Figure 5-5). The controller monitors the temperature rise and The water in the bucket is drained out of the bucket determines the final temperature rise by either the and routed to the drain connection.

  • Page 34: Figure 5-5 Drain Flow Diagram

    PERATING NSTRUCTIONS Figure 5-5 Drain Flow Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 35: Samples

    60 mesh, or smaller, and compressed into a pellet with a 2811 Parr Pellet Press. The 6300 Calorimeter has been designed to operate with an oxygen filling pressure of 30 atm. Significant Large particles may not burn completely and small changes from this value are not recommended.

  • Page 36: Foodstuffs And Cellulosic Materials

    1138CL Bomb. tape which might interfere with the determination. The approximate Heat of Combustion of the tape is 6300 These bombs are 250 mL in volume and are rated to a cal/g. An actual amount should be determined by run- maximum working pressure of 2000 psi.

  • Page 37: Poor Combustion

    6300 PERATING NSTRUCTIONS Note: OMBUSTION Tape should always be stored in a sealed container to minimize changes in its moisture and solvent content Because of the difference in combustion characteristics of the many different materials which may be burned in...
  • Page 38 PERATING NSTRUCTIONS This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 39: Hapter

    6300 & F ORRECTIONS INAL EPORTS If the Spiking Correction is used, a spiking correction HAPTER must be entered before obtaining a Final Report. & F ORRECTIONS INAL After the last entry has been made, the calorimeter will automatically produce a Final Report.
  • Page 40 & F ORRECTIONS INAL EPORTS This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 41: Hapter

    Select From List This key displays the stored results specified with the following two keys: The 6300 Calorimeter can transmit its stored test data in either of two ways. The REPORT DESTINATION Run Data Type key on the Reporting Controls Page toggles the report...

  • Page 42: Reporting Instructions

    EPORTING NSTRUCTIONS EPORT ENERATION ONTINUED The EDIT key brings up a sub-menu which enables the operator to edit any of the data in the report or add thermochemical corrections to convert preliminary reports to final reports. Final reports can only be edited if EDIT FINAL reports on the reporting control page is turned on.

  • Page 43: File Management

    The RUN DATA FILE MANAGER key leads to a listing of the files. The 6300 Calorimeter will hold data for 1000 tests in its • Single files can be deleted by highlighting the file memory.
  • Page 44 ANAGEMENT This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 45: Chapter Maintenance

    Quarterly Fuses Change water in the Water Tank and replace the 1245DD and 149C water filters. The replacement of protective fuses for the 6300 Calorimeter should be performed by qualified personnel. 500 Tests Under normal usage Parr oxygen bombs will give long All fuses except Parr part # 139E23 are located on service if handled with reasonable care.
  • Page 46 • The bomb has been machined by any source other thermistor probe. Set this unit aside. than Parr Instrument Company. Remove the vessel spacer, 964DD and the associ- ated O-ring, 969DD. After repeated use with samples high in chlorine (over...
  • Page 47 6300 & T AINTENANCE ROUBLESHOOTING 6300 M AINTENANCE HECKLIST Quarterly Maintenance Date Date Date Date Change water Replace 149C Clean grill on heat sink.(6520A) 50 to 100 Test Maintenance Date Date Date Date Replace 8400DD2 Heating Wire Clean 986DD Elec-...

  • Page 48: Inspection Of Critical Sealing Surfaces

    & T AINTENANCE ROUBLESHOOTING applying sufficient pressure on the seal to cause it to NSPECTION OF RITICAL EALING URFACES pucker out of the groove. With the other hand, grab the exposed, pinched section and pull the seal from The sealing grooves and related surfaces for most of the groove.
  • Page 49 6300 & T AINTENANCE ROUBLESHOOTING The second condition can be eliminated by replacing WARNING: the tubing and clearing all connections. This screen allows unconditional and arbi- The third condition can be eliminated by following the trary output control for testing purposes. Be...

  • Page 50: Jacket Fill And Cooling Problems

    Turn off the water handling system and re-attach jacket fill process. To troubleshoot this error start with the water filter and tube to the back of the 6300. step 3 below. Refill the water handling system if it needs it. Turn the water handling system back on.

