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Distek Evolution 4300 Operation Manual

Dissolution sampler
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Operation
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Evolution 4300
Dissolution Sampler

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Summary of Contents for Distek Evolution 4300

  • Page 1 Evolution 4300 Dissolution Sampler Operation Manual...
  • Page 2 Distek Model Evolution 4300 Dissolution Sampler Operation Manual Document 3843-0005  Distek, Inc. 121 North Center Dr. • North Brunswick, NJ 08902 Phone 732.422.7585 • Fax 732.422.7310 http://www.distekinc.com Email: info@distekinc.com...

  • Page 3: Document Revision History

    Email: info@distekinc.com CenterChek, HeightChek, RPMChek, ShaftChek, and TempChek are trademarks of DISTEK, Inc. The DISTEK logo is a registered trademark of DISTEK, Inc. All other company and product names are trademarks or registered trademarks of their respective holders. Document Revision History...

  • Page 4: Table Of Contents

    Audience .................. ii Contents .................. ii Prerequisites ................iii Documentation................iii Conventions ................iii Introduction .................1-1 Overview ................1-2 Evolution 4300 Site Requirements ..........1-2 Specification ................1-2 Physical Site Requirements ............1-3 Environmental Considerations............1-4 Ambient Laboratory Temperatures ..........1-4 Ambient Laboratory Humidity ............1-4 Air Quality Considerations............1-5 Operation Warnings and Notes ............1-6...
  • Page 5 Setting Up Communication with Distek Model 2100B/Model 2100C ...2-9 Setting Up Communication with Distek Premiere 5100 ....... 2-11 Setting Up Communication with Distek Evolution 6100/6300 Dissolution System................. 2-12 Configuring the Syringe Pump Address (Single Bath System)....2-12 Configuring the Syringe Pump Address (Dual Bath System)....2-13 Changing the Syringe Pump Address..........
  • Page 6 Printing Method Settings ............3-24 Running Methods..............3-24 Standalone System ............... 3-25 Controlling a Distek Model 2100B or Model 2100C Dissolution System ... 3-25 Controlling a Distek Premiere 5100 Dissolution System (Paddles) ..3-25 Controlling a Distek Premiere 5100 Dissolution System (Baskets) ..3-26 Controlling a Distek Evolution 6100/6300 Dissolution System (Paddles).

  • Page 7: About This Manual

    About This Manual About this Manual About This Manual includes information about what is contained in this manual and the conventions used. Purpose..................ii Audience .................. ii Contents .................. ii Prerequisites ................iii Documentation................iii Conventions ................iii Operation Manual: Evolution 4300...

  • Page 8: Purpose

    Distek Evolution 4300 Dissolution Sampler. It has information regarding the commands, menus, indicators and controls. Chapter 1 provides an overview of the Evolution 4300. Chapter 2 covers the steps to unpacking and installation of the system. Chapter 3 includes operation and programming information.

  • Page 9: Prerequisites

    This manual assumes that you understand the principles of dissolution testing. Documentation This manual contains important information regarding the safe operation, maintenance and repair of your Distek Evolution 4300 Dissolution Sampler. Conventions Warning statements are used in this manual to prevent WARNING injury to personnel.

  • Page 10: Introduction

    Chapter 1: Introduction Introduction This chapter provides an overview of the Evolution 4300 and system specific specifications. Overview ................1-2 Evolution 4300 Site Requirements ..........1-2 Specification ................1-2 Physical Site Requirements ............1-3 Environmental Considerations............1-4 Ambient Laboratory Temperatures ..........1-4 Ambient Laboratory Humidity ............1-4 Air Quality Considerations............1-5...

  • Page 11: Overview

    Chapter 1: Introduction Overview The Distek Evolution 4300 Dissolution Sampler is a media sampling instrument capable of sampling into test tubes or directly injecting into HPLC vials. The system can be configured as a single or dual bath capable unit via one or two eight channel syringe pump(s).

  • Page 12: Physical Site Requirements

    24” (0.61m). However, the minimum recommended bench depth is 25” (0.64m). 2. The minimum linear bench space requirement is 38” (0.97m). Distek recommends that at least 39” (.99m) be allocated to allow for adequate clearance to power off the syringe pumps.

  • Page 13: Environmental Considerations

    Maximum Conditions: 1. The Evolution 4300 is designed to be installed and operated in laboratories where the maximum operating temperature does not exceed 25°C. 2. The maximum allowable ambient operation temperature is 30°C.

