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1290 Infinity II LC
Agilent Technologies 1290 Infinity II LC Manuals
Manuals and User Guides for Agilent Technologies 1290 Infinity II LC. We have
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Agilent Technologies 1290 Infinity II LC manual available for free PDF download: User Manual
Agilent Technologies 1290 Infinity II LC User Manual (395 pages)
Solution for MassHunter TOF and Q-TOF
Brand:
Agilent Technologies
| Category:
Measuring Instruments
| Size: 13.82 MB
Table of Contents
Table of Contents
5
Introduction
10
Product Description
11
Features
12
Terms Related to 2D-LC
14
2 Concepts of 2D-Lc
15
Concepts of 2D-LC Heart-Cutting 2D-LC (LC-LC)
15
Concepts of 2D-LC
16
Multiple Heart-Cutting and High Resolution Sampling 2D-LC
19
Principles of Heart-Cutting 2D-LC
22
Comprehensive 2D-LC (Lcxlc)
30
Concept of Peak Triggering
32
Triggering of 2D-LC
32
Concept of Time Triggering
34
Active Solvent Modulation (ASM)
35
Introduction to Active Solvent Modulation (ASM)
35
Operating Principle
37
Understanding the ASM Factor
42
Comprehensive 2D-LC and Active Solvent Modulation
44
3 Compatibility Matrix
45
Supported Chromatographic Data Systems
46
Supported Drivers
47
Supported Operating Systems
48
Supported Firmware
49
Available Languages
50
PC Requirements
51
Licensing
52
4 Installation
53
Delivery Checklist
54
Hardware Installation
54
Options
55
Recommendations for Instrument Setup
60
Licensing the 2D-LC Instrument
87
LC Software Installation in Agilent Masshunter Workstation
89
Software Installation
89
LC Software Configuration Agilent Masshunter Workstation
93
5 2D-Lc Data Acquisition in Masshunter Workstation 11
103
LC Data Acquisition in Masshunter Workstation
104
Start the Data Acquisition Software
104
Overview 2D-LC in Masshunter Acquisition 11
106
Instrument Status
107
2D-LC User Interface
108
Additional Information in the 2D-LC User Interface
108
LC Valves Online Monitor in the 2D-LC User Interface
114
Method Editor Window
116
Sample Run Window
117
Worklist Window
118
Tune Window
119
Instrument Details
120
Use Module List to Obtain Instrument Details
120
Use Instrument Configuration Report to Obtain Instrument Details
121
Log Book in Masshunter Acquisition 11
123
6 Method Parameters
125
Method Editor 2D-LC
126
2D LC Operation Mode
127
Set the 2D-LC Method Parameters
127
Define the 1D Pump Flow
129
Define the 2D Pump Flow
129
Define the 2D Solvent
130
Define the Stoptime
130
Define the Posttime
132
Edit the Sampling Table
133
Define the 2D Gradient
139
Use the Flush Gradient
147
Use Peak Trigger
148
Use the Advanced 2D Pump Settings
152
Preview (2D-LC)
154
Further Graphical Explanation
162
Set up a Peak-Based Experiment Graphically
168
Setup 2D Gradient Graphically
173
Setup Second Dimension Gradient with the Graphical User Interface
175
Additional Information
177
Multi-Inject
177
Dynamic Peak Parking
179
7 Method Development of Active Solvent Modulation (Asm)
185
Method Development of Active Solvent Modulation (ASM)
186
Method Parameters
187
Optimize the Dilution by Using ASM Capillaries
188
Optimize the Sample Loop Flush
189
Include the ASM Phase to the 2D Gradient
190
Optimize Dilution through Method Settings
191
8 Run the System
192
Familiarization to Start a System Run
193
Prepare the 2D-LC System
194
Configure the 2D-LC System
195
Checkout Familiarization Procedure
198
Prepare the Experiment
199
Run the Checkout Familiarization Procedure for Standard Heart-Cutting 2D-LC (LC-LC)
201
Run the Experiment
201
Run the Checkout Familiarization Procedure for Multiple Heart-Cutting (2D-LC)
206
Run the Checkout Familiarization Procedure for High Resolution (LC-LC)