  • Page 51: Bomb Removal And Replacement

    To replace, follow these steps in reverse. and re-start the unit. However, if this error occurs more than three times in a row, then it may be a true 6300 C ALORIMETER RROR thermistor problem and the user should contact Parr Technical Service.
  • Page 52 & T AINTENANCE ROUBLESHOOTING Rinse Tank Level May Be Low. You Have Exceeded The Run Data File Limit (1000 The controller decrements the rinse tank counter each Files). The memory set aside for test runs has been filled. Use time the bomb is rinsed. This message will be issued the memory management techniques to clear out non- when the counter is at or below zero when the bomb current tests.

  • Page 53: Appendixa

    This appendix describes all pages of the menu-based This key appears in the Escape key location when the operating system of the 6300 Calorimeter. main menu is displayed. This key is used to shut down the calorimeter program before turning off the power.

  • Page 54: Temperature Vs. Time Plot

    PERATING NSTRUCTIONS ALORIMETER PERATION EMPERATURE ETUP ONTINUED Start Preweigh: This key is used to start the sample pre-weigh process. The user is presented with or prompted for a sample ID. Next, the user is asked to key in the associated sample mass or alternatively the mass is retrieved from a con- nected balance.

  • Page 55: Operating Controls Menu

    6300 PERATING NSTRUCTIONS Jacket Plot Symbol: PERATING ONTROLS Toggles between: (same as Bucket Plot Color, p. 54). Jacket Min Value: Press this key to access its numeric dialog box to set a minimum jacket value. Time Window: Sets the time scale for the X-axis.
  • Page 56 PERATING NSTRUCTIONS • Report Rinse Tank Empty. When turned on the PERATING ONTROLS ONTINUED calorimeter will notify the user when it believes the rinse tank is empty based upon capacity of • Use Spiking. When set to ON, the calorimeter tank and number of tests.
  • Page 57 6300 PERATING NSTRUCTIONS “Other” Multiplier: Date & Time: Press this key to display the Other Multiplier dialog Accesses a sub-menu to set the current date and time. box, where the user can enter a final multiplier to be used when the reporting units are set to “Other”.
  • Page 58 PERATING NSTRUCTIONS Bomb Type Select: ROGRAM NFORMATION AND ONTROL This key toggles through the different bomb models ONTINUED available for the calorimeter. When the user chooses a bomb, the instrument must be re-booted to load the cor- rect version of the software. (Note that the calorimeter will not let you exit this function without re-booting the system).

  • Page 59: Data Entry Controls Menu

    • Bomb EE Value. Displays the calculated EE value. The 6300 is a .1 Process Sigma calorimeter. • # Runs, EE Val. Displays how many runs have been used to determine the EE value. •...

  • Page 60: Calculations

    Protect EE Value: Toggles between OFF and ON. When set to OFF, the 6300 automatically updates the EE value as new tests are run. When set to ON, it keeps the EE value pro- tected, whether it has been revised manually via the Manual EE Entry key or calculated by the instrument.
  • Page 61 Options for the Acid Correction: When any fixed correction is set to ON, the specified value will be used in the final reports, and the 6300 Fixed HNO will not prompt for actual corrections to be entered. Calculated HNO...
  • Page 62 PERATING NSTRUCTIONS Nitric Acid Factor: HERMOCHEMICAL ALCULATIONS Ratio of the nitric acid correction when the released ONTINUED energy corresponds to 6318 calories. The default is 1.58 calories per 1000 calories of released energy. Fixed Sulfur Correction: Acid Multiplier: Press this key on the LEFT side to toggle ON or OFF This multiplier is the normality of the sodium carbonate the fixed sulfur correction for determination runs.
  • Page 63 6300 PERATING NSTRUCTIONS ACTORS NTRY ONTROLS Fixed Hydrogen: Prompt for Bomb ID: Press the LEFT side to toggle this setting On/Off. Toggles ON or OFF. In the ON position the controller Press the RIGHT side to display the Fixed Hydrogen will prompt for a Bomb ID (1-4) when a test is started.
  • Page 64 PERATING NSTRUCTIONS • Next Auto Sample ID Number. Establishes the NTRY ONTROLS ONTINUED initial sample number for a series of tests and then shows the next sample ID which will be as- Hydrogen Entry Mode: signed. Used when the Automatic Sample ID is This key steps through the options for entering hydro- set to ON.
  • Page 65 6300 PERATING NSTRUCTIONS Moisture as Received Entry Mode: EPORTING ONTROLS This key steps through the options for entering the moisture as received correction value either manually or Report Width: through the touch screen or automatically through the Toggle this key to set the column width of the printer balance (USB) port.
  • Page 66 PERATING NSTRUCTIONS Balance Port: EPORTING ONTROLS ONTINUED Accesses sub-menu, Balance Port Communications. Use New EE Value in Recalculation: When set to ON, any recalculation made will use the most recent EE value in the calculations. In the OFF position, all calculations will be made using the EE value which was effective when the test was originally run.

