Saeco Talea Ring Operation And Maintenance Manual
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Saeco Talea Ring Operation And Maintenance Manual

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4005
0423
LGC Science and Technology Division
LGC Produced Reference Materials Catalogue
July 2014

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  • Page 1 4005 0423 LGC Science and Technology Division LGC Produced Reference Materials Catalogue July 2014...

  • Page 2: Table Of Contents

    Contents Code ......Batch ..Description ........Page Number Melting Point Materials ERM-FC021 ....a ..... Carbazole ............... 9 ERM-FC022 ....a ..... 2-Chloroanthraquinone ........... 9 ERM-FC023 ....a ..... p-Anisic Acid..............9 ERM-FC024 ....a ..... Diphenylacetic Acid ............10 ERM-FC025 ....
  • Page 3 Code ......Batch ..Description ........Page Number Elemental Analysis Materials LGC4001 ....1 ....Dibenzothiophene ............17 LGC4002 ....1 ....Acetanilide ..............17 LGC4003 ....1 ....Benzoic Acid..............17 LGC4008 ....1 ....4-Bromobenzoic Acid ........... 17 LGC4009 ....1 ....2-Iodobenzoic Acid ............17 Optical Materials ERM-FB012 ....
  • Page 4 Code ......Batch ..Description ........Page Number Freshwater Sediment Materials Cont. LGC6189 ...... 1 ..... River Sediment – Extractable Metals ......26 Soil Materials ERM-CC135 ....a ..... Brick Works Soil – Metals ..........27 LGC6115 ...... 1 ..... Contaminated Soil – PCBs and PAHs ......27 LGC6145 ......
  • Page 5 Code ......Batch ..Description ........Page Number Fruit and Vegetable Products ERM-BC084 ....a ..... Tomato Paste – Metals ..........35 LGC7111 ...... 2 ..... Potato Powder – Sulfur Dioxide ........35 LGC7162 ...... 1 ..... Strawberry Leaves – Trace Elements ......35 Drink Products ERM-BD011 ....
  • Page 6 Code ......Batch ..Description ........Page Number CLINICAL MATERIALS Whole Blood Material ERM-DA110 ....a ..... Tacrolimus in Human Blood ......... 44 Serum Materials ERM-DA120 ....a ..... Copper, Selenium, Zinc in Frozen Human Serum ..45 ERM-DA200 ....a ..... Frozen Human Serum – Digoxin High Level ....45 ERM-DA201 ....
  • Page 7 Disclaimer While every reasonable precaution has been taken in the preparation of this document, the author does not assume responsibility for errors or omissions in the information contained herein. Please contact LGC Standards for more information before purchase. Version 10.0 – July 2014...
  • Page 8 Introduction LGC’s Science and Technology Division acts as the designated UK National Measurement Institute (NMI) for Chemical and Biochemical measurement and has a long history in the development and validation of analytical methods and the production of reference materials. Many of the analytical methods used to characterise the reference materials are accredited to ISO/IEC 17025 (Requirements for the competency of testing and calibration laboratories) and have been verified through participation on key comparison studies organised by the Consultative Committee for the Amount of Substance (CCQM) of the International Weights and Measures Organisation (BIPM).

  • Page 9: Code

    Melting Point Materials Code Batch Description Unit Size ERM-FC021 Carbazole 0.25 g A batch of commercial carbazole was purified by recrystallisation and vacuum sublimation, then ground, homogenised and dried. This material is intended for use in checking and calibrating apparatus used for the determination of melting points of samples in glass capillary tubes.

  • Page 10: Erm-Fc024

    Code Batch Description Unit Size ERM-FC024 Diphenylacetic Acid 0.25 g A batch of commercial diphenylacetic acid was ground, homogenised and dried. This material is intended for use in checking and calibrating apparatus used for the determination of melting points of samples in glass capillary tubes. Certified Value Liquefaction Point ..

  • Page 11: Erm-Fc027

    Code Batch Description Unit Size ERM-FC027 Benzil 0.25 g A batch of commercial benzil was ground, homogenised and dried. This material is intended for use in checking and calibrating apparatus used for the determination of melting points of samples in glass capillary tubes. Certified Value Liquefaction Point ..

  • Page 12: Enthalpy Of Fusion Materials

    Enthalpy of Fusion Materials Code Batch Description Unit Size LGC2601 Indium 0.5 g A suitable supply of pure material was obtained. This material is intended for the calibration of differential scanning calorimeters and similar instruments. Certified Values Enthalpy of Fusion .... 3.295 ± 0.010 kJ/mol Melting Temperature ....