  • Page 14: Air Quality Considerations

    Chapter 1: Introduction Air Quality Considerations Distek autosampling systems are designed to be operated in a lab environment that has no visible dust problem, and with organic solvent vapor levels as low as possible. Operation is not recommended in dusty lab environments, or in labs with significant chlorinated or reactive solvent vapor levels.

  • Page 15: Operation Warnings And Notes

    External cables (excluding power cable) are limited to less than 3 meters length in order to maintain electromagnetic compliance. Some forms of electromagnetic interference may cause unexpected operation. If this occurs, the unit will return to normal operation once the interference is removed. Operation Manual: Evolution 4300...

  • Page 16: Installation

    Setting Up the Rinse Station............2-6 Installing the Rack Assembly ............2-7 Setting Up the Power and Communication Connections ......2-8 Setting Up Communication with Distek Model 2100B/Model 2100C ...2-9 Setting Up Communication with Distek Premiere 5100 ....... 2-11 Setting Up Communication with Distek Evolution 6100/6300 Dissolution System.................

  • Page 17: Unpacking

    Notify DISTEK or your shipper immediately with any discrepancies or damage to cartons or contents in transit. The Evolution 4300 will arrive in 1 box containing the collector and either one or two pumps depending on the purchased configuration.

  • Page 18: Installing The Fluid Connections

    See Figure 2-1 for specific locations on the rear of the syringe pump. The end of each line contains a ferrule and fitting. 1. To Dissolution Vessels 2. To Collector/Sampler 3. To Replacement, pH or Dilution Media Figure 2-1: Tubing Outlet Diagram from Syringe Pump Operation Manual: Evolution 4300...

  • Page 19: Installing The Syringe Filter Adapter (If Applicable)

    Figure 2-2: Installing the Fluid Connections Installing the Syringe Filter Adapter (If Applicable) One of the option accessories for the Evolution 4300 is a syringe filter adapter. The adapter enhances the unit’s performance when a syringe filter will be utilized. For more information contact Distek and ask about Part Number 2800- 0110.

  • Page 20: Routing The Waste Tubes

    (5/16” O.D.) is a waste line and should be placed into a waste container (See Figure 2-4). The waste tube empties the rinse tank and recycle bin by the use of gravity, therefore it is critical that the waste tube is positioned well below the collector! Operation Manual: Evolution 4300...

  • Page 21: Setting Up The Rinse Station

    Figure 2-4: Rinse Station, Recycle Bin and Waste Tubes Setting Up the Rinse Station The Evolution 4300 is equipped with a needle rinse station. The rinse station is used to clean the outside sleeve of the collector needles between methods or sampling intervals.

  • Page 22: Installing The Rack Assembly

    Chapter 2: Installation Installing the Rack Assembly The Evolution 4300 comes configured with a split rack that can be configured for both test tubes and HPLC vials. Depending on what was purchased the unit will be equipped with two test tube racks or two vial racks, or a combination of the two.

  • Page 23: Setting Up The Power And Communication Connections

    (each unit contains two RS-485 connections). Repeat the connection for an additional pump in a dual bath configuration. 4. If the Evolution 4300 will be connected to a DISTEK Model 5100, Model 2100B or Model 2100C an additional RS-485 connection is necessary.

  • Page 24: Setting Up Communication With Distek Model 2100B/Model 2100C

    The firmware revision for the TCS must be 1.30 or higher. The Evolution 4300 is capable of controlling a Distek Model 2100B and Model 2100C Dissolution system. Follow these steps to configure the connection: 1. The Model 2100 must be configured to run in Slave mode in order to accept commands from the Evolution 4300.
  • Page 25 2. Connect a RS-485 from the rear of the Syringe Pump to an open RS-485 on the Model 2100. 3. The Evolution 4300 now needs to be configured with the address of the 2100 and the TCS. These addresses can be obtained by turning the power off and then on.

  • Page 26: Setting Up Communication With Distek Premiere 5100

    3.0 or higher for the motor board and 3.24 or higher for the stage board. The Evolution 4300 is capable of controlling a Distek Premiere 5100 Dissolution system. Follow these steps to configure the connection: 1. Connect a reverse RS-485 cable from the rear of the Syringe Pump to an open RS-485 on side of the 5100 (any available port will work).

  • Page 27: Setting Up Communication With Distek Evolution 6100/6300 Dissolution System

    Configuring the Syringe Pump Address (Single Bath System) If the Evolution 4300 is configured as a single bath system the address of Pump B must be set to N/A. Setting the address to N/A will disable certain functions that can only be used in a dual bath system.