  • Page 67: Run Data File Manager

    6300 PERATING NSTRUCTIONS ANAGEMENT » Data Precision. This key allows the user to establish the number of digits to the right of the decimal point that are passed from the Run Data File Manager: balance handler. This key activates the File Manager. The File Manager »...
  • Page 68 PERATING NSTRUCTIONS ANAGER IAGNOSTICS The white upper portion of the Run Data File Manager Provides the user with the means to test many of the screen presents all tests in memory in a scrollable win- components and subsystems of the calorimeter. These dow.
  • Page 69 6300 PERATING NSTRUCTIONS keys for fifteen items that can be individually selected for logging. By default, both the bucket and jacket temperatures are logged. All records are date and time stamped. Helpful items to log are: » D0 - Corrected calorimeter drift rate »...

  • Page 70: Diagnostics Menu

    PERATING NSTRUCTIONS I/O Diagnostics: IAGNOSTICS ONTINUED • Combine Det. Reports. Pressing this key com- bines all determination reports into a single file named /tmp/bigdetfile.txt. • Combine Std. Reports. Pressing this key com- bines all determination reports into a single file named /tmp/bigstdfile.txt.

  • Page 71: Calculating The Heat Of Combustion

    Celsius. Since it is directly related to the mass of the calorimeter, it will change whenever any The 6300 Calorimeter will automatically make all of of the components of the calorimeter (i.e. the bomb, the calculations necessary to produce a gross heat of bucket or amount of water) is changed.
  • Page 72 Thermochemical Calculation Details The 6300 Calorimeter can be set up to apply the acid Traditionally, standard solutions and procedures have correction by either the ASTM or ISO convention, as...

  • Page 73: Acid And Sulfur Corrections

    (heat of formation of H2SO4). value which appears in the test report. Acid Correction: Note: In the 6300 there are a number of settings for the acid Calculation Factors,- Fuse Multiplier is normally set to correction. 1.0 so the entered value is in calories.

  • Page 74: Astm Treatment For Acid And Sulfur

    ALCULATIONS Example: For a test run with energy equivalent of CID AND ULFUR ORRECTIONS 927.4022 and a corrected temperature rise of 6.892 ONTINUED would result: e1 = (1.58/1000)(927.4022)(6.892) Fixed Total: The Acid Correction represents the e1 = 10.0988 calories total base required to titrate the bomb washings (in milliliters).

  • Page 75: Iso Calculations

    Hcs = Heat of combustion of the spiking somewhat different than ASTM procedures. Provision material (cal/g) has been made in the 6300 Controller for dealing with = Mass of spiking material these different procedures. This factor is added to the calculations when Spike The analysis of bomb washings in these methods call Controls, Use Spiking is set to ON.
  • Page 76 ALCULATIONS This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...

  • Page 77: Appendixc C Standardization

    UTOMATIC TATISTICAL ALCULATIONS substituting the following equation: The 6300 Calorimeter includes a provision for Hm + e calculating and using a mean energy equivalent for each of up to 4 separate bomb and bucket combinations. ASTM procedures recommend that the energy Where: equivalent be determined by averaging ten tests.

  • Page 78: Automatic Statistical Calculations

    TANDARDIZATION The user can elect to have any number of stored UTOMATIC TATISTICAL ALCULATIONS standardization runs used in determining the EE value ONTINUED by entering this number on Calibration Data & Controls Page - Calibration Run Limit. Any outliers or other tests which should not be included EE Max Std Deviation on this same page establishes in the average EE Value must be deleted from the the maximum allowable standard deviation for the EE...

  • Page 79: Calorimeter Control Limit Values In Cal/G When Benzoic Acid Is Used As A Test Sample

    6300 TANDARDIZATION Table C-2 Calorimeter Control Limit Values in cal/g When Benzoic Acid is Used as a Test Sample Accepted heat of combustion taken as 6318 cal/g. Instrument precision 0.10%. Control limits based on 99% confidence (3 sigma) values. Values are in cal/g.