  • Page 13: Lgc2608

    Code Batch Description Unit Size LGC2608 Lead 0.5 g A suitable supply of pure material was obtained. This material is intended for the calibration of differential scanning calorimeters and similar instruments. Certified Values Enthalpy of Fusion .... 4.765 ± 0.012 kJ/mol Melting Temperature ....

  • Page 14: Purity Materials

    Purity Materials Code Batch Description Unit Size ERM-AC200 Digoxin A batch of digoxin was obtained from a commercial supplier of reagents. 0.5 g This material is intended for use in the validation and calibration and monitoring of methods to determine digoxin content and it can be used in the training and evaluation of staff.

  • Page 15: Erm-Ac803

    Code Batch Description Unit Size ERM-AC803 Theophylline 0.5 g A batch of theophylline was obtained from a commercial supplier of reagents. This material is intended for use in the validation of new methods, and monitoring the performance of methods and instruments commonly used in clinical laboratories to determine the theophylline content of human blood samples.

  • Page 16: Lgc1205

    Code Batch Description Unit Size LGC1205 Malathion 0.25 g A batch of malathion was dried at ambient temperature under vacuum. This material is intended for use as a calibration standard in methods of analysis for malathion in food, environmental and other relevant matrices. Certified Value Purity .......

  • Page 17: Elemental Analysis Materials

    Elemental Analysis Materials Code Batch Description Unit Size LGC4001 Dibenzothiophene 0.5 g A supply of dibenzothiophene of adequate purity was obtained, from which aliquots were sub-sampled and sealed in vials. This material is a micro-analytical standard intended for use in checking the performance of elemental analysers.

  • Page 18: Optical Materials

    Optical Materials Code Batch Description Unit Size ERM-FB012 IR Wavelength Standard 1 mL This wavelength standard is intended for use in the verification and calibration of infra-red spectrometers within the range of spectral bandwidths quoted. Certified Values True Peak Position Shifts of Wavelength by Resolution Spectral Bandwidth 0.5 cm Spectral Bandwidth 2 cm...

  • Page 19: Flash Point Materials

    Flash Point Materials Code Batch Description Unit Size ERM-FC032 n-Nonane 100 mL A supply of n-nonane, of nominally 99 % purity, was obtained from a commercial supplier. This material is intended for use in validation work, or in quality control procedures, for the determination of non-equilibrium flashpoint determined by the Abel closed cup method as described in the Institute of Petroleum Standard IP170/95, and also published as British Standard BS2000:Part 170: 1995.

  • Page 20: Forensic Alcohol Materials

    Forensic Alcohol Materials Code Batch Description Unit Size ERM-AC401 Aqueous Ethanol – 80 mg/100 mL 25 mL The purity of a suitable supply of ethanol was determined following estimation of organic impurities by gas chromatography and the water content by Karl Fischer titration ERM-AC401 is primarily intended for use as a reference material for the calibration and validation of methods for the determination of ethanol in biological fluids.

  • Page 21: Erm-Ac510

    Code Batch Description Unit Size ERM-AC510 Aqueous Ethanol – 50 mg/100 mL 25 mL ® This ERM , produced by LGC is a solution of ethanol in water at a nominal concentration of 50 mg/100 mL. ERM-AC510 is primarily intended for use as a reference material for the calibration and validation of methods for the determination of ethanol in biological fluids.

  • Page 22: Environmental Matrix Materials

    ENVIRONMENTAL MATRIX MATERIALS Code Batch Description Unit Size DRINKING WATER MATERIALS ERM-CA011 Hard Drinking Water UK – Metals 250 mL Hard drinking water was sourced from Tamworth (Staffordshire, UK) potable mains supply. The water was filtered through a 0.2µm in-line filter and acidified to approximately 0.1% nitric acid.

  • Page 23: Erm-Ca022

    Code Batch Description Unit Size ERM-CA022 Soft Drinking Water UK – Metals 250 mL Soft drinking water was sourced from the Bury (Lancashire, UK) potable mains supply. This material is intended for use in development, validation or quality control of analytical methods for the determination of metals in soft drinking water.

  • Page 24: Miscellaneous Water Materials

    Code Batch Description Unit Size MISCELLANEOUS WATER MATERIALS LGC6016 Estuarine Water – Trace Metals 50 mL Collected from the Severn Estuary, UK, offshore from a heavily industrialised area near Avonmouth. This material is intended for use in development, validation or quality control of analytical methods for the determination of metals in estuarine water.

