Buchi K-365 Dist Line Manuals

Manuals and User Guides for Buchi K-365 Dist Line. We have 1 Buchi K-365 Dist Line manual available for free PDF download: Operation Manual

Buchi K-365 Dist Line Operation Manual (106 pages)

Brand: Buchi | Category: Laboratory Equipment | Size: 5 MB

Table of Contents
3
About this Document
9
Mark-Ups and Symbols
9
Trademarks
9
Connected Devices
9
Safety
10
Proper Use
10
Use Other than that Intended
10
Staff Qualification
10
Personal Protective Equipment
11
Warning Notices in this Document
11
Warning and Directive Symbols
11
Protection Devices
12
Residual Risks
12
Hot Surfaces
13
Faults During Operation
13
Glass Breakage
13
Not Suitable Titrators
13
Dosing Pump Defect
13
Modifications
13
Product Description
14
Description of Function
14
Configuration
14
Front View
14
Rear View
16
Receiving Area
16
Communication Connections
18
Connections on the Rear Side
20
Scope of Delivery
23
Type Plate
23
Technical Data
24
Dist Line
24
Ambient Conditions
26
Materials
26
Installation Site
27
Transport and Storage
28
Transport
28
Storage
28
Lifting the Instrument
28
Installation
29
Before Installation
29
Establishing Electrical Connections
29
Securing against Earthquakes
29
Installing the Cooling Water Supply
30
Installing a Tap Water Supply (Option)
30
Installing the Recirculating Chiller on the Condenser (Option)
30
Installing the Drain Tubing (Option)
31
Installing the Waste Pump Connection (Basicdist, Multidist, Multidist T Only)
31
Installing the Sample Waste Pump Connection (Multidist T Only)
32
Installing the H₂O Supply for Steam Generation
32
Installing Naoh Supply (Multidist, Multidist T Only)
33
Installing H₃BO₃ Supply (Multidist, Multidist T Only)
33
Installing the H₂O Supply for the Sample Tube (Multidist, Multidist T Only)
34
Installing the Level Sensor on the Canister (Option)
35
Installing a Titrator with LAN (Multidist T with Eco Titrator Only)
35
Installing a Titrator with RS232 (Multidist T Only)
36
Installing a Dispenser (Multidist T Only)
37
Installing the Reaction Detection Sensor (Multidist T Only)
37
Installing a SD Card (Interface Pro Only)
37
Installing the Level Detection Sensor (Option)
37
Installing the Stirrer (Multidist Only)
38
Description of the Interface
39
Layout of the Interface
39
Function Bar Interface
40
Menu Bar Interface
40
Home Menu
40
Manual Control Menu
40
Method Menu
41
Configuration Menu
41
Determination Data Menu
41
Status Bar Interface
43
Description of the Interface Pro
45
Layout of the Interface Pro
45
Function Bar Interface Pro
46
Menu Bar Interface Pro
47
Home Menu
47
Manual Control Menu
47
Configuration Menu
47
Determination Data Menu
47
Status Bar Interface Pro
50
Preparations for a Determination
52
Editing the Preheating Function
52
Editing the Priming Function
52
Editing the Single Determination
52
Changing the Name of the Single Determination
52
Selecting the Determination Type for a Single Determination
53
Selecting the Method for a Single Determination
53
Changing the Sample Quantity for Single Determination
54
Changing the Unit for a Single Determination
54
Editing a Series
55
Creating a New Series
55
Changing the Name of a Series
55
Adding a Determination to a Series
56
Deleting a Determination from a Series
56
Changing the Determination Name for a Series
56
Selecting the Determination Type Within a Series
57
Selecting the Method for a Determination Within a Series
58
Changing the Sample Quantity for Determination Within a Series
58
Changing the Amount Unit for a Determination Within a Series
58
Editing a Template
59
Creating a New Template
59
Changing the Name of a Template
60
Editing a Method
60
Creating a New Method
60
Deleting a Method
60
Changing the Name of a Method
61
Changing the Reaction Detection for a Method (Option for Multidist Only)
61
Changing the H₂O Volume for a Method (Multidist Only)
62
