Dionex ASE 100 Solvent Extractor Manuals

Manuals and User Guides for Dionex ASE 100 Solvent Extractor. We have 1 Dionex ASE 100 Solvent Extractor manual available for free PDF download: Operator's Manual

Dionex ASE 100 Operator's Manual

Dionex ASE 100 Operator's Manual (150 pages)

ACCELERATED SOLVENT EXTRACTOR

Brand: Dionex | Category: Ventilation Hood | Size: 3 MB

Table of Contents

Table of Contents
3
1 Introduction

9
- Overview
  9
- About this Manual
  11
  - Typefaces
    12
  - Safety Messages and Notes
    12
- Safety Labels
  14
2 Description

15
- Operating Features
  15
  - Control Panel Screen
    17
  - Control Panel Keypad
    18
  - Extraction Cells and Rinse Cells
    20
  - Collection Bottle
    21
  - Solvent Bottle
    22
  - Waste Bottle
    23
- Rear Panel
  23
- Extraction Process
  25
- Method Control
  27
- Preprogrammed Methods
  28
3 Operation and Maintenance

33
- Preparing to Run an Extraction
  33
  - Selecting and Preparing Solvent
    33
  - Filling the Solvent Bottle
    35
  - Preparing the Sample
    37
  - Installing the Cell Filter
    39
  - Filling the Cell
    41
  - Installing the Collection Bottle
    43
  - Rinsing/Priming the System
    44
- Editing a Custom Method (1-24)
  45
- Guidelines for Method Development
  49
- Running an Extraction
  52
- Post-Extraction Procedures
  56
  - Cleaning the Cells
    56
  - Processing Extracts
    56
- Aborting a Run
  57
- Routine Maintenance
  58
  - Daily Maintenance
    58
  - Periodic Maintenance
    58
- Shutdown
  59
4 Troubleshooting

61
- Error Messages
  61
- Liquid Leaks
  68
- Gas Leaks
  70
- System Stops
  70
5 Service

71
- Replacing the Seal in the Cell End Cap
  72
- Replacing the Cell O-Ring
  74
- Removing the Right Side Panel
  75
- Cleaning And/Or Replacing Pump Check Valves
  78
  - Removing the Pump
    78
  - Removing the Check Valves
    80
  - Cleaning the Check Valves
    80
  - Reinstalling the Inlet Check Valve
    80
  - Reinstalling the Outlet Check Valve
    81
  - Reinstalling the Pump
    81
  - Completing the Procedure
    81
- Replacing the Piston Seal
  82
  - Removing the Pump
    82
  - Replacing the Piston Seal
    83
  - Reinstalling the Pump
    84
  - Completing the Procedure
    84
- Replacing the Relief Valve
  85
- Replacing the Static Valve
  88
- Replacing the Source Needle
  90
- Replacing the Solvent Outlet Line
  93
- Replacing the Lower Autoseal Tip
  99
- Replacing the Main Power Fuses
  104
A • Specifications

107
- Physical
  107
- Environmental
  107
- Electrical
  107
- A.1 Physical
  107
- Pneumatic
  108
- Front Panel Display and Keypad
  108
- Extraction Cells
  108
- Collection Bottles
  108
- Interior Components
  108
- A.4 Pneumatic
  108
B • Installation

111
- Facility Requirements
  111
- B.1 Facility Requirements
  111
- Installation Instructions
  112
  - Nitrogen Connections
    112
  - B.2 Installation Instructions
    112
  - Electrical Connections
    114
  - B.2.2 Electrical Connections
    114
  - Checking Pressure Readings
    116
  - Solvent Bottle Connections
    118
  - Waste Bottle Installation
    120
  - Rinsing the System
    121
  - Adjusting the Cell Holder
    123
  - Inspecting the Cell
    125
  - Completing the Installation
    126
100 C • User Interface

128
- Operational Screens
  128
  - Main Screen
    128
  - C.1 Operational Screens
    128
  - Status Screen
    129
  - C.1.2 Status Screen
    129
  - Setup Screen
    130
  - C.1.3 Setup Screen
    130
  - Method Editor Screen
    133
- Diagnostic Screens
  135
  - Diagnostics Screen
    135
  - C.2 Diagnostic Screens
    135
  - Sensors Screen
    136
  - C.2.2 Sensors Screen
    136
  - Regulators Screen
    137
  - C.2.3 Regulators Screen
    137
  - Hydrocarbon Sensor Screen
    138
  - Extraction Counters Screen
    139
  - Moduleware Screen
    140
  - C.2.6 Moduleware Screen
    140

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