Knauer Azura DAD 6.1L Detector Manuals

Manuals and User Guides for Knauer Azura DAD 6.1L Detector. We have 2 Knauer Azura DAD 6.1L Detector manuals available for free PDF download: User Manual, Instructions Manual

Knauer Azura DAD 6.1L User Manual

Knauer Azura DAD 6.1L User Manual (150 pages)

Detector

Brand: Knauer | Category: Analytical Instruments | Size: 6 MB

Table of Contents

English

2
- Table of Contents
  2
- Intended Use
  
  5
  - Device Overview
    5
    
    Front View
    5
    
    Rear View
    5
    
    Side View
    6
  - Features
    6
  - Solvents
    8
- Scope of Delivery
  
  10
- Safety for Users
  
  11
  - Definition of Personal and Material Damage
    13
  - Decontamination
    13
- Symbols and Signs
  
  14
- Installation
  
  15
  - Contact Data
    15
  - Transport
    15
    
    Installation Site and Space Requirements
    15
  - Operating Environment
    16
    
    Space Requirements
    16
  - Setup
    16
    
    Unpacking
    16
  - Inserting the Flow Cell
    17
    
    Inserting the Flow Cell with Fiber Optics
    18
  - Connecting the Capillaries
    19
    
    Using PEEK Fittings
    19
  - Connecting the Leak Management
    20
  - Control
    21
    
    Connecting the Device to the Computer
    22
    
    Configuring the LAN Settings
    22
    
    Connecting the Cables
    23
    
    Configuring the Router
    23
    
    Integrating the LAN into a Company Network
    24
    
    Controlling Several Systems Separately in a LAN
    24
    
    Pin Header Connectors
    24
    
    Wiring the Pin Header
    27
    
    Integrator Connector
    28
  - Power Supply
    28
  - Integrating the Detector into a System
    29
    
    Pre-Installed Capillaries
    29
- Operation
  
  30
  - Initial Start-Up
    30
  - Switch-On
    30
  - Control
    31
    
    Operation with Chromatography Software
    31
    
    Control with Control Unit
    31
    
    Control with Mobile Control
    31
  - Meaning of the Leds
    32
  - Re-Setting the Device
    33
- Optimizing the Detector
  
  34
  - Location
    34
  - Warm-Up Time
    34
  - Selecting the Flow Cell
    34
    
    Flow Cell Volume
    34
    
    Path Length
    35
    
    Material
    36
    
    Pressure Stability
    36
    
    Connection
    36
    
    Remote Operation (Fiber Optics)
    36
    
    Selecting the Wavelength
    37
    
    Bandwidth
    37
    
    Spectral Range
    38
    
    Time Constant and Data Rate
    38
    
    Integration Time
    40
    
    Subtraction of the Baseline Chromatogram
    40
    
    General
    40
- Functionality Tests
  
  41
  - Installation Qualification (IQ)
    41
  - Operation Qualification (OQ)
    41
- Troubleshooting
  
  42
  - Lan
    42
  - Possible Problems and Solutions
    43
  - System Messages
    43
- Maintenance and Care
  
  48
  - Contact the Technical Support
    49
  - Maintenance Contract
    49
  - Maintenance Intervals
    49
  - Cleaning and Caring for the Device
    49
  - Checking the Fittings
    50
  - Putting the Device out of Operation
    50
  - Storage
    50
    
    Disconnect from Power Supply
    51
  - Cleaning the Flow Cell
    51
    
    Rinsing the Flow Cell
    51
  - Replacing the Flow Cell
    51
  - Replacing the Lamp
    52
    
    Removing the Deuterium or Halogen Lamp
    52
    
    Installing the Deuterium or Halogen Lamp
    54
  - Removing a Leak
    55
- Technical Data
  
  56
  - Dad 6.1L
    56
  - Dad 2.1L
    57
  - Mwd 2.1L
    58
  - Conditions for Specifications
    60
- Disposal
  
  61
- Legal Information
  
  62
  - Warranty Conditions
    62
  - Transport Damage
    62
- HPLC Glossary
  
  63
- Repeat Orders
  
  66
  - Modules
    66
  - Accessories and Spare Parts
    66
    
    Flow Cells
    67
    
    Flow Cells with Fiber Optics Connectors
    67
    
    Fiber Optics
    68
- Table of Figures
  
  69
- Index
  
  70
Deutsch

74
- Bestimmungsgemäße Verwendung
  
  77
  - Geräteübersicht
    77
    
    Vorderansicht
    77
    
    Rückansicht
    77
  - Abb. 1 Vorderansicht (Beispiel DAD 6.1L)
    77
    
    Seitenansicht
    78
  - Leistungsübersicht
    78
  - Abb. 2 Rückansicht (Beispiel DAD 6.1L)
    78
  - Abb. 3 USB-Anschluss für die Control Unit
    78
  - Abb. 4 Optisches System DAD 6.1L
    79
  - Eluenten
    80
- Lieferumfang
  
  82
- Sicherheit für Anwender
  
  83
  - Definition Möglicher Personen- oder Sachschäden
    85
  - Dekontamination
    85
- Symbole und Kennzeichen
  
  86
- Installation
  
  87
- Betrieb
  
  103
  - Erstinbetriebnahme
    103
  - Einschalten
    103
  - Abb. 22: Netzschalter mit Netzanschluss auf der Geräterückseite
    103
  - Bedienung
    104
    
    Bedienung mit Chromatografie-Software
    104
    
    Bedienung mit Control Unit
    104
    
    Bedienung mit Mobile Control
    104
  - Bedeutung der Leds
    105
  - Abb. 23: Leds und Schalter/Standby-Taste an der Vorderseite des Geräts
    105
  - Gerät Zurücksetzen
    106
- Detektor Optimieren
  
