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CEM liberty Equipment and Supplies Manuals
Manuals and User Guides for CEM liberty Equipment and Supplies. We have
3
CEM liberty Equipment and Supplies manuals available for free PDF download: Operation Manual, Manual, User Manual
CEM liberty Operation Manual (118 pages)
microwave peptide synthesis
Brand:
CEM
| Category:
Laboratory Equipment
| Size: 2.86 MB
Table of Contents
Table of Contents
3
Section 1: Introduction
9
Introduction
9
About this Manual
9
Common Abbreviations and Units
10
How to Obtain Support
12
Applications Support
12
Technical Support
12
Requested Information
12
Contact CEM
13
CEM Corporation Headquarters
13
CEM International Subsidiaries
13
CEM Distributors
14
Safety Information
15
Safety Notations
15
Safety Information
16
Fume Ventilation
16
Waste Disposal
16
System Requirements
16
Bench And/Or Fume Hood Space
16
Environmental Conditions
17
Inert Gas Source
17
Electrical Requirements
17
Section 2: Operation of the Liberty
18
Introduction to the Liberty
18
Components and Parts
20
Reaction Vessel Components
21
Introduction to Pepdriver
22
Pepdriver Main Screen
23
Control Buttons
24
Menu Buttons
24
Indicators
24
Tabs
25
Revision 5 • October
26
Editors
27
Microwave Editor
27
Microwave Method Folders
27
Microwave Method Types
27
Creating a New Microwave Method
28
Editing an Existing Microwave Method
29
Cycle Editor
30
Cycle Folders
30
Copying and Modifying an Existing Microwave Method
30
Cycle Types
31
Creating a Cycle
31
Editing an Existing Cycle
32
Copying and Modifying an Existing Cycle
33
Sequence Editor
34
Creating a New Sequence
34
Modifying a Sequence
35
Using the External Amino Acid Positions
35
Importing a Sequence
36
Method Editor
38
Creating a New Method
38
Modifying an Existing Method
40
Calculators
41
Usage Calculator
41
Reagent Calculator
42
Resin Calculator
42
Deprotection Calculator
43
Activator Base Calculator
43
Activator Calculator
44
Amino Acid Calculator
44
Cleavage Calculator
45
Setting up a Synthesis
46
Configuring Methods to Run
46
Loading a Method
46
Loading Multiple Methods
47
Preparing Reagents
47
Standard Concentrations
47
Preparing Activator Solution
48
Preparing Activator Base Solution
48
Preparing Amino Acids
48
Preparing Deprotection Solution
49
Preparing Capping Solution
49
Preparing Cleavage Solution
50
Setting up the Liberty
50
Loading Reagents Onto the Liberty
50
Revision 5 • October
51
Loading Resin Onto the Liberty
52
Changing the Reaction Vessel
52
125 Ml Reaction Vessel
52
Running the Liberty
53
Preparing the Liberty to Run
53
Running the Liberty
54
Generating Reports
56
Method Reports
56
Creating a Method Report
56
Sample Method Report
57
Run History Reports
58
Creating a Run History Report
58
Sample Run History Report
58
Section 3: Quick Setup Guide
59
Peptide Setup
59
Create and Load the Method
59
Prepare Reagents
60
Ensure the Liberty Is Ready to Run
61
Section 4: Mainteance of the Liberty
63
Routine Maintenance
63
Daily Maintenance
63
Weekly Maintenance
63
Biweekly Maintenance
63
Monthly Maintenance
63
Semiannual Maintenance
64
Standby Procedure
64
Maintenance Screen
65
Cleaning Tab
65
Using the Change Bottle Command
67
Performing a Backflush
68
Performing a System Check
69
Revision 5 • October
70
Sample System Check File
71
Volume Calibration Tab
72
Performing a Volume Calibration
72
Importing and Exporting Volume Calibration Values
