LAR Process Analysers QuickTOC ultra Manuals

Manuals and User Guides for LAR Process Analysers QuickTOC ultra. We have 1 LAR Process Analysers QuickTOC ultra manual available for free PDF download: Instruction Manual

LAR Process Analysers QuickTOC ultra Instruction Manual (297 pages)

Brand: LAR Process Analysers | Category: Measuring Instruments | Size: 14 MB

Table of Contents
3
Certificates
11
General Information
15
Safety Notes
15
Safety Symbols
16
Warning Sign on Casings with Explosion Protection
17
Operating Principle of the Analyser
19
The Sum Parameter TOC
19
High Temperature Method at 1,200°C
20
High Temperature Method Vs. Wet Chemical Method
20
The Measurement Principle of the TOC-Difference Method
20
Proceeding
21
Advantages
21
The Measurement Principle of the TOC-Direct Method (NPOC-Method)
21
Proceeding
22
Advantages
22
The Measurement Principle of the Tconly Method
22
2.7 Measurement and Working Ranges of the Quicktoc®Ultra
24
Explosion Protection
25
Product
27
Scope of Delivery
27
Identification Plate
28
Construction of the Analyser
29
Front View of the Analyser
29
Right-Hand Side View of the Analyser
31
Components of the Analyser
31
Pump System
31
Tube Cassette Pump
33
Tubes (for the Tube Cassette Pump)
33
Sample Pump
34
Glass Components
35
Ceramic Furnace
37
Explosion Protection Components
38
Overpressure System
38
Cooling and Emergency Cooling
39
Components of the Ex-Protection
40
Overpressure System
40
Cooling and Emergency Cooling
41
Connections
45
Mains Connection
47
Electronic Connections (Digital and Analog Connections)
48
Connections on the TRC-Board
48
RS232 Serial Interface
50
Digital Input
50
Relays
51
Analog Outputs
51
Carrier Gas
55
Installation
57
Installation Process
57
Installation of the Analyser
57
Installation of Optional Accessories
58
Site Selection - Ambient Conditions
60
Mounting and Installation of the Analyser On-Site
61
Maximum Swing Open of the Housing
62
Wall Mounting
63
Carrier Gas
64
Sample Inlet and Drain
64
Power Supply
64
Signal Connections
64
Rinsing Water
65
Provide Acid Solution (TOC-Direct and TOC-Difference Method)
65
Provide Calibration Standards
66
Start-Up
67
Procedure
67
Start-Up of the Analyser
67
Start-Up of Options
67
Checking the Pre-Fusing
69
Checking the Installation Plate
69
Remove Transportation Locks
69
Furnace Transport Screw
70
Transport Lock of the XY-System
71
Voltage Alignment
72
Fuses Switch-On
72
Reactor Pipe Filling and Installation
73
Completion of the Furnace
75
Installation of Glass Components
77
Installation of the Pump Tubes
78
Installation of the Tubes into the Tube Cassette Pump
78
Installation of the Tubes into the Sample Pump
78
Analyser Tubing
80
Electrical Connection of the Control Unit and the Relays
80
Emergency Shutdown
81
Restart after Emergency Shutodown
82
Connection of the Emergency Cooling for the Furnace
82
Switch on the Analyser
83
Setting the Bypass of the Control Unit
84
Perform a Test-Run
86
Rinse the Injection System und Sample Tubes
86
Costumisation of Application-Specific Settings
86
Checking Status Parameters
86
Perform a Calibration
87
Reagents and Calibration Standards
89
Reagents
89
Deionised Water for Calibration Standards
89
Rinsing Water
89
Phosphoric Acid (H3PO4) for TOC-Difference Method
90
Hydrochloric Acid (Hcl) for TOC-Direct Method (NPOC-Method)
90
Cleaning Solution for Glass Components
91
Calibration Standards
92
Calibration Standards - TOC-Difference Method
92
Stock Solution - TOC-Difference Method
93
Dilution of the Stock Solution - TOC-Difference Method
94
Calibration Standards - TOC-Direct Method / Tconly Method
95
Stock Solution - TOC-Direct Method / Tconly Method
95
Dilution of the Stock Solution - TOC-Direct Method / Tconly Method
96
How to Work with the Analyser
97
General
97
User Level
97
User Interface
98
Status Bar
98
User Level Navigation Bar
99
Control Bar
99
Main View
100
Keyboard
100
Registration
101
Operating Status
101
Home Screen
102
Reading Screen
103
Channel Selection
104
Daily Variation
105
Single View
106
Status Screen
107
Waveform
109
Measurement Settings
110
Measurement Parameters
111
Measurement Interval
114
Measuring Channel Settings
115
Channel Settings
116
Relays
118