  • Page 80: Calorimeter Control Limit Values In Btu/Lb When Benzoic Acid Is Used As A Test Sample

    TANDARDIZATION Table C-3 Calorimeter Control Limit Values in BTU/lb When Benzoic Acid is Used as a Test Sample Accepted heat of combustion taken as 11373 BTU/lb. Instrument precision 0.10%. Control limits based on 99% confidence (3 sigma) values. Values are in BTU/lb. NUMBER OF UCL FOR THE RANGE UCL FOR THE...

  • Page 81: Appendixd

    USB P USB Connection The 6300 Calorimeter is equipped with a USB port for connection to either a 40 or 80 column printer and/or a The ID field must contain “S_” to indicate a stable computer. mass. The data field contains the current mass, right justified, with a decimal point.

  • Page 82: Generic Interface

    JacketTemp jacket temperature InitTemp initial temperature Table D-1 DeltaT temperature rise 6300 Data File Naming Convention gross heat of combustion NetHOC dry net HOC (net calc options en- Test data files are named with the following convention. abled) Test Type...

  • Page 83: Ethernet Interface

    6300 OMMUNICATIONS NTERFACES Users who don’t have a network infrastructure can THERNET NTERFACE create a simple network by connecting a router with DHCP server capability to the calorimeter using an Calorimeter test data can be transferred to an Ethernet ordinary CAT 5 network cable. The calorimeter should network connected computer using the FTP File Trans- be connected to LAN side of the router.

  • Page 84: Samba Server Feature (Optional)

    Main Menu. Next, select FEATURE KEY and enter the feature key purchased from Parr Instru- The Samba server feature option in the Parr 6300 Calo- ment Company into the instrument by using the touch- rimeter offers seamless file services to Windows based pad.
  • Page 85 6300 OMMUNICATIONS NTERFACES The following screenshot illustrates the contents of the calorimeter data directory as presented by a web browser. w w w . p a r r i n s t . c o m...
  • Page 86 OMMUNICATIONS NTERFACES The calorimeter offers a web server service. Test reports can be viewed with a web browser using a URL of the fol- lowing form. http://10.1.5.10 Where 10.1.5.10 is the IP address of the calorimeter. The following screenshot illustrates the calorimeter home page. P a r r I n s t r u m e n t C o m p a n y...
  • Page 87 6300 OMMUNICATIONS NTERFACES Clicking on the Config button will display the screen below. Changes made on this screen will change the settings in the calorimeter. w w w . p a r r i n s t . c o m...
  • Page 88 OMMUNICATIONS NTERFACES Clicking on the Run Data button displays a list of reports currently in the instrument memory. Clicking on a test under the select sample ID box will display the data for the selected sample ID. P a r r I n s t r u m e n t C o m p a n y...
  • Page 89 6300 OMMUNICATIONS NTERFACES Clicking on the System Info button will display the screen below. w w w . p a r r i n s t . c o m...
  • Page 90 Note: This is a picture only. The calorimeter cannot be remotely operated from this screen. Remote operation requires the ap- propriate Feature Key. Please contact Parr Instrument Company for more details about available Feature Keys. P a r r I n s t r u m e n t...
  • Page 91 6300 OMMUNICATIONS NTERFACES Clicking on the Documentation button will display the screen below. Clicking on any of the links will open the cor- responding web page. Note: Connection to the internet is required for these links. w w w . p a r r i n s t . c o m...

  • Page 92: Bar Code Port

    AND CONTROL key from the Main Menu. Next, select FEATURE KEY and enter the feature key purchased from Parr Instrument Company into the instrument by using the touch pad. Pressing the key labeled “ABC” allows the user to switch from upper case letters, to lower case letters and finally to numerals.

  • Page 93: Appendix E Technical Service

    Any correspondence must include the following basic Ship repair to: information: Parr Instrument Company The model and serial # of the instrument. Attn: Service Department Software version(s) shown on the “Software and RMA # XXXX Hardware Information”...
  • Page 94 ECHNICAL ERVICE This page intentionally left blank. P a r r I n s t r u m e n t C o m p a n y...
  • Page 95 Propeller Assembly, stirrer A1256DD Water Tank Assembly A1257DD Water Regulator Assembly A1260DD Water Level Assembly A1264DD Air Can Assembly 6300 A1265DD Bucket and Stirrer Tube Assembly A1275DDEB Cartridge, Heater Assembly, 120V A1275DDEE Cartridge, Heater Assembly, 230V A1274DD Wash Pump Divert Valve Assembly...

