GBC SavantAA S Manuals

Manuals and User Guides for GBC SavantAA S. We have 1 GBC SavantAA S manual available for free PDF download: Operation Manual

GBC SavantAA S Operation Manual (102 pages)

Atomic Absorption Spectrometer

Brand: GBC | Category: Measuring Instruments | Size: 3 MB

Table of Contents
3
Table of Contents
4
About this Manual
9
Introduction
9
For Your Safety
9
Instrument Installation
9
Software Overview
9
Installing and Optimising Lamps
9
Flame Atomisation System
9
Flame Auto Sampler and Flame Analysis Tutorial
9
Graphite Furnace (System 5000) and Furnace Analysis Tutorial
10
Maintenance
10
Using this Manual
10
If You Are a First Time AA User
10
If You Are Unfamiliar with the Windows® Platform
10
If You Are an Experienced AA and Windows® User
10
Introduction
11
Equipment Overview
12
Savantaa Model Range
12
Savantaa Model Configurations
12
Savantaa Accessories
12
System 5000 Graphite Furnace
13
SDS720 X-Y-Z Auto Sampler
13
PS720 Auto Dilutor
13
HG3000 Hydride Generator
13
MC3000 Mercury Concentrator
13
Other Accessories
14
For Your Safety
15
Intended Use of the Instrument
16
Instrument Positioning
16
Safety Signs
16
Warning
16
Electrical Hazard
16
Electrical Hazards
16
Fuse Replacement
16
High Voltages
16
Earthing Requirement
17
Gaseous Emissions
17
Gas Cylinders and Lines
17
Acetylene
18
Air
18
Radiation
18
Waste Container
18
Flammable Samples
19
Liquid Trap
19
Instrument Installation
21
Introduction
22
Controls
22
Site Preparation
22
Operating Environment
22
Location
23
Exhaust Requirements
24
Power Requirements
24
Gas Requirements
24
Acceptable Instrument Inlet Pressure Ranges
25
Unpacking Instructions
25
Connections
26
Installing Specific Components
27
Savantaa Software
29
Introduction
30
Software Definitions
30
Software Conventions
30
Installing the Software
31
Selecting the Hardware Setup
32
The Software Modules
34
File Saving
34
Method
34
Samples
34
Analysis
35
Results
36
Report
37
Instrument
38
On-Line Help System
38
On-Line Help Conventions
39
Searching On-Line Help
39
Installing and Optimising Lamps
43
Installing Lamps
44
Additional Lamps
46
Super Lamps
46
Optimising Lamps
47
Super Lamp Optimisation
47
Super Lamp Operating Hints
47
Deuterium Lamps
48
Flame Atomisation System
51
Savantaa Flame Atomisation System with Automatic Burner Rotation
52
Liquid Trap/Spray Chamber
53
Setting up the Liquid Trap
53
Filling the Liquid Trap
54
Use of Organic and Aqueous Solvents
54
Emptying the Liquid Trap
54
Spray Chamber/Liquid Trap Removal/Replacement
54
Burners
56
Burner Removal and Insertion
56
Burner Cleaning
57
Savantaa Power-Up Procedure
57
Optimising the Burner Position
58
Motorised Vertical Only Movement Burner (MVOM) Option
59
Programmable Flame Control
60
Safety Interlocks
60
Gasbox Status
61
Interlock Status
62
Last Shutdown
63
Pre-Ignition Checklist
63
Igniting the Burner Flame
64
Extinguishing the Flame
64
Gas Flow Optimisation for Programmable Flame Control
64
Optimising Gas Flow Rates
64
Nebuliser Optimisation
65
Impact Bead
65
Optimising the Burner Angle
66
Automatic Burner Rotation (ABR) - Optional
66
Description
66
Referencing
66
Optimising the Zero Position for Normal Samples
66
Optimising the Burner Angle for Over-Range Samples
67
Sds720 Auto Sampler
69
Description
70
SDS720 Auto Sampler Installation
70
Aspiration Tube
71
SDS720 Auto Sampler Rack Loading
71
Maintenance
71
Flame Analysis Tutorial
73
Lamp Selection
74
Method Development
76
Performing an Analysis
79
Generating a Report
79
Graphite Furnace (System 5000) Installation
81
GF5000 Controls
82
Installation
82
Location
82
Power Requirements
82
Gas Requirements
82
Water Requirements
83
Unpacking
83
Connections
83
Optimisation of Light Paths
83
Workhead Installation
84
Optimising the Furnace Workhead Position
84
PAL Furnace Auto Sampler
85
Unpacking
85
Connections
85
GF5000 Power up
86
Setting the Probe Tip Position
86
Furnace Analysis Tutorial
89
Instrument Configuration
90
Lamp Installation
91
Installing Other Lamps
91
Deuterium Lamp Alignment
92
Workhead Installation
92
Method Development
92
Performing an Analysis
95
Generating a Report
95
Maintenance
97
Optics
98
Deuterium Lamp Removal/Replacement
98
Flame System
98
Bleeding Gas Lines
98
Nebuliser Removal/Replacement
98
Impact Bead Adjustment
99
Nitrous Oxide-Acetylene Burner Cleaning
100
Graphite Furnace
100
Furnace Tube Removal/Replacement
100
PAL Auto Sampler
101
Syringe Removal/Replacement
101
Syringe Trouble-Shooting
102

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GBC SavantAA S Operation Manual (102 pages)

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