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2.850.2230
Metrohm 2.850.2230 Manuals
Manuals and User Guides for Metrohm 2.850.2230. We have
1
Metrohm 2.850.2230 manual available for free PDF download: Manual
Metrohm 2.850.2230 Manual (150 pages)
Anion - MSM-HC - MCS - LP Gradient
Brand:
Metrohm
| Category:
Laboratory Equipment
| Size: 5 MB
Table of Contents
Table of Contents
5
1 Introduction
11
Instrument Description
11
Intended Use
13
About the Documentation
14
Symbols and Conventions
14
Safety Instructions
15
General Notes on Safety
15
Electrical Safety
15
Tubing and Capillary Connections
16
Flammable Solvents and Chemicals
16
Recycling and Disposal
16
2 Overview of the Instrument
18
Front
18
Figure 1 Front 850 Professional IC - Anion - MSM-HC - MCS - LP Gradi
18
Ent
18
Rear
20
Figure 2 Rear 850 Professional IC Anion - MSM-HC - MCS - LP Gradient
20
3 Installation
23
About this Chapter
23
Initial Installation
23
Installation of the Low Pressure Gradient
26
Installation Diagram
27
Figure 3 Installation Diagram
28
Setting up the Instrument
30
Packaging
30
Checks
30
Location
30
Capillary Connections in the IC System
30
Figure 4 Connection of Capillaries with Pressure Screws
31
Rear of the Instrument
32
Rollers and Handle
32
Figure 5 Rollers and Handle
33
Figure 6 Handle as Mpak Holder
34
Positioning and Connecting the Detector
35
Figure 7 Removable Rear Panel
35
Transport Locking Screws
37
Leak Sensor
37
Drainage Tubing
38
Figure 8 Connection for the Leak Sensor on the Rear of the Instrument
38
Figure 9 Drainage Tubing
39
Capillary and Cable Feed-Throughs
40
Figure 10 Capillary Feed-Throughs on the Doors
41
Figure 11 Capillary Feed-Throughs Base Tray/Covering Plate
42
Eluent
43
Connecting Eluent Bottle
43
Figure 12 Installing Eluent Bottle Attachment
44
Figure 13 Mounting Aspiration Filter
44
Figure 14 Installing Tubing Weighting and Aspiration Filter
45
Figure 15 Eluent Aspiration Tubing Fully Equipped
45
Figure 16 Eluent Bottle - Connected
46
Eluent Degasser
47
Figure 17 Eluent Degasser
47
Low Pressure Gradient
48
Figure 19 Connecting Mixing Coil for Low Pressure Gradients
50
Figure 20 Connecting Eluent Connection Tubings
51
High Pressure Pump
52
Capillary Connections High Pressure Pump/Purge Valve
52
Figure 21 Capillary Connections High Pressure Pump/Purge Valve
52
Connecting Low Pressure Gradient
53
Deaerating the High Pressure Pump
54
Figure 22 Mixing Coil for Low Pressure Gradients Connection
54
Figure 23 Deaerating the High Pressure Pump
55
Inline Filter
56
Pulsation Damper
57
Figure 24 Connecting Inline Filter
57
Sample Degasser
58
Figure 25 Pulsation Damper - Connection
58
Injection Valve
60
Connecting the Injection Valve
60
Figure 27 Injection Valve - Connected
60
Mode of Operation of the Injection Valve
61
Figure 28 Injection Valve - Positions
61
Selecting the Sample Loop
62
Column Thermostat
62
High Capacity Metrohm Suppressor Module
65
(Msm-Hc)
65
General Information on the MSM-HC
65
Connecting the MSM-HC
65
Figure 30 MSM-HC - Connectors
66
Peristaltic Pump
68
Principle of the Peristaltic Pump
68
Figure 31 Peristaltic Pump
68
Installing the Peristaltic Pump
69
Figure 32 Installing the Pump Tubing
69
Figure 33 Install Pump Tubing Connection with Filter
70
Figure 34 Install Pump Tubing Connection Without Filter
71
Metrohm CO Suppressor (MCS)
73
General Information on the MCS
73
Connecting MCS
73
Figure 35 MCS - Connection
73
Installing the Adsorption Cartridges
74
Figure 36 Adsorption Cartridge Holder
75
Conductivity Detector
76
Figure 37 Conductivity Detector Front
77
Figure 38 Conductivity Detector Rear
78
Connecting the Instrument
79
Connecting the Instrument to the PC
79
Connecting the Instrument to Mains Supply
79
Figure 39 Connection Detector - MCS
79
Guard Column
80
Separation Column
82
4 Start-Up
84
Initial Start-Up
84
Conditioning
85
5 Operation and Maintenance
87
General Information
87
Care
87
Maintenance by Metrohm Service
87
Operation
88
Shutting down
88
Capillary Connections
88
Door
89
Eluent
89
Production
89
Operation
90
High Pressure Pump
90
Protection
90
Maintenance
91
Figure 40 Removing Piston
92
Figure 41 Components of the Piston Cartridge
93
Figure 42 Tool for Piston Seal 6.2617.010
94
Figure 43 Removing the Piston Seal
95
Figure 44 Inserting the Piston Seal into the Tool
95
Figure 45 Inserting the Piston Seal into the Pump Head
96
Figure 46 Removing Valves
97
Figure 47 Dismantling Valve
98
Figure 48 Components of the Inlet Valve and Outlet Valve
99
Inline Filter
101
Maintenance
101
Figure 49 Changing the Filter
101
Inline Sample Preparation
103
Rinsing the Sample Path
103
Sample Degasser
105
Operation
105
Injection Valve
105
Protection
105
High Capacity Metrohm Suppressor Module (MSM-HC)
105
Maintenance
106
Figure 50 MSM-HC - Components
108
Peristaltic Pump
111
Operation
111
Maintenance
112
Figure 51 Pump Tubing Connection - Changing the Filter
113
Replacing the CO 2 Adsorption Cartridge
114
Regenerating the H O Adsorption Cartridge
114
Conductivity Detector
115
Maintenance
115
Separation Column
115
Separating Efficiency
115
Protection
116
Storage
116
Regeneration
116
Quality Management and Validation with Metrohm
117
6 Troubleshooting
118
Problems and Their Solutions
118
7 Technical Specifications
123
Reference Conditions
123
Instrument
123
Leak Sensor
123
Ambient Conditions
123
Housing
124
Eluent Degasser
124
Low Pressure Gradient
124
High Pressure Pump
125
7.9 Sample Degasser
126
Injection Valve
126
Column Thermostat
126
High Capacity Metrohm Suppressor Module (MSM-HC)
127
Peristaltic Pump
127
Conductivity Measuring System
128
Mains Connection
129
Interfaces
129
7.18 Safety Specification
130
Electromagnetic Compatibility (EMC)
130
Weight
130
8 Conformity and Warranty
131
Declaration of Conformity
131
Quality Management Principles
132
Warranty (Guarantee)
133
9 Accessories
135
Scope of Delivery
135
Optional Accessories
146
Index
148
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