Setting a Custom Relay
119
Programming Tools (Logical Links)
120
Testing the Relays
120
Sample Stream Settings (Only User Level 3)
121
Sensor Settings
122
Sensors
123
Threshold and Integration
124
Service
125
Service Parameters
126
Service Actions
128
Test Run
130
Positioning / Adjustment of the Injection Positions (Only User Level 3)
132
PC Settings
133
Calibrate Analog Outputs
134
Quick Test (Analog Outputs)
134
Live-Zero-Feature
135
Multi I/O
136
Digital in
137
Digital out (Only User Level 3)
138
Single Measurement
139
Settings
140
Archive
141
Single Measurement - Single View
141
Calibration
143
Calibration Settings
145
7.10.1.1 Calibration Archive
147
7.10.1.2 Calibration Archive - Calibration Points (Parameter) - Info
148
7.10.1.3 Calibration Archive - Calibration Points (Parameters) - Calibration Graph
148
7.10.1.4 Calibration Archive - Calibration Points (Parameters) - Waveform
150
Carrying out the Calibration - Info
151
Carrying out the Calibration - Graph
152
Calibration Parameter Settings (User Level 3)
153
Performing a Pre-Set Two-Point Calibration (User Level 2)
154
Carrying out a Two-Point Calibration (User Level 3 Only)
154
Performing a Multi-Point Calibration (User Level 3 Only)
155
Auto-Calibration (Only User Level 3)
156
Database
157
Table of Measured Values
158
Single View of the Measured Value (Info)
159
Single View of the Channel
160
Logbook
161
Fault Message View
162
Activity Overview
163
Update Manager
164
Additional Functions
165
Zoom
165
Export
166
Status Recognition
167
Status Codes
167
Fault Codes
168
7.15.2.1 Yellow Fault Codes
168
7.15.2.2 Red Fault Codes
169
Care and Maintenance
171
Overview of Regular Care and Maintenance Actions
172
Visual Inspections
173
Performing the Visual Inspections
174
Zero Signal (Weekly)
174
Carrier Gas (Weekly)
174
Injection System (Weekly)
175
Injection Needle (Weekly)
176
Glass Components (Weekly)
176
Canister and Supply Tubes (Weekly)
176
Inlet and Drain Tubes (Weekly)
176
Injection Tube (3 Months)
177
TIC-Stripping Vessel (3 Months)
178
Running Rails (XY-System) (3 Months)
179
Tube Cassette Pump and Pump Tubes (3 Months)
179
Sample Pump and Pump Tubes (3 Months)
179
Viton Tubes (3 Months)
179
Acid Trap (3 Months)
179
Quartz Wool Filter (3 Months)
180
Care Actions
181
Perform Care Actions
182
Rinse the Injection System
182
Clean Glass Components
182
Fill Canisters
182
Clean Canisters
183
Clean Supply Tubes
183
Clean Inlet and Drain Tubes
183
Clean Teflon Tube (Reactor Foot)
183
Clean the Reactor Foot
184
Clean Injection Tube
184
Cleaning the Reactor Pipe
185
Clean TIC Stripping Vessel
186
Clean Gas Cooling Pipe
186
Clean Running Rails (XY-System)
186
Grease Running Rails (XY-System)
187
Cleantube Cassette Pump and Pump Cassettes
187
Clean Sample Pump
188
Adjust Sample Pump
188
Clean Viton Tube
189
Clean Injection Needle
189
Renew Calibration Standard
189
Clean Needle Guide (Injection Port)
189
Furnace System Check
190
Check the Gas Cooling Pipes
191
Clean and Oil Injection Port
192
Move Pump Tubes (Tube Cassette Pump)
193
Check the Mechanical Backlash of the XY-System
193
Check the Injection Port
194
Maintenance Actions
195
Perform Maintenance Actions
196
Replace Supply Tubes
196
Replace Inlet and Drain Tubes
196
Replace Teflon Tube (Reactor Foot)
196
Replace Reactor Pipe Filling / Reactor Pipe
197
Replace Small Furnace Head Seal
199
Replace Big Furnace Head Seal (Silicone O-Ring with PFA Coat)
200
Replace Injection Tube
200
Replace Viton Tube
200
Replace Acid Trap Filling
201
Replace Acid Trap
201
Replace Quartz Wool Filter Filling
202
Replace Quartz Wool Filter
202
Replace Injection Needle
203
Replace Silicone Seal for TIC-Port (TOC-Difference Method)
203
Replace Needle Guide Seal (Injection Port)
204
Replace Silicone Seals for Glass Components
204
Replace Reactor Foot Seal
205
Replace Pump Tube (Tube Cassette Pump)
206
Replace Pump Tube (Sample Pump)
207
Replace Gas Filter
207
8.8 Function Tests
208
Check Analyser Status
209
Tightness Test
210
Test Run (XY-System)
210
Checking the Measurement Results
210
Checking the Measurement Process
210
Short-Time- and Long-Time Interruptions
211
Switching On/Off for Short-Time-Interruptions (<1 Week)
211
