ESA Corona CAD Manuals

ESA Corona CAD Manuals

Manuals and User Guides for ESA Corona CAD. We have 1 ESA Corona CAD manual available for free PDF download: Operating And Maintenance Manual

ESA Corona CAD Operating And Maintenance Manual

ESA Corona CAD Operating And Maintenance Manual (190 pages)

Brand: ESA | Category: Security Sensors | Size: 2 MB

Table of Contents

Safety/Operating Symbols

5
Warnings and Safety Precautions

6
Important Operating Considerations

10
Do's and Don'ts

13
- Table of Contents
  15
Chapter 1: Introduction

21
Chapter 2 Installation

35
- Introduction
  35
- Environmental Conditions
  35
  - Physical Location of the Corona Detector
    35
  - Power Requirements
    37
  - Space Requirements
    38
  - Nebulization Gas
    39
- Unpacking the Detector
  39
- Installing the Detector
  40
  - Basic Installation
    40
    
    Locating the Detector
    40
    
    Power Source
    41
    
    Gas Source
    42
    
    Exhaust
    43
    
    Drain and Vent Installation
    43
    
    HPLC System
    47
    
    USB Connections
    49
    
    Other Connections
    49
    
    Setting up Corona Plus Nebulizer Heater
    49
- Test Protocol
  50
  - Role of the Test Protocol
    50
  - Setup
    50
  - Protocol
    51
- ESA Biosciences Corona CAD Detector Test Worksheet
  54
- General Operations
  55
- Other Detector Configurations
  56
  - Using the Corona in Parallel with Another Detector
    56
- Setting up the Thermal Organizer
  57
- Making Electrical Connections
  58
- Mobile Phase Formulation
  63
  - Supplies
    63
  - Procedure
    63
    
    Mobile Phase Preparation
    63
  - Degassing Mobile Phase
    64
  - Wrap up
    66
  - Mobile Phase Qualification
    66
- Column Conditioning Procedure
  67
  - Supplies
    67
  - Procedure
    67
Chapter 3: The Corona Cad Firmware

69
- Introduction
  69
- Initialization of the Detector
  70
- The Keypad
  72
- Creating/Editing a Corona CAD Detector Method
  73
  - Overview
    73
  - Edit the Method Select Screen
    73
  - Edit the Security Screen
    74
  - Edit the Parameters Screen
    75
  - Creating/Editing a CAD + TL Method
    76
    
    Timeline Screen
    76
    
    End Event Screen
    78
    
    Set Contact Screen
    78
    
    Autozero Screen
    79
    
    Filter Screen
    79
    
    Marker Screen
    79
    
    Range Screen
    80
    
    Gas Screen
    80
    
    Hold Screen
    80
    
    Loop Screen
    81
    
    Reset Screen
    81
  - Save Method Screen
    81
  - Method # Zero
    82
- Using a Method to Collect Data
  83
  - The System Screens
    86
    
    Role of the System Screens
    86
    
    RS232 Setup Screen
    86
    
    Deleting Methods Screen
    87
    
    Event Marks Screen
    88
    
    Date & Time Setup Screen
    89
    
    Remote Screen
    89
    
    Inputs Screen
    90
    
    Contacts Screen
    91
    
    Thermal Organizer Setup Screen
    92
    
    Self Test Screen
    93
    
    Nebulizer Heater Setup Screen
    93
  - How to Create a Timeline Method
    95
Chapter 4: Using the Detector in a Hplc System

97
- Introduction
  97
- Operating the Corona Detector
  97
- Mobile Phase Considerations
  100
- Column Considerations
  100
- Sample Considerations
  101
- Maximizing the Performance of the Assay
  102
  - Overview
    102
  - Selection of the Proper Output Range
    102
  - Setting the Filter
    102
- An Experiment to Ensure that the Chromatograph and the Detector Are Functioning Properly
  103
- Analysis of Data
  105
- Effects of Gradient Elution on Response
  107
Chapter 5 Maintenance and Troubleshooting