  107
  - Einsatzort
    107
  - Aufwärmzeit
    107
  - Durchflusszelle Auswählen
    107
  - Abb. 24 Temperaturprofil nach Kaltstart
    107
    
    Volumen der Durchflusszelle
    108
    
    Schichtdicke
    108
  - Abb. 25 Vergleich des Volumens
    108
  - Abb. 26 Lambert-Beersches Gesetz
    108
    
    Material
    109
    
    Druckstabilität
    109
    
    Verbindungsart
    109
  - Abb. 27 Vergleich der Schichtdicke
    109
    
    Remote-Betrieb (LWL)
    110
    
    Wellenlänge Auswählen
    110
  - Abb. 28 Vergleich mit und ohne Referenzwellenlänge
    110
    
    Bandbreite
    111
    
    Spektralbereich
    111
    
    Zeitkonstante & Datenrate
    111
  - Abb. 29 Bandbreite
    111
    
    Integrationszeit
    113
    
    Basislinie Subtrahieren
    113
    
    Sonstiges
    113
  - Abb. 30 Rauschen bei Unterschiedlichen Datenraten
    113
- Funktionstests
  
  115
  - Installation Qualification (IQ)
    115
  - Operation Qualification (OQ)
    115
- Fehlerbehebung
  
  116
  - Lan
    116
  - Mögliche Probleme und Abhilfen
    117
  - Systemmeldungen
    118
- Wartung und Pflege
  
  123
  - Kontakt zur Technischen Kundenbetreuung
    124
  - Wartungsvertrag
    124
  - Wartungsintervalle
    124
  - Gerät Reinigen und Pflegen
    124
  - Verschraubungen Kontrollieren
    125
  - Außer Betrieb Setzen
    125
  - Lagerung
    125
    
    Stromanschluss Trennen
    126
  - Durchflusszelle Reinigen
    126
    
    Durchflusszelle Spülen
    126
  - Abb. 31 Durchflusszelle Entriegeln
    127
  - Abb. 32 Übersicht zur Deuterium- und Halogenlampe
    128
  - Abb. 33 Lampenklappe
    129
  - Abb. 34: Arretierungsring des Lampensteckers
    129
  - Abb. 35: Schrauben am Lampensockel
    129
  - Abb. 36: Lampentopf der D2-Lampe
    130
  - Abb. 37: Lampentopf der Halogenlampe
    130
  - Abb. 38: Deuteriumlampe Anschrauben
    130
  - Abb. 39: Lampenklappe
    130

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Knauer Azura DAD 6.1L Instructions Manual

Knauer Azura DAD 6.1L Instructions Manual (81 pages)

Detector

Brand: Knauer | Category: Laboratory Equipment | Size: 2 MB

Table of Contents

Table of Contents
3
1 General

7
- About These Instructions
  7
- Signal Words
  7
- Additional Typographical Conventions
  7
- Legal Information
  8
  - Liability Limitation
    8
  - Transport Damage
    8
  - Warranty Conditions
    8
  - Warranty Seal
    8
  - Declaration of Conformity
    8
2 Basic Safety Instructions

9
- Intended Use
  9
  - Operating Ranges
    9
  - Foreseeable Misuse
    9
- User Qualification
  9
- Operator Responsibility
  10
- Personal Safety Equipment
  10
- Safety Features on the Device
  10
- Working with Solvents
  11
- Specific Environments
  12
  - Earthqake-Endangered Areas
    12
  - Explosive Environment
    12
  - Cooling Room
    12
- Maintenance, Care and Repair
  12
- Service Request Form and Decontamination Report
  12
3 Product Information

13
- Features
  13
- Scope of Delivery
  13
- Views
  13
- Performance Overview
  14
- Symbols and Signs
  16
4 Installation and Initial Startup

17
5 Operation

35
- Initial Startup
  35
- Switch on
  35
- Software Operation
  36
  - Control Methods
    36
  - Operating with Mobile Control
    36
- Meaning of the Leds
  36
- Default Settings
  37
- Glp
  38
6 Optimizing the Detector

40
- General
  40
- Selecting the Flow Cell
  40
- Selecting the Wavelength
  43
  - Bandwidth
    43
- Spectral Range
  44
- Time Constant & Data Rate
  44
- Integration Time
  45
- Subtraction of the Baseline Chromatogram
  46
  - Extended Linear Range
    46
7 Functionality Tests

47
- Installation Qualification (IQ)
  47
- Operation Qualification (OQ)
  47
8 Troubleshooting

48
- Lan
  48
- Possible Problems and Solutions
  49
- System Messages
  50
9 Maintenance and Care

53
- General
  53
- Cleaning and Caring for the Device
  54
  - Handling the Flow Cell Cartridge
    54
  - Surfaces
    55
- Cleaning the Flow Cell
  55
- Replacing the Flow Cell
  58
- Replacing the Lamps
  59
  - Removing the Deuterium or Halogen Lamp
    60
  - Installing the Deuterium or Halogen Lamp
    61
- Checking the Fittings
  62
- Removing a Leak
  62
- Removing a Leakage
  62
- Decommissioning
  63
10 Transport and Storage

64
- Taking the Device out of Operation
  64
- Packing the Device
  64
- Transporting the Device
  64
- Storing the Device
  64
11 Disposal

65
12 Technical Data

66
- Dad 6.1L
  66
- Dad 2.1L
  67
- Mwd 2.1L
  68
- Conditions for Specification
  70
13 Reorders

70
- Devices and Accessories
  70
- Flow Cells
  71
- Flow Cells with Fiber Optics
  72
- Fiber Optic Cables
  74
14 Chemical Compatibility of Wetted Materials

75
- General
  75
- Plastics
  75
- Non-Metals
  77
- Metals
  78
15 Index

79

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