  • Page 25: Sediment Materials

    SEDIMENT MATERIALS Code Batch Description Unit Size FRESH WATER SEDIMENT MATERIALS LGC6187 River Sediment – Extractable Metals 80 g River sediment which was obtained from monitoring station lagoon on the River Elbe close to the Czech-German border. This material is intended for use in development, validation or quality control of analytical methods for the determination of elements in landfill leachates.
  • Page 26 Code Batch Description Unit Size FRESH WATER SEDIMENT MATERIALS LGC6189 River Sediment – Extractable Metals 30 g River sediment was collected from a monitoring station lagoon on the River Elbe close to the Czech-German border. Assessed values for extractable metals precisely following the ISO11466 (1995) method.
  • Page 27 Code Batch Description Unit Size SOIL MATERIALS ERM-CC135 Brick Works Soil – Metals 50 g This material is a contaminated soil that was obtained from a brickworks site in Hackney, London. This material is intended for use as a reference material in the development, validation or quality control of analytical methods for the determination of extractable metals and total metals in soils.
  • Page 28 Code Batch Description Unit Size LGC6145 Contaminated Clay Loam Soil – Extractable Metals, PAHs and 50 g Inorganics This material was blended from two soils, sourced from the Czech Republic and one soil sourced from the UK. This material is intended for use in validating methods for the determination of metals in soil materials.
  • Page 29 Code Batch Description Unit Size LGCQC3005 Loamy Sand Soil 1 – Metals, Inorganics and PAHs 2 x 250 g A supply of dried soil was purchased from a supplier in Germany. This material is intended for use as a quality control material for analytical methods used in the investigation of soil for contamination.
  • Page 30 Code Batch Description Unit Size SEWAGE SLUDGE MATERIALS ERM-CC136 Sewage Sludge – Metals 25 g Aged sewage sludge collected from a disused sewage works site at Heathrow in London, UK. Dried, sterilised and ground to a powder. The extractable metal content refers to metals soluble in aqua regia using methods based on ISO11466 (1995).
  • Page 31 Code Batch Description Unit Size LGC6184 Sewage Sludge – PCBs 30 g Digested sewage sludge of mixed origin, taken from a city water treatment plant in the Czech Republic, immediately after discharge from a digestion tank. This material is intended for use in development, validation or quality control of analytical methods for the determination of polychlorinated biphenyls in sewage sludge.
  • Page 32 Code Batch Description Unit Size ASH, PARTICULATE AND DUST MATERIALS LGC6180 Pulverised Fuel Ash – Extractable and Total Metals 50 g This material was obtained from a disposal site near Carmarthen Bay in South Wales, UK. Pulverised fuel ash is a waste product of coal-fired power stations. This material is intended for use in development, validation or quality control of analytical methods for the determination of the extractable metal content in ash- based material.
  • Page 33 FOOD MATRIX PRODUCTS Code Batch Description Unit Size MILK AND MILK PRODUCTS LGC7104 Sterilised Cream – Proximates and Nutrient Elements 170 g A cream product was prepared by a UK food company. This material is intended for use in development, validation or quality control of analytical methods for the determination of the major constituents and elements in foods.
  • Page 34 Code Batch Description Unit Size LGC7222 Ground Raw Pork 10 g Pork was purchased from a commercial source as three pieces of boned leg. The pieces were trimmed and the lean meat homogenised to produce a paste. This material is intended for use as a reference standard for species identification analytical methods.
  • Page 35 Code Batch Description Unit Size FRUIT AND VEGETABLE PRODUCTS ERM-BC084 Tomato Paste – Metals 50 g This material was prepared by adding solutions containing cadmium, tin and lead to a commercial tomato paste. This material is intended for use in the validation of methods for the determination of tin, lead and cadmium in a fruit or vegetable based material.
  • Page 36 Code Batch Description Unit Size DRINK PRODUCTS ERM-BD011 Orange Juice 3 mL Commercially obtained orange juice was diluted with water. This material is intended for use as a reference material in the development, validation or quality control of analytical methods for the determination of degrees Brix or Refractive Index of sugar solutions and food extracts.
  • Page 37 Code Batch Description Unit Size PROCESSED FOOD PRODUCTS ERM-BC210 Wheat Flour Selenium and Selenomethionine 30 g Selenised wheat was obtained from a UK university. The grain was cleaned with water, milled at a temperature between 18 ° C and 20 ° C and 60 % relative humidity, and sieved twice to a final particle size of 140 µm.
  • Page 38 Code Batch Description Unit Size LGC7105 Rice Pudding – Proximates and Elements 200 g A rice pudding dessert was prepared by a UK food company. This material is intended for use in the development, validation or quality control of analytical methods for the determination of the major constituents and elements in foods.
