Dionex MSQ Manuals

Manuals and User Guides for Dionex MSQ. We have 1 Dionex MSQ manual available for free PDF download: User Manual

Dionex MSQ User Manual

Dionex MSQ User Manual (132 pages)

Brand: Dionex | Category: Laboratory Equipment | Size: 3 MB

Table of Contents

Chapter 1 Introducing the Msq

3
- Table of Contents
  3
- Introducing the MSQ
  5
- Introduction
  5
- System Overview
  6
- What Is Mass Detection
  8
- Exterior Features of the MSQ
  9
- The Source-An Introduction to API Techniques
  12
  - Electrospray
    13
  - Atmospheric Pressure Chemical Ionization
    17
  - Source Fragmentation
    20
  - Cone Voltage Ramping
    22
  - Polarity Switching
    23
  - Application of API Techniques
    24
- The Self-Cleaning Source: Cone Wash
  27
  - Introduction
    27
  - Functional Description
    28
- The Reference Inlet System
  29
  - Introduction
    29
  - Functional Description
    29
- The Mass Analyzer and Detector
  30
- The Vacuum System
  31
- The Data System
  32
  - Software
    32
  - Raw Data
    34
  - Raw Data Types
    35
2. Changing Ionization Modes

41
- Chapter 2 Changing Ionization Modes
  43
- Introduction
  43
- Switching from ESI to APCI
  44
- Switching from APCI to ESI
  46
Chapter 3 Lc/Ms and the Cone Wash

49
- LC/MS and the Cone Wash
  51
  - Introduction
    51
  - LC/MS Considerations
    52
- Flow Rates
  52
- HPLC Solvents and Mobile Phase Additives
  53
- Setting up the Cone Wash
  57
- Flow Splitting
  59
4. Reference Inlet System

61
- Chapter 4 Reference Inlet System
  63
- Introduction
  63
- Overview
  64
- Setting up the Reference Inlet System
  65
Chapter 5 Routine and Preventive Maintenance

69
- Introduction
  71
- Routine and Preventive Maintenance
  71
- Maintenance Schedule
  72
- Flushing the Capillaries
  73
- The Electrospray and APCI Probes
  73
- ESI Probe Removal
  74
- ESI Probe Disassembly
  75
- Cleaning the ESI Probe
  76
- Replacing the Capillary
  76
- ESI Probe Assembly
  77
- APCI Probe Removal
  78
- APCI Probe Disassembly
  79
- Cleaning the APCI Probe
  79
- APCI Probe Assembly
  80
- Replacing the Capillary
  80
- The Source Block Assembly
  81
- The Heater
  91
  - Heater Removal
    91
  - Cleaning the Heater
    91
  - Heater Replacement
    92
  - Checking the Rotary Pump Oil Level and Color
    93
  - Changing the Rotary Pump Oil
    95
Chapter 6 Troubleshooting

97
- Troubleshooting
  98
- Troubleshooting Help
  100
- Resolving Common Problems
  101
  - Checking the MSQ Power Supply Requirements
    101
  - Restarting the PC
    101
- HPLC System Troubleshooting
  102
  - Buffers and Additives
    102
  - Mobile Phase Reservoir
    102
  - Bubble Problems and Degassing
    102
  - Contamination in the LC System
    103
  - Tubing and Fittings
    103
  - Injection Valves
    105
  - UV Detectors
    105
  - Preventive Maintenance and Spares
    107
Chapter 7 Shutting down and Restarting the System

109
- Introduction
  111
- Shutting down and Restarting the System
  111
- Instrument Standby and Shutdown
  112
- Restarting the System
  116
  - Pre-Switch on Checklist
    116
  - System Start-Up Procedure
    117
  - Pumping down the MSQ
    118
  - Consumables and Spares
    121
    
    Introduction
    121
    
    Consumables
    122
- Chapter 8
  122
- General Consumables Kit (P/N 060046)
  122
- Probe Maintenance Kit (P/N 061495)
  124
- Source Maintenance Kit (P/N 061494)
  125

Advertisement

Advertisement

Related Products

Dionex Categories

Laboratory Equipment Measuring Instruments Analytical Instruments Security Sensors Water Pump

More Dionex Manuals