  • Page 96: Drawings

    & D ARTS ISTS RAWINGS A1250DD2 C ONTROLLER SSEMBLY Item Description 1926E Film Guard, LCD 1802E A1821E Speaker Assembly with Cable A1822E Power Cable Assembly A1823E Touchscreen Cable Assembly, 12” A2140E I/O Board A2141E LCD Transition Board A2154E CPU Board (GCM) A2163E LCD Cable A2164E...

  • Page 97: A1257Dd Water Regulator Assembly

    ISTS RAWINGS A1257DD W ATER EGULATOR SSEMBLY Item Description 1211DD Bracket, Water Regulator 1244DD Regulator, Water, 6300 1245DD Filter, Water, 1/4 NPT 447VB Connector, Female, 1/4 T X 1/4 NPTF 60HW3HJ Hose Barb, Nylon A1258DD T EMPERATURE ONTROL SSEMBLY Item...

  • Page 98: A1264Dd Air Can Assembly

    1037DD Baffle, Bucket, Brass 1137DD Snap Ring, 0.75” 1138DD O-ring, 1/2” I.D. 1139DD Insert, Cylinder 1140DD Cylinder, Bomb Release, 6300 1141DD Spacer 1143DD O-ring, Type 316, .614 ID x .07 CS 1235DD Gasket, Air Can A1248DD2 Air Can Assembly,6300 A92HWAD Male Connector, 1/4T –...

  • Page 99: A1265Dd Bucket And Stirrer Tube Assembly

    946DD Seal ¼ SS 1129DD Pin, Anti-rotating (A940DD) 1416E Thermistor, Bucket 1462E2 Thermistor Cable A940DD Tube Assy, Bucket; Soldered A1255DD Bucket Stirrer Assembly, 6300 w w w . p a r r i n s t . c o m...
  • Page 100 Ball Bearing, .50 OD 690DD V-Seal, Nitrile 715HC O-ring NBR 1-1/4 ID 954DD Propeller 1029DD Baffle Assembly 1242DD2 Pulley, Timing (6300) SA114ORD04 4-40 X 1/4 RHMS 18-8 SS SN1140HLHJ Nut, 4-40 Hex Lock A1266DD C OVER SSEMBLY Item Description Contact Pin Assembly...
  • Page 101 Filter, In Line 1/8T BR 15 Mic 1235DD Gasket, Air Can 6300 1241DD Belt, Timing 6300 A1395DD Tubing Kit, Water Replace 6300 1245DD Filter, Water; Brass Mini 1/4M w w w . p a r r i n s t . c o m...

  • Page 102: Parts Diagram For The 1136 And 1136Cl Oxygen

    & D ARTS ISTS RAWINGS Figure F-1 Parts Diagram for the 1136 and 1136CL Oxygen Bombs P a r r I n s t r u m e n t C o m p a n y...
  • Page 103 6300 & D ARTS ISTS RAWINGS 1136 1136CL O XYGEN Key No. Item Description 888DD2 Cylinder 889DD Outer Ring 821DD (2) O-ring 1/16 ID NBR 668DD Check Valve 882DD O-ring 1/2 ID NBR 925DD Bomb Retainer SA1632RD06 (2) 8-32 x 3/8 RHMS...

  • Page 104: Parts Diagram For The 1138 And 1138Cl Oxygen

    & D ARTS ISTS RAWINGS Figure F-2 Parts Diagram for the 1138 and 1138CL Oxygen Bombs P a r r I n s t r u m e n t C o m p a n y...
  • Page 105 6300 & D ARTS ISTS RAWINGS 1138 1138CL O XYGEN Key No. Item Description 888DD2 Cylinder 889DD Outer Ring 821DD O-ring 1/16 ID NBR 668DD Check Valve 882DD O-ring 1/2 ID NBR 925DD Bomb Retainer SA1632RD06 (2) 8-32 x 3/8 RHMS...

  • Page 106: 6300 Oxygen Bomb Calorimeter Cutaway Right

    & D ARTS ISTS RAWINGS Figure F-3 6300 Oxygen Bomb Calorimeter Cutaway Right P a r r I n s t r u m e n t C o m p a n y...

  • Page 107: 6300 Oxygen Bomb Calorimeter Cutaway Left

    6300 & D ARTS ISTS RAWINGS Figure F-4 6300 Oxygen Bomb Calorimeter Cutaway Left w w w . p a r r i n s t . c o m...

  • Page 108: 6300 Oxygen Bomb Calorimeter Cover Open

    & D ARTS ISTS RAWINGS Figure F-5 6300 Oxygen Bomb Calorimeter Cover Open P a r r I n s t r u m e n t C o m p a n y...