  • Page 39 ALCOHOL MATRIX MATERIALS Code Batch Description Unit Size ERM-AC404 Reference Spirit – 5 % ABV 25 mL A suitable supply of ethanol was obtained, checked for purity and diluted with water to produce a solution with a nominal ethanol concentration of 5 % ABV. The primary use of this reference material is for checking the calibration of automatic density meters commonly used in industry to determine alcoholic strength, and for checking analyst and method performance.
  • Page 40 Code Batch Description Unit Size ERM-BA005 Lager – 5 % ABV 330 mL A commercial supply of pasteurised lager was obtained. This material is intended for use as a reference material for the development, validation or quality control of methods for the determination of alcohol in alcoholic beverages.
  • Page 41 Code Batch Description Unit Size LGC5100 Whisky – Congeners 10 mL A suitable supply of whisky was obtained from a commercial source. This material is intended for use in development, validation or quality control of analytical methods for the determination of congeners in spirit samples. The material may also be applicable to other matrices where suitable reference materials are not available.
  • Page 42 ANIMAL FEEDING STUFFS Code Batch Description Unit Size LGC7173 Poultry Feed – Proximates and Elements 50 g A sample of poultry feed was purchased from a commercial animal feed manufacturer. This material is intended for use in the development, validation or quality control of analytical methods for the determination of proximates and elements in animal feeding stuffs.
  • Page 43 INDUSTRIAL MATRIX MATERIALS Code Batch Description Unit Size ERM-EB503 Automobile Catalyst – Platinum Group Elements 100 g This material is a mixture of unused automobile catalysts supplied and prepared by a commercial manufacturer. This material is intended for use as a reference material in the development, validation or quality control of analytical methods for the determination of platinum group elements (PGE) in automobile catalysts.
  • Page 44 CLINICAL MATERIALS Code Batch Description Unit Size WHOLE BLOOD MATERIAL ERM-DA110 Human Blood - Tacrolimus 1 mL The material was prepared by Analytical Services International (London, UK) by spiking blank pooled human whole blood with a standard solution of tacrolimus to give a nominal concentration of 8 µg/kg tacrolimus in blood.
  • Page 45 SERUM MATERIALS ERM-DA120 Frozen Human Serum – Trace Metals 2 mL Human serum from a single donor was prepared from blood obtained at the Royal Surrey County Hospital (Guildford, UK). This material is intended for the validation of new and existing methods, and monitoring the performance of methods, commonly used in clinical laboratories to determine the importance of trace elements copper, selenium and zinc in human serum samples.
  • Page 46 Code Batch Description Unit Size ERM-DA250 Creatinine and Electrolytes in Frozen Human Serum 1 mL Human blood serum was obtained from donors at the University Hospital of Wales. This material is intended for the validation and on-going monitoring of methods of analysis for the determination of creatinine and electrolytes in human blood samples Certified Values 4005...
  • Page 47 GYPSUM MATERIALS Code Batch Description Unit Size LGC2700 Natural Gypsum – Major Oxides and Trace Elements 75 g Natural gypsum, in the form of small chippings, was obtained from British Gypsum (East Leake, Leicestershire, UK). The material was prepared using a jaw crusher fitted with hardened chromium steel jaws to provide a powder, nominally 3 mm maximum diameter.
  • Page 48 Code Batch Description Unit Size LGC2701 Natural Anhydrite – Major Oxides and Trace Elements 75 g Anhydrite, in the form of coarse chippings, was obtained from British Gypsum (East Leake, Leicestershire, UK). The material was prepared using a jaw crusher fitted with hardened chromium steel jaws to provide a powder, nominally 3 mm maximum diameter.
  • Page 49 Code Batch Description Unit Size LGC2702 Blended Gypsum – Major Oxides and Trace Elements 75 g Blended gypsum, in the form of chippings and powders, was obtained from British Gypsum (East Leake, Leicestershire, UK). The material was dried at 30 ° C in a calibrated drying oven, then ball-milled in a cleaned 250 mL capacity agate milling vessel until the powder passed a calibrated 75 µm stainless steel sieve mesh.
  • Page 50 Code Batch Description Unit Size LGC2703 Melnik desulfurised Gypsum – Major Oxides and Trace Elements 75 g Melnik desulfurised (DSG) gypsum, in powder form, was obtained from British Gypsum (East Leake, Leicestershire, UK). The material was dried at 30 ° C in a calibrated drying oven.
  • Page 51 CARBON ISOTOPE RATIOS Code Batch Description Unit Size ERM-AE672 Glycine – Absolute Carbon Isotope Ratio 0.5 g The material was prepared from a single batch of commercially available high purity glycine. This material is intended for use in the calibration of instruments, the validation of new methods and the monitoring of the performance of methods used for the determination of carbon isotope ratios.

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