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Dionex DX-120 Ion Chromatograph Manuals
Manuals and User Guides for Dionex DX-120 Ion Chromatograph. We have
1
Dionex DX-120 Ion Chromatograph manual available for free PDF download: Operator's Manual
Dionex DX-120 Operator's Manual (162 pages)
ION CHROMATOGRAPH
Brand:
Dionex
| Category:
Laboratory Equipment
| Size: 3 MB
Table of Contents
Table of Contents
3
1 • Introduction
10
About this Manual
10
Typefaces and Conventions
11
Safety Messages and Notes
12
Symbols
13
2 • Description
15
Operating Features
15
Front Control Panel
17
Pump
20
Eluent Reservoirs
21
Component Panel
22
Rheodyne Injection Valve
25
Detector Cells
26
DS4 Detection Stabilizer
27
Dual-Column Configuration Features
29
Column Select Mode
30
Eluent Select Mode
32
Fluid Schematics
33
Control Modes
36
TTL Control
37
Injection Valve/Remote Start Control
37
Recorder Range Control
37
3 Operation and Maintenance
39
Preparing Eluents
39
Degassing Eluents
39
Filtering Eluents
40
Pressurizing Eluent Reservoirs
40
Preparing Samples
41
Collecting and Storing
41
Pretreating
41
Diluting
42
Operating
43
Starting up
43
Injecting the Sample
45
Using an Integrator
47
Running under Peaknet Control
47
Optimizing Temperature Compensation
48
With a DS4
48
With a CDM-3 Cell
48
Maintenance
49
4 Troubleshooting
51
Alarms
51
Error Codes
53
Liquid Leaks
54
Pump Difficult to Prime
58
Pump Loses Prime
58
Pump Does Not Start
59
No Flow
59
Excessive System Backpressure
59
Peak "Ghosting
60
Nonreproducible Peak Height or Retention Time
61
Abnormal Retention Time or Selectivity
61
DS4 Temperature Inaccurate
62
No Detector Response
63
Low Detector Output
64
High Detector Output
64
Noisy or Drifting Baseline
65
5 Service
67
Replacing Tubing and Fittings
68
Changing the Sample Loop
68
Isolating a Restriction in the Liquid Plumbing
69
Replacing the DS4 Cell
69
Cleaning Cell Electrodes
71
Calibrating the Cell Constant
72
Calibrating the Pump Flow Rate
74
Cleaning and Replacing Pump Check Valves
74
Replacing a Pump Piston Seal
75
Replacing a Pump Piston
78
Replacing the Pressure Transducer Waste Valve O-Ring
80
Changing the Main Power Fuses
81
A.1 Electrical
83
A.3 Control Panel
84
A.7 Conductivity Cell
85
A.10 Delay Volume
86
B.1 Facility Requirements
87
B.3 Rear Panel Connections
88
B.3.3 Waste Lines
91
B.4 Eluent Reservoir Connections
94
B.5.2 Checking the Pump Flow Rate Calibration
95
Connections to Chromatography Components
96
B.6.1 Backpressure Requirements
98
B.6.2 Self-Regenerating Suppressor (SRS Installation
99
B.6.3 Column Installation
103
TTL Control Connections (Overview)
105
B.7.2 TTL Outputs
106
B.7.3 Ferrite Core Installation on TTL Output Cables
107
Autosampler Connections (Optional)
108
B.8.3 AS3500 Automated Sampler Connections
110
B.9.1 Chart Recorder Connections
113
Recorder and Integrator Connections
113
Configuration DIP Switch Settings
115
DS4 Detection Stabilizer Installation
119
Cell Installation
121
Injection Valve Connections
122
Column Switching Valve Connections
123
DX-LAN Card Installation (Optional)
124
C • Integrator Programming
127
Integrator Power-Up Configuration
127
Setting Offsets
128
Area Percent Mode
128
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