74
Performing a Large Scale Calibration
75
Sensor Calibration Tab
78
Performing a Sensor Calibration
78
Importing and Exporting Sensor Calibration Values
81
Pressure Calibration Tab
81
Performing a Pressure Calibration
82
Section 5: Advanced Features
84
Default Cycle Editor
84
Changing Default Cycles
84
Options Menu
85
Program Options Tab
85
Defaults Tab
87
Run History Tab
87
Test System Screen
88
Pressure Adjustment
89
Main Pressure Adjustment
89
Low Pressure Adjustment
90
Leak Check
90
Test Rotary Valves
91
Internal, Nitrogen, and Liquid Delivery Tests
92
Setting up the Liberty for a Delivery Test
92
Performing a Delivery Test
93
Test Sensors
93
Reagent, Amino Acid, and External Amino Acid Addition
95
Leak Check Reaction Vessel
96
Flow Performance
96
Diagnostics Screen
97
Commands Tab
97
Sensors Tab
97
Valves Tab
98
Status Tab
98
Revision 5 • October
98
Delay Times Tab
99
Section 6: Troubleshooting
100
Tips for Recovering from Errors
101
Section 7: Spare Parts and Consumables
102
Reaction Vessel Parts
102
Filters
103
Solvent Keg
103
Bottles
104
Bulk Tubing and Fittings
105
Bottle Tubing Assemblies
106
Bottle Caps
107
Dip Tubes
108
O-Rings
108
Valves and Valve Wiring
109
Liquid Sensors
110
Waste Container
111
Accessories and Tools
111
Computer Accessories
112
Circuit Boards
113
Regulators
113
Documentation
113
Revision 5 • October
114
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CEM liberty Manual (63 pages)
Automated Microwave Peptide Synthesizer
Brand:
CEM
| Category:
Synthesizer
| Size: 3.24 MB
Table of Contents
Table of Contents
3
Introduction
5
About the Instrument
5
Common Abbreviations and Units
5
How to Obtain Support
6
Applications Support
6
Technical Support
6
Requested Information
6
CEM Corporation Headquarters
6
CEM International Subsidiaries
7
Safety
9
Safety Notations
9
Personal Laboratory Safety
9
Waste Disposal
9
Fume Ventilation
9
Safety Safety Notations
9
Operating Precautions
10
System Requirements
11
Bench And/Or Fume Hood Space
11
System Components Space Requirements
11
Environmental Conditions
11
Inert Gas Source
11
Electrical Requirements
11
Fuse Replacement
11
Introduction to the Liberty Blue
12
Components and Parts
12
Quick Setup Guide
14
Create and Load the Liberty Method
14
Prepare and Load Reagents
15
Run the Method
16
Operation of the Liberty Blue
18
Software Terminology
18
Liberty Blue Software Main Screen
18
Microwave Editor
20
Cycle Editor
22
Liberty Method Editor
26
Calculators
32
Edit Users and User Group
34
Setting up a Synthesis
37
Loading a Method
37
Standard Reagents and Concentrations
37
SPPS on the Liberty Blue
37
Preparing Reagents
40
Setting up the Liberty Blue
41
Running the Liberty Blue
43
Generating a Run History Report
44
Cleavage
45
Maintenance of the Liberty Blue
46
Recommended Routine Maintenance Schedule
46
Maintenance Procedures
47
Maintenance Screen
51
Using the Change Bottle Operations
51
Calibration Screen
52
Advanced Features
54
Cycle Rules
54
Reagent Library
54
Bottle Setup
56
Refill Reagents Button
57
Diagnostics Screen
57
Settings Screen
57
Reaction Vessel Camera Option
58
Warranty
59
Limited Warranty Information
59
Warranty Limited Warranty Information
59
CEM liberty User Manual (8 pages)
Automated Microwave Peptide Synthesizer
Brand:
CEM
| Category:
Laboratory Equipment
| Size: 0.37 MB
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