Endress+Hauser Analytik Jena multi N/C Manuals

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Endress+Hauser Analytik Jena multi N/C Operating Manual (106 pages)

pharma UV TOC Analyzer

Brand: Endress+Hauser | Category: Laboratory Equipment | Size: 5 MB

Table of Contents
3
Basic Information
7
User Manual Notes
7
Intended Use
8
Warranty and Liability
8
Safety Instructions
9
Safety Markings on the Analyzer
9
Technical Condition
9
Requirements for the Operating Personnel
10
Safety Instructions, Transport and Installation
11
Safety Instructions - Operation
11
General
11
Safety Instructions - Protection against Explosion and Fire
12
Safety Instructions - Electrical Equipment
12
Safety Instructions for Compressed Gas Containers and Systems
12
Safety Notes on UV Radiation
13
Handling of Auxiliary and Operating Materials
13
Safety Instructions - Service and Repair
14
Behavior During Emergencies
14
Function and Setup
15
System Design
15
Fig. 1 Front View (Doors Open)
15
UV Reactor with Control Gear
16
Components for Sample Preparation
16
Fig. 2 UV Reactor with Control Gear (Right-Hand Side Wall Open)
16
Hose System
17
Fig. 3 Syringe Pump with 9 Port Valve
17
Fig. 4 Hose Diagram
18
Fig. 5 Different FAST Connector Designs
19
Fig. 6 Fingertight Screw Connection
19
Fig. 7 Needle Valve to Adjust the NPOC Purge Flow (See Arrow)
19
Components for Gas Drying and Cleaning
20
Fig. 8 Condensate Pump
20
Fig. 9 TIC Condensation Module
21
Fig. 10 Water Traps
21
NDIR Detector
22
Fig. 11 Halogen Trap
22
Indicator and Control Elements, Connectors
23
Fig. 12 Diode to Indicate Readiness for Operation
23
Fig. 13 Connections on the Rear of the Device
23
Reagent Accessories
24
Autosampler for the Analyzer
24
Principle of Operation
24
Fig. 14 Principle of Operation
25
Measuring Method
26
TC Analysis
26
TOC Analysis
26
TIC Analysis
27
NPOC Analysis
27
NPOC Analysis According to the NPOC Plus Method
27
Calibration
28
Calibration Strategies
28
Day Factor
28
Calibration Method in Multiwin
29
Method Characteristics
30
Other Calculations
31
Blank Values
32
Blank Water Values
32
Reagent Blank Value
33
Eluate Blank Value
34
System Suitability Test (SST)
34
First Commissioning
36
Site Requirements
36
Installation Conditions
36
Space Requirement
36
Energy Supply
37
Gas Supply
37
Unpacking and Placing the Analyzer
37
Connecting Add-On Devices
38
AS Vario Autosampler
38
Fig. 15 Layout of the as Vario Autosampler
39
Fig. 16 Transport Lock on Autosampler as Vario
40
Fig. 17 Sleeve with 2 Cannulas
40
Sampler as 21
41
Fig. 18 Hose in Fingertight Connection
41
Fig. 19 Layout of the Sampler as 21
42
Fig. 20 Connections at the Bottom of the Sampler as 21
43
Fig. 21 Cannula Holder for Parallel Purging
44
Sampler as 10
45
Fig. 22 Layout of the as 10 Autosampler
46
EPA Sampler
47
Fig. 23 EPA Sampler
48
Fig. 24 Rear of the EPA Sampler
48
Fig. 25 Electrical Connections on the Rear of the EPA Sampler
49
Fig. 26 Transport Lock
49
Fig. 27 Fitting the Stirring Arm to the Autosampler
49
Fig. 28 Hose in Fingertight Connection
51
Operation
52
General Information for the Analysis Work
52
Reagents and Materials Required
52
Switching on the Analyzer (Standard Commissioning)
53
Switching off the Analyzer
54
Switching to Standby Mode
54
Switching off before Longer Periods of Rest
55
Carrying out the Calibration
56
Preparing and Starting the Calibration
56
Fig. 29 Calibration Window - DATA of NEW CALIBRATION
56
Displaying Calibration Results
58
Fig. 30 Window CURRENT SAMPLE DATA (with Sampler Operation)
58
Fig. 31 CALIBRATION Window - Data of the Completed Calibration
59
Editing an Existing Calibration
60
Transferring Calibration Parameters to a Method
61
Fig. 32 Disabling Individual Measured Values of a Calibration
61
Fig. 33 Window Link to Method
62
Fig. 34 Window LINK with METHOD with Three Areas
63
Managing Calibration Data
64
Fig. 35 Window CALIBRATION REPORT SELECTION
64
Performing Measurements
65
Measurement with Manual Sample Supply
65
Measurement with Sampler
66
Maintenance and Care
68
Maintenance Intervals
68
Adjustment and Setup Tasks
69
General Notes for Adjusting the Autosampler
69
Adjusting the as Vario Autosampler
69
Fig. 36 Adjustment Points on the Sample Tray
70
Adjust the NPOC Purge Flow
71
Adjusting the EPA Sampler
72
Replacing the Water Traps
74
Fig. 37 Water Traps on the Inside of the Device, Left Side Panel Opened
76
Replacing the Halogen Trap
77
Maintaining the UV Reactor
78
Checking the Illumination of the Lamp
78
Cleaning the UV Reactor
79
Cleaning the TC Condensation Vessel
79
Cleaning and Replacing the Syringe Pump
81
Removing and Replacing the Pump Hose
82
Replacing the Hose Connections
83
7.10 Checking the System for Tightness
84
Fig. 38 Angled FAST Connector with Connected Hose
84
Fig. 39 Replacing the Fingertight Connection
84
Fault Removal
86
General Information
86
Error Messages in Multiwin
87
Status Errors - Indications in the Window S
91
Ystem State
91
Equipment Faults and Analytical Problems
92
Transport and Storage
95
Transport
95
Preparing the Analyzer for Transport
95
Transport Notes
96
Preparing the Autosampler as Vario for Transport
96
Fig. 40 Transport Lock on Autosampler as Vario
96
Moving the Analyzer in the Laboratory
97
Storage
97
Recommissioning after Transport or Storage
98
Assembling the Analyzer after Transport or Storage
98
Connecting the Analyzer
98
Fig. 41 Mains Connection and Gas Connections at the Multi N/C Pharma UV
99
Disposal
101
10.1 Waste Water
101
10.2 Halogen Trap
101
10.3 Analyzer
101
10.4 UV Module
101
10.4.1 Removing the UV Module
101
Specifications
104
11.1 Technical Data
104
11.2 Standards and Directives
105

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Endress+Hauser Analytik Jena multi N/C Operating Manual (106 pages)

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