109
- Introduction
  109
- Detector Maintenance
  110
  - Overview
    110
  - Daily Maintenance
    111
  - Weekly Maintenance
    111
  - Monthly Maintenance
    112
  - Quarterly Maintenance
    112
  - Additional Periodic Maintenance
    112
  - Nitrogen Generator
    113
- Customer Service of the Detector
  113
  - In-Line Filter Elements
    113
    
    Frequency of Changing Filter Elements
    113
    
    Checking the Pressure Drop Across the Filter
    114
    
    Changing a Filter
    114
- Changing the Line Fuses
  115
- Replacing the Gas Filters
  116
- Cleaning the Detector
  117
  - Cleaning the Corona Detector Unit
    117
  - Cleaning the Corona Detector Organizer and Thermal Organizer
    117
- Establishing a System Log
  118
- General Troubleshooting Approach
  118
- Detector Related Issues
  120
  - Internal Electronic Diagnostic Programs
    120
  - Gas
    122
  - Drainage
    123
  - Gain Range
    124
  - Grounding Issues
    125
- HPLC Related Issues
  126
  - Pump Noise
    126
  - Mobile Phase Flow
    127
  - Column
    128
  - Mobile Phase
    129
- Standard and Sample Related Issues
  130
- Thermal Organizer Issues
  131
- Noise Review
  132
- General Troubleshooting Guidelines
  133
  - Erratic/Noisy Baseline
    135
  - High Background Currents
    136
  - Increase in Back Pressure
    137
  - Loss of Response
    138
  - Inability to Autozero the Signal
    139
  - Detector Test Procedure
    139
- Power Supply Board and Logic Board Replacement
  140
  - Replacing the Power Supply Board
    140
  - Replacing the Logic Board
    140
Appendix A: Corona and Corona Plus Detector Specifications

141
- General Operating Specifications
  141
- A.2 Timeline Specifications
  142
- External Requirements
  142
- Physical Specifications
  142
- Timeline Specifications
  142
- A.5 Environmental
  143
- Certifications
  143
- Environmental
  143
Appendix Brecommended Supplies and Spare Parts

145
- B.1 Corona Accesories
  145
- Cables
  145
- Corona Accesories
  145
- Corona Replacement Parts
  145
- B.4 Manuals
  146
- Fuses
  146
- Manuals
  146
- Nitrogen Gas Supply
  146
- Organizer Module Spare Parts
  146
- Test Standards and Guard Column
  146
- Thermal Organizer Module Spare Parts
  146
Appendix C: Organizer and Thermal Organizer

147
- C.1 Overview
  147
- Overview
  147
- Unpacking the Organizer
  147
- Installing the Corona Organizer Module
  149
  - General Information
    149
  - Removing the Organizer Chassis Plate
    151
  - Installing the Pulse Damper
    151
  - Installing a Rheodyne Manual Sample Injector Valve
    152
  - Installing the In-Line Filter
    153
  - Installing the Column Holder
    153
  - Manual Sample Injector Overflow Line Bracket
    154
  - Final Assembly
    155
- Installing the Corona Thermal Organizer Module
  156
  - General Information
    156
  - Installing the Pulse Damper
    157
  - Removing the Organizer Chassis Plate
    157
  - Installing a Rheodyne Manual Sample Injector Valve
    158
  - Installing the Column Holder
    159
  - Installing the In-Line Filter
    159
  - Installing the Temperature Probe
    159
  - Final Assembly
    161
  - Manual Sample Injector Overflow Line Bracket
    161
  - C.5 Troubleshooting
    163
  - Cleaning
    164
  - Maintenance on a Daily Basis
    164
  - Maintenance on a Monthly Basis
    164
- Maintenance and Cleaning
  163
- Troubleshooting
  163
Appendix D: Firmware Flow Chart

165
Appendix Edrain/Vent Assembly - Old Styles

167
- Installing the Drain/Vent Assembly
  168
- Installing the Drain/Vent Assembly
  173
Glossary

177
Index

187

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