ecodyst EcoChyll X3 Operating Manual

12l hi-speed evaporator system
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Accelerating the Extraction Process™
EcoChyll X3
12L Hi-Speed Evaporator System
OPERATING MANUAL
1

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Summary of Contents for ecodyst EcoChyll X3

  • Page 1 Accelerating the Extraction Process™ EcoChyll X3 12L Hi-Speed Evaporator System OPERATING MANUAL...
  • Page 2 Accelerating the Extraction Process™ ECOCHYLL X3 SUMMARY DESCRIPTION The EcoChyll® X3 is routinely used downstream of botanical extractions via BHO, CO2, or ethanol. With twin metallic condenser coils, the EcoChyll® X3 carries out continuous direct cooling of incoming vapors in an efficient and environmentally friendly manner. A key performance indicator of the entire EcoChyll® lab equipment range is the ability to free up operator time due to low-intervention requirements. The EcoChyll® X3 enables scientists in smaller facilities to automate their processes, ultimately saving time and money without compromising the quality of your results. Based on the same pioneering technology as our disruptive EcoChyll® range of evaporators, the EcoChyll® X3 bridges the gap between small-footprint lab equipment and the full-scale, high throughout alternatives.
  • Page 3: Table Of Contents

    Accelerating the Extraction Process™ TABLE OF CONTENTS SAFETY INSTRUCTIONS ........................4 General Safety Instructions ......................... 4 Intended use ................................ 4 Improper use ................................ 4 Installation / Electrical Safety ........................ 4 Personnel Qualification ............................. 5 Operating Company’s Obligations ........................ 5 Safety During Use .............................. 6 Disposal .................................. 6 ACCESSORIES AND SPARE PARTS ....................7 Scope of Delivery .............................. 7 DEVICE DESCRIPTION ........................10 Device Overview ..............................10 Technical Data ..............................12 ASSEMBLY ............................12 Installation ................................12 Condenser controller .
  • Page 4: Safety Instructions

    Accelerating the Extraction Process™ SAFETY INSTRUCTIONS General Safety Instructions The device has been constructed according to state-of-the-art technology and recognized safety regulations. However, risks may still arise during installation, operation and maintenance. Please ensure the operating manual is available at all times. The device may only be used under the following circumstances • Only operate the device, if it is in full working order. • Ensure all operators of the device possess the necessary safety and risk awareness. • Operate the device according to the instructions stipulated in this manual only. • If there is something you do not understand, or certain information is missing, ask your manager or contact the manufacturer. •...
  • Page 5: Personnel Qualification

    Accelerating the Extraction Process™ Personnel Qualification The device may only be operated by qualified persons. • The device may only be operated by individuals who have been instructed in its • proper use by qualified persons. The device may only be operated and maintained by persons who are of legal age. • Other personnel may only work with the unit under continuous supervision of an • experienced qualified operator. This manual must be read and understood by all persons working with the device.
  • Page 6: Safety During Use

    Accelerating the Extraction Process™ C. Safety for the Personnel Ensure that only qualified personnel operate the device. Observe the following regulations: o Laboratory guidelines o Accident prevention regulation o Ordinance on Hazardous Substances o Other generally accepted rules of safety engineering and occupational health o Local regulations Safety During Use • Wear the appropriate protective clothing when working on the device (clothing, protective glasses and if necessary, safety gloves).
  • Page 7: Accessories And Spare Parts

    Accelerating the Extraction Process™ ACCESSORIES AND SPARE PARTS Scope of Delivery Qty Part No Image Description ECO-555-X3-12 ECOCHYLL X3 12 LITER HIGH SPEED EVAPORATOR COMPLETE SYSTEM, TO INCLUDE: ECO-555-X3 Ecodyst EcoChyll X3, 115V dual condenser double loop Halar coated stainless steel coils ECO-777-133 Condenser Body, Left Side, 120mm Flat O-Ring Flange, Vacuum Port 1" OD Pipe ECO-777-134 Condenser Body, Right Side, 120mm Flat O-Ring Flange, 1" OD Pipe ECO-777-199 120mm Quick Release Clamp ECO-777-197 120mm Viton O-ring ECO-777-005 1” PFA Elbow Compression Fitting ECO-777-015 1” PFA Tee Compression Fitting ECO-777-006 FEP Tubing, 1” O.D. x 7/8” I.D., 6ft Length ECO-777-007 Vacuum tubing, 12ft length ECO-777-008 Advanced Self Cleaning Dry Vacuum with Digital Controller...
  • Page 8 Accelerating the Extraction Process™ ECO-777-010 1” to 1’’ PFA Tee Compression Fitting ECO-777-011 Inlet feed tubing 5ft length ECO-777-115 12 Liter Evaporator Flask, 150mm Flat O-Ring Bottom Drain Valve Flange, 1.5" ECO-777-013 150mm Reaction Vessel Lid, 4 Neck, 45/50 Outer joint CN, 1-Verti al 24/40 joint, 2- Elbow 1” TC ECO-777-014 Bottom Drain Valve, 2" Beaded Pipe, 1" Beaded Pipe Sidearm ECO-777-003 120mm Quick Release Clamp ECO-777-015 120mm Viton O-Ring ECO-777-016 Bottom Valve Clamp, 2” Coupling ECO-777-017 19mm Polished Stir Shaft, overall length 30.6" ECO-777-018 5.5" O.D. Teflon Agitator, High Viscosity ECO-777-019 19mm Flake-Free Stirrer Bearing, 45/50 ECO-777-020 Stirrer Shaft Coupling, 19mm ECO-777-108 Compact Overhead Stirrer with mounting rod ECO-777-103 12 Liter Heating Mantle, 4" Diameter Hole in Bottom, 2 Circuits Rated @770 Watts, 115V, 1540 watts total...
  • Page 9 Accelerating the Extraction Process™ ECO-777-105 Digital Temperature Controller, 230V, 15 amps, 1800 watts ECO-777-024 Coiled cord type T type plug ECO-777-106 Teflon coated Temperature probe ¼x22 ECO-777-107 PTFE ¼” Thermocouple Adapter, 24/40 ECO-777-027 1.5” TC Ball Valve with Hope Nipple ECO-777-028 1.5” TC Elbow Hose Adapter 1” ECO-777-128 Beam Torque Wrench with 7/16’’ deep socket ECO-777-030 EcoChyll X3 and Evaporator Support Stand ECO-777-031 Coreflex Vapor Hose, 1" ID PTFE, End Connection 1” OD ECO-777-063 Universal Kiwik Klamp and L mount rod. ECO-777-124 Positive Displacement Pump for emptying keg ECO-777-129 1/6B Keg Receiving System with accessories for 12 and 22 liter systems...
  • Page 10: Device Description