  • Page 109: A1250Dd2 Control Schematic

    6300 & D ARTS ISTS RAWINGS Figure F-6 A1250DD2 Control Schematic w w w . p a r r i n s t . c o m...

  • Page 110: A1251Dd Oxygen Solenoid Assembly

    & D ARTS ISTS RAWINGS Figure F-7 A1251DD Oxygen Solenoid Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 111: A1200Dd Internal Plumbing Diagram

    6300 & D ARTS ISTS RAWINGS Figure F-8 A1200DD Internal Plumbing Diagram w w w . p a r r i n s t . c o m...

  • Page 112: A1252Dd Water Solenoid Assembly

    & D ARTS ISTS RAWINGS Figure F-9 A1252DD Water Solenoid Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 113: A1416Dd Bomb Wash Pump Assembly And Fittings

    6300 & D ARTS ISTS RAWINGS Figure F-10 A1416DD Bomb Wash Pump Assembly and Fittings w w w . p a r r i n s t . c o m...

  • Page 114: A1254Dd Circulatory Pump Assembly

    & D ARTS ISTS RAWINGS Figure F-11 A1254DD Circulatory Pump Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 115: A1255Dd Bucket Stirrer Assembly

    6300 & D ARTS ISTS RAWINGS Figure F-12 A1255DD Bucket Stirrer Assembly Note: Apply thread sealant (Locktite or equivalent) to set screw in 1242DD2 pulley before installing. w w w . p a r r i n s t . c o m...

  • Page 116: A1256Dd Water Assembly Tank

    & D ARTS ISTS RAWINGS Figure F-13 A1256DD Water Assembly Tank P a r r I n s t r u m e n t C o m p a n y...

  • Page 117: A1257Dd Water Regulator Assembly

    6300 & D ARTS ISTS RAWINGS Figure F-14 A1257DD Water Regulator Assembly w w w . p a r r i n s t . c o m...

  • Page 118: A1258Dd Temperature Control Assembly

    & D ARTS ISTS RAWINGS Figure F-15 A1258DD Temperature Control Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 119: Cover Contact Pin Assembly

    6300 & D ARTS ISTS RAWINGS Figure F-16 Cover Contact Pin Assembly w w w . p a r r i n s t . c o m...

  • Page 120: Stirrer Motor And Mount

    & D ARTS ISTS RAWINGS Figure F-17 Stirrer Motor and Mount P a r r I n s t r u m e n t C o m p a n y...

  • Page 121: A1260Dd Water Level Control Assembly

    6300 & D ARTS ISTS RAWINGS Figure F-18 A1260DD Water Level Control Assembly w w w . p a r r i n s t . c o m...

  • Page 122: A1265Dd Bucket Assembly

    & D ARTS ISTS RAWINGS Figure F-19 A1265DD Bucket Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 123: 6300 Air Can Assembly

    6300 & D ARTS ISTS RAWINGS Figure F-20 6300 Air Can Assembly w w w . p a r r i n s t . c o m...

  • Page 124: A1450Dd Bomb Head Assembly (1)

    & D ARTS ISTS RAWINGS Figure F-21 A1450DD Bomb Head Assembly (1) P a r r I n s t r u m e n t C o m p a n y...

  • Page 125: A1450Dd Bomb Head Assembly (2)

    6300 & D ARTS ISTS RAWINGS Figure F-22 A1450DD Bomb Head Assembly (2) w w w . p a r r i n s t . c o m...
  • Page 126 & D ARTS ISTS RAWINGS This page left blank intentionally. P a r r I n s t r u m e n t C o m p a n y...

  • Page 127: Appendixg

    6300 Calorimeter. This device allows for complete and systematic recovery of Break the connection at the rear of the 6300 Calorim- the bomb combustion products. eter to the bomb exhaust hose. In place of this, connect the “tube and 3/8”...

  • Page 128: Bombs

    10% chlorine and liberates at least 5000 calo- ries. Five thousand calories corresponds to roughly a Most users find it useful to add the contents of the 6.4 °C temperature rise in a 6300 Calorimeter. rinsed combustion capsule to the washings collected in the bottle.
  • Page 130 nstrument ompany 211 53rd Street Moline, Illinois 61265 USA Phone: 1-309-762-7716 or 1-800-872-7720 Fax: 1-309-762-9453 E-mail: parr@parrinst.com http://www.parrinst.com Revision 11/5/10...

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