210
Run the Checkout Familiarization Procedure for Comprehensive (Lcxlc)
214
Run the Checkout Familiarization Procedure for ASM Multiple Heart-Cutting (MHC)
219
Run the Checkout Familiarization Procedure for ASM Comprehensive
224
Data Analysis
229
LC Data Analysis/Data Evaluation for Masshunter
230
GC Image Basic Information
256
10 Troubleshooting and Diagnostics
275
Overview of the Module's Indicators and Test Functions
276
User Interfaces
277
Agilent Lab Advisor Software
278
Integrated 2D-LC Functions in the Lab Advisor Software
279
Lab Advisor Instrument Control
280
2D-LC Hardware License Handling
280
2D-LC Capillaries Configuration Tool
283
Instrument Control of the 2D-LC Cluster
284
Lab Advisor Service & Diagnostic
286
Decluster the 2D-LC Cluster
286
Pump Head Leak Test for the 2D Pump
287
Pump Leak Rate Test for the 2D Pump
288
System Pressure Test for the 2D Pump
289
2D-LC Capillary Leak Test
291
Replace the Module Firmware
292
The Basic Principle of Troubleshooting
294
Table of Contents
296
Pressure too High
297
Pressure too Low
298
Peak Area and Peak Height Related
299
Retention Time Related
300
Missing Signal Linearity
301
Drifting Signal
302
Signal Noisy
303
Recommended Tests to Conclude Troubleshooting
304
11 Error Information
305
What Are Error Messages
306
General Error Messages
307
Timeout
307
Shutdown
308
Lost CAN Partner
309
Remote Timeout
309
Leak Sensor Open
310
Leak Sensor Short
310
Compensation Sensor Open
311
Compensation Sensor Short
311
Fan Failed
312
Leak
312
Module-Specific Error Messages
313
Initialization of Valve Failed
313
Valve Switching Failed
314
Valve Tag Violation
314
Position Cluster Partner Missing
315
Pressure Cluster Partner Missing
315
External Valve Falls into Resident Mode
316
12 Maintenance
317
Introduction to Maintenance
318
Warnings and Cautions
319
Overview of Maintenance
321
Cleaning the Module
322
Correcting Leaks
323
Correcting Leaks (G1170A)
323
Replace Valve Heads
324
Correcting Leaks (G7116B)
323
Replace Valve Heads (G7116B)
324
Replace Valve Heads (G1170A)
327
Replacing Parts of the Valve Head
330
Replacing the Fuses of the Infinity Valve Drive
332
13 Parts for Maintenance
334
2D-LC Loops
335
2D-LC Capillaries
336
ASM Capillaries
337
Pressure Release Kit
338
2D-LC Easy Starter Kit
339
Valve Drive Parts
340
Valve Driver Parts Infinity II
341
Valve Head Parts
342
Technical Specifications
343
Tools
343
Vale Options Overview (for 2D-LC)
344
Obsolete Valve Heads
347
MS Diverter Valve
348
Additional Parts for the MS Diverter Valve Setup
349
Valve Options Overview (for G7116B)
350
Additional Heater Devices
352
Additional Heater Devices (for G7116B)
353
Accessories and Consumables (for G7116B)
354
Infinitylab Quick Connect and Quick Turn Fittings
356
Infinitylab Quick Connect Fittings
357
Infinitylab Quick Connect Fitting Replacement Capillaries
358
Infinitylab Quick Turn Fitting
359
Capillary Kits
360
Important Customer Web Links
361
Theoretical Background
362
Theoretical Basis of 2D-LC
363
Orthogonality
364
Resolution
365
Peak Capacity
368
As Detector
371
Successful Mode Combinations
373
Solvent Elution Modes
374
Practical Issues
380
15 Appendix
382
General
383
General Safety Information
383
Safety Standards
383
Before Applying Power
384
Ground the Instrument
384
Do Not Modify the Instrument
385
Do Not Operate in an Explosive Atmosphere
385
Do Not Remove the Instrument Cover
385
In Case of Damage
385
Solvents
386
Safety Symbols
387
Waste Electrical and Electronic Equipment (WEEE) Directive
389
Radio Interference
390
Sound Emission
391
Solvent Information
392
Further Information
393
Agilent Technologies on Internet
394
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