  • Page 28: Configuring The Syringe Pump Address (Dual Bath System)

    4 in Pump B’s address field. Be sure to use an address other than the one used for Pump A. 11. Turn on Pump A. 12. From the MAIN screen press the ESC/HOME button to home the system. The pump address should never be permanently set to 00. 2-13 Operation Manual: Evolution 4300...

  • Page 29: Changing The Syringe Pump Address

    7. Turn on the other pump. 8. From the MAIN screen press the ESC/HOME button to home the system. The pump address should never be permanently set to 00. 2-14 Operation Manual: Evolution 4300...

  • Page 30: Logging On To The System For The First Time (Factory Setting)

    13. Highlight the Logout menu and press ENTER. 14. Log on to the system using the new username and password. 15. Highlight the System menu and press ENTER. 16. Highlight the Distek user from the list and press the DEL key from the keypad. Installation Checkout Your instrument has been tested thoroughly prior to shipment.

  • Page 31: Operation

    Administration Settings ............3-6 Login Procedures ..............3-6 Creating a New Account ............3-7 Changing the Privileges of an Existing Account ......3-8 Changing a Password ............3-8 Deleting an Account .............3-9 Configuration Settings .............3-9 System Parameter Settings............3-10 Printing a Report..............3-11 Operation Manual: Evolution 4300...
  • Page 32 Printing Method Settings ............3-24 Running Methods..............3-24 Standalone System ............... 3-25 Controlling a Distek Model 2100B or Model 2100C Dissolution System ... 3-25 Controlling a Distek Premiere 5100 Dissolution System (Paddles) ..3-25 Controlling a Distek Premiere 5100 Dissolution System (Baskets) ..3-26 Controlling a Distek Evolution 6100/6300 Dissolution System (Paddles).

  • Page 33: Control Keypad

    Chapter 3: Operation Control Keypad The control keypad is shown below: Figure 3-1: Evolution 4300 Keypad The functions of the buttons are as follows: ESC/HOME Button The ESC/HOME button will allow the operator to navigate back to the higher level menu screen within the interface. If this button is selected while in the main screen with the system IDLE, both the sampler and syringe pumps will reset to their home positions.

  • Page 34: Arrow Keys

    This button is also used to scroll through “A”, “B” and “A B” when setting a method to run via the Method screen. - Button The – button works in conjunction with the + button to scroll in the opposite direction. Operation Manual: Evolution 4300...

  • Page 35: Display Screens

    This format is consistent throughout the interface. System Administration System administration incorporates three screens that can be found under the ADMIN, CONFIG and SYSTEM menu picks. The table below described the basic functions within each section. Operation Manual: Evolution 4300...

  • Page 36: Administration Settings

    System Parameter Settings on page 3-10. Administration Settings The Evolution 4300 is equipped with login access to allow for USER and MANAGER group settings. A USER can view and select a method to run on a particular bath. The MANAGER is able to create/modify methods, change configuration settings, modify parameters and has user administration control.

  • Page 37: Creating A New Account

    8. Enter the password using the keyboard. Use the arrow keys to navigate through the keyboard and press ENTER to select an alphanumeric value (maximum of 8 characters). 9. Once the password is entered navigate to the OK button and press ENTER. Operation Manual: Evolution 4300...

  • Page 38: Changing The Privileges Of An Existing Account

    Use the arrow keys to navigate through the keyboard and press ENTER to select an alphanumeric value (maximum of 8 characters). 4. Once the new password is entered navigate to the OK button and press ENTER. Operation Manual: Evolution 4300...

  • Page 39: Deleting An Account

    The valid settings are ON or OFF. • PUMP 1: Sets the address of Pump 1 (see Configuring the Syringe Pump Address (Dual Bath System) on page 2-12 for more information). Operation Manual: Evolution 4300...

  • Page 40: System Parameter Settings

    2100C or a Premiere 5100 Dissolution Test System. This field will set the type of bath that is connected to the Evolution 4300. Select N/A if the Evolution 4300 will be running independently of a dissolution bath (not controlling the bath parameters).

  • Page 41: Printing A Report

    The media is then discarded through the replacement lines. Printing a Report • A printer must be connected to the Evolution 4300 via the parallel port in order to produce a printout. • A maximum of 12 reports can be stored.

  • Page 42: Using Quick Action Commands

    Chapter 3: Operation Using Quick Action Commands The Evolution 4300 is capable of running one-time quick action commands. These actions are accessed from the Main screen (See Figure 3-3). Simply highlight the ACTION field, use the + and – buttons to toggle through the available options and press ENTER to run a one-time action.