Changing the H₂SO₄ Volume for a Method (Multidist Only)
62
Changing the Naoh Volume for a Method (Multidist Only)
63
Changing the Acid Volume for a Method (Basicdist, Multidist Only)
63
Changing the Reaction Time for a Method (Basicdist, Multidist Only)
64
Changing the Number of Steam Steps for a Method
64
Changing the Time a Steam Step Is Carried out for a Method
65
Changing the Steam Power for a Method
66
Changing the Level Detection Sensor Settings (Option) for a Method
66
Changing the Distillation Time for a Method
67
Changing the Distillation Stirring Speed for a Method (Multidist T Only)
67
Changing the Titration Type for a Method (Multidist T Only)
68
Changing the H₃BO₃ Volume for a Method (Multidist Only)
68
Changing the Dosing Unit Volume for a Method (Multidist T Only)
69
Changing the Titration Stirring Speed for a Method (Multidist T Only)
69
Changing the Titration Start Time for a Method (Multidist T Only)
69
Changing the Aspiration Time for the Sample Tube for a Method (Basicdist, Multidist, Multidist T Only)
70
Changing the Aspiration Time for the Receiving Vessel for a Method (Multidist T Only)
70
Editing User Setting
71
Creating a New User
71
Deleting a User
71
Changing the Name of a User
72
Selecting a User
72
Installing the Sample Tube
72
Installing a Receiving Vessel
73
Preparing the End Stop for the Sample Tube Size
73
Preparing the Level Detection Sensor (Option)
74
Selecting the Operation Mode
74
Dosing Manually
74
Dosing H₂O Manually
74
Dosing Naoh Manually
75
Dosing H₃BO₃ Manually
75
Aspirating Manually
75
Aspirating the Sample Tube Manually
75
Aspirating the Receiving Vessel Manually
76
Changing the Stirring Speed Manually
76
Switching Valve Adjustment (Multidist Only)
76
Carrying out a Determination
78
Preparing the Instrument
78
Starting a Determination
78
Ending a Determination
79
Shutting down the Instrument
79
Filtering Determination Data
79
Showing Determination Data
79
Deleting Determination Data
79
Deleting One Determination
79
Deleting All Determination Data
80
Exporting Determination Data (Interface Pro Only)
80
Exporting One Determination (Interface Pro Only)
80
Exporting All Determination Data (Interface Pro Only)
80
Cleaning and Servicing
81
Regular Maintenance Work
82
Cleaning and Servicing the Sample Tube
82
Cleaning the Glass Components
83
Cleaning and Servicing the Hoses and Hose Connections
83
Cleaning and Servicing the Sample Tube Seal
83
Cleaning and Servicing the Splash Protector
84
Cleaning and Servicing the Steam Inlet and Condenser Outlet Tube
84
Cleaning the Housing
84
Cleaning and Servicing the Warning and Directive Symbols
84
Cleaning and Servicing the Bridge Splash Protector to Condenser
84
Cleaning and Servicing the Dosing Pumps
84
Cleaning and Servicing the Condenser
84
Cleaning and Servicing the Steam Generator
85
Calibrating the Pumps
85
Calibrating the H₂O Pump
85
Calibrating the Acid Pump
86
Calibrating the Naoh Pump
86
Calibrating the H₃BO₃ Pump
87
Decalcifying the Instrument
87
Replacing the Splash Protector
88
Replacing the Condenser
89
Attaching and Removing the Protection Shield
89
Removing the Protection Shield
89
Attaching the Protection Shield
90
Cleaning the Drip Tray
90
Rinsing a Pump
90
Replacing the Sample Tube Seal
90
Help with Faults
92
Troubleshooting Digestion
92
Troubleshooting Distillation
93
Troubleshooting Instrument
95
Turning the Splash Protector Nut
97
Taking out of Service and Disposal
98
Taking out of Service
98
Disposal
98
Returning the Instrument
98
Removing Water from the Steam Generator
98
Appendix
99
Spare Parts and Accessories
99
Accessories
99
Splash Protector Spare Parts
100
Tank Spare Parts
101
Condenser Spare Parts
101
Titration Spare Parts
102
Sample Tubes
103
Cable and Tubing
103
Other Spare Parts
104
Consumables
104
Maintenance Kit
105
Upgrade Kits
105
Documentation
105

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