Switching On/Off for Long-Time Interruptions (>1 Week)
211
Accessories and Options
216
Overview
216
Reagent Cabinet
217
Construction of the Reagent Cabinet
217
Installation of the Reagent Cabinet
218
Start-Up of the Reagent Cabinet
219
Activated Carbon
219
Soda Lime Pellets with Indicator
220
The Carrier Gas for the Measurements Must Meet Certain Criteria (). Ambient Air Must be Conditioned Accordingly if Used. the Tubing for the Ambient Air Preparation Unit Is Shown below
221
Use the Holes Q1 and Q2 of the Mounting Rack and the Air Preparation Brackets
221
This Prevents Consumption of Soda Lime Cookies with Indicator
221
Maintenance
222
Perform Visual Inspection
223
Once All Test Criteria Are Met, Proceed with the Next Stepsoda Lime
223
Tube Connections
223
Pre Pressure of the Carrier Gas
223
Perform Care and Maintenance Actions (Ambient Air Preparation Unit)
224
Replace Soda Lime
224
Replace Gas Filter
225
Replace Filter Mats
227
Replace Fine Filter Unit
227
Replace Coarse Filter Unit
228
Replace Activated Carbon
228
9.3 Proceed Analogously to the Replacement of the Soda Lime in Chapter 9.2.7.1 From Page 213Flowsampler
231
Flowsampler® DN25
231
Flowsampler® DN17
231
Installation of the Flowsampler
232
Start-Up of the Flowsampler
232
Care and Maintenance Actions (Flowsampler®)
233
Perform Visual Inspections (Flowsampler®)
234
Flow
234
Sampling Pipe (Needle)
234
Perform Care and Maintenance Actions (Flowsampler®)
235
Clean Sampling Pipe (Needle)
235
Clean Flowsampler
235
Overflow Sampler
236
Construction of the Overflow Sampler
236
Connections
236
Set-Up
237
Care and Maintenance (Overflow Sampler)
238
Perform Visual Inspection (Overflow Sampler)
239
Flow
239
Perform Care and Maintenance (Overflow Sampler)
239
Clean Overflow Sampler
240
CO2-Remover
241
Start-Up of the CO2-Remover
243
Care and Maintenance Actions (CO2-Remover)
244
Perform Visual Inspections (CO2-Remover)
245
Housing
245
Service Lamp
245
Mounting Rack
246
Trackball
248
Multi Stream Option
249
Multi Parameter Option
250
High Salt Option
251
Auto-TIC-Port
252
Construction of the TIC Reactor with Auto-TIC-Port
252
Start-Up of the TIC Reactor with Auto-TIC-Port
252
Care and Maintenance Actions (Auto-TIC-Port)
253
Perform Visual Inspections (Auto-TIC-Port)
254
Microswitch on Auto-TIC-Port (6 Months)
254
Perform Care and Maintenance Actions (Auto-TIC-Port)
255
Replace Needle Guide Seal (Auto-TIC-Port) (1 Month)
255
Clean Needle Guide (Auto-TIC-Port) (1 Month)
256
Clean and Oil Auto-TIC-Port (3 Months)
257
Internal Sample Dilution
258
Software Settings for the Internal Sample Dilution
258
Flow Diagram with Internal Sample Dilution
259
Minor Disruptions - Quickly Solved
260
Preconditions for Fault-Free Measurement Mode
260
Breakdowns
261
Check the Fuses - Automatic Circuit Breaker
262
Breakdowns of the Temperature Regulators
263
Technical Information
264
Device Specifications
264
Ambient Conditions
265
Specifications for Accessories and Options
265
Flow Diagrams
266
Component Labelling
266
TOC-Difference Method (1 Sample Stream)
268
TOC-Difference Method (3 Sample Streams)
269
TOC- Direct Method (1 Sample Stream)
270
TOC-Direct Method (2 Sample Streams)
271
Tconly-Method (1 Sample Stream)
272
Tconly-Method (2 Sample Streams)
273
Flow Diagram with Internal Sample Diluition (Option)
274
Operating, Care and Maintenance Logs
276
Operating Log
277
Visual Inspections Log (Analyser)
278
Care Log (Analyser)
279
Maintenance Log (Analyser)
280
Function Test Log (Analyser)
281
Visual Inspection Log (Ambient Air Preparation Unit)
282
Care and Maintenance Log (Ambient Air Preparation Unit)
283
Visual Inspection Log (Flowsampler)
284
Care and Maintenance Log (Flowsampler)
285
Care and Maintenance Log (Overflow Sampler)
286
Visual Inspection Log (CO2-Remover)
287
Care and Maintenance Log (CO2-Remover)
288
Visual Inspection Log (Auto-TIC-Port)
289
Care and Maintenance Log (Auto-TIC-Port)
290
Safety Data Sheets
292
Contact
294
Contact to LAR
294
Distributors / Authorized Service Partners
294
Optimization
294

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LAR Process Analysers QuickTOC ultra Instruction Manual (297 pages)

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