    Accelerating the Extraction Process™ DEVICE DESCRIPTION Device Overview Crossbeam Overhead Stirrer Heating Mantle Controller Shaft Coupling Shaft Bearing Stir Shaft Inlet Feed Valve Vapor Hose Quick Release Clamp O-Ring Inside Stainless Steel Lid Evaporator Flask Bottom Drain Valve Heating Mantle Evaporator Stand Cross Section of Evaporator Flask Agitator Valve Clamp...
  • Page 11 Accelerating the Extraction Process™ Vacuum port Temperature Controller Left Side Condenser Quick Release Clamp Right Side Condenser Condenser Connector Hose Elbow Compression Fitting Adapter Connection to EcoChyll Vent Valve Full Level Sight Glass Drain Valve Keg Receiver...
  • Page 12: Technical Data

    Accelerating the Extraction Process™ Technical Data Power Supply Four 115V, 15 amps 4 115V receptacles 1. EcoChyll X3, 115V, 10 amps, 1150 watts 2. 12L EcoChyll X3 Digital Temperature Controller. 2 Circuits @770 watts fused, 1540 watts total Input voltage: 120 Vac, single phase Power: 15 amps, 1800 watts. Customer Provides Outlet Receptacles NEMA 5-15R Cord end plug is NEMA 5-15P 3. Vacuum pump, 115V 150W 4. Overhead Stirrer, 115V 150W ASSEMBLY Installation Please refer to the Installation Guide Condenser controller Press to set the value as required.
  • Page 13: Led Functions

    Accelerating the Extraction Process™ LED Functions LED Functions On Indicates the Setup Mode has been entered (This LED is labeled SET on indicator models) Flashing Indicates the manual mode has been entered (On indicator models this LED is labeled SET and flashes when in Configuration Mode) On Indicates that Controller Self Tune mode is engaged Flashing Indicates that Controller Pre-Tune mode is engaged Flashing Indicates that an alarm condition is present Flashes In unison with Time Proportioning Primary outputs, or for Current Proportioned outputs, ON indicates primary power is >0% (On indicators these lights when the stored Max PV value is displayed) Flashes In unison with Time Proportioning Secondary outputs, or for Current Proportioned outputs, ON indicates primary power is >0% (On indicators these lights when the stored Max PV value is display...
  • Page 14: Post Operations

    Accelerating the Extraction Process™ POST OPERATIONS Cleaning Recommended to clean condenser glass after use and replace tubing as needed. Maintenance The unit is maintenance-free. Any necessary repair must be performed by an authorized Ecodyst distributor. Please contact Ecodyst or your local Ecodyst distributor. Troubleshooting Loss of Vacuum Assess and tighten clamps on various components Check vacuum seal on rotary evaporator Ice Build Up on Condenser Ensure EcoChyll is not left on for long periods without Condensing Transportation and Storage • Store and transport the unit and its components only if they were emptied and cleaned in the original packing material. • Alternatively store and transport the unit in a container which prevents damages during transportation.
  • Page 15: Service

    In the case of repair, copy and complete the Confirmation of condition of unit and send it to Ecodyst. Product number Serial number Reason for repair Has the device been cleaned, decontaminated/sterilized? _____ Yes _____ No Is the unit in a condition which does not represent any health threats for the staff of our service department? _____ Yes _____ No If not, which substances has the unit come into contact with? _________________________________________________________________________________________________________ _________________________________________________________________________________________________________ _________________________________________________________________________________________________________ Legally binding declaration The customer is aware of being legally liable to Ecodyst for any damages arising from incomplete and incorrect information. Signature: Date: Please note: The shipper is responsible for the return of the goods in well packed condition, suitable for the mode of transport. Last name, first name Company Street Zip code, city, country E-mail...
  • Page 16: Contact Details

    Accelerating the Extraction Process™ CONTACT DETAILS Ecodyst, Inc. 1010 Goodworth Dr. Apex, NC 27539 919-717-4061 info@ecodyst.com www.ecodyst.com Instagram LinkedIn Facebook Twitter Invented for scientists by scientists.

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