  • Page 43: Auto Action

    5. Once the desired value is set press the ENTER key. 6. The method name at the top of the screen located under the bath name should now reflect the change. Figure 3-10: Method Screen 3-13 Operation Manual: Evolution 4300...

  • Page 44: Programming A New Method

    12. Use the arrow key to highlight the SAVE menu and press ENTER. 13. Highlight the PARA menu and press ENTER. 14. Configure to desired parameter setting. See Setting up Method Parameters on page 3-15 for more information on parameters. 3-14 Operation Manual: Evolution 4300...

  • Page 45: Setting Up Method Parameters

    The parameter screen (see Figure 3-12) allows the operator to set up parameters for pump flow rate, volumes and media volume options. Definitions of Parameter settings: Pump Flow Rates Collection: Flow rate at which the sample volume will be delivered to the tubes/vials. 3-15 Operation Manual: Evolution 4300...
  • Page 46 5. If set to ON the washing will run continuously until the operator aborts the action. If set to OFF only one wash cycle will occur. Setting 1-5 allows the user to set a specific number of wash cycles. 3-16 Operation Manual: Evolution 4300...
  • Page 47 2. Highlight the method name from the list and press NEW/OPEN. 3. Highlight PARA from the menu and press ENTER. 4. Using the arrow keys scroll through the pump flow rates, volumes and options adjusting the values using the + and – keys. 3-17 Operation Manual: Evolution 4300...

  • Page 48: Media Replacement

    The loss is due to the fact that some equipment is incapable of returning the unused portion of the sample medium to the vessel from which it was withdrawn. Utilizing the media recycle option with the Evolution 4300 will allow this media to be recycled back to the respective test vessels. When media recycle is set to on, the flush and offset volume will be returned to each vessel.
  • Page 49 4. Select the BATH menu button. Figure 3-13 and Figure 3-14 show sample screen for a 2100C and 5100 dissolution system. 5. Make the necessary changes to the bath parameters. 6. Select SAVE. Figure 3-13: Model 2100C Settings Figure 3-14: Model 6100 Settings 3-19 Operation Manual: Evolution 4300...

  • Page 50: Programming A Method Using The Dilution Functionality

    Varying Volume Dilution Varying volume dilution allows for different volume to be applied to each sample row. For example, a method with 5 sample time points could have 3-20 Operation Manual: Evolution 4300...

  • Page 51: Programming A Method Using The Ph Change Functionality

    2. At any point in the sample list a pH adjustment step may be added. Add a step at the desired time and set the 'ACTION' to 'PH_ADJ'. 3. Set the 'VOLUME' field to the desired volume. 3-21 Operation Manual: Evolution 4300...

  • Page 52: Programming A Method For Large Volume Sampling (> 9 Mls)

    Chapter 3: Operation Programming a Method for Large Volume Sampling (> 9 mls) The Evolution 4300 is capable of sampling up to 20mL per time interval. In order to obtain large volume sample results, one time point must be dispensed into multiple rows.

  • Page 53: Open/View An Existing Method

    6. To delete a step: Highlight a row in the sample time point list and press the DEL key. 7. The time, row #, action and setup fields can be modified by highlighting the field and selecting the + or – button to toggle through the available options. 3-23 Operation Manual: Evolution 4300...

  • Page 54: Deleting A Method

    4. Press the ENTER button from the keypad. Running Methods The Evolution 4300 can be configured as a standalone dissolution sampler or can be setup to run a Distek Model 2100B, Model 2100C, Premiere 5100 Dissolution System, Evolution 6300 and/or Evolution 6100. See Chapter 2 for more information on configuring bath communication.

  • Page 55: Standalone System

    The following sections describe the steps necessary to run methods under the various configurations. Standalone System 1. Select RUN METHOD from the Main screen (see Figure 3-3). 2. This will trigger an audible beep from the Evolution 4300 and the Main screen will display the message: DROP TABLET! TIMER: 20 SECONDS 3.

  • Page 56: Controlling A Distek Premiere 5100 Dissolution System (Baskets)

    Activate the method on the Premiere 5100 and press the HEAT button to start the test. 7. The test can only begin when both the Evolution 4300 and the Premiere 5100 display ready messages. When the bath temperature has been...

  • Page 57: Controlling A Distek Evolution 6100/6300 Dissolution System (Baskets)

    Chapter 3: Operation 3. The Evolution 4300 will display the message “PLEASE WAIT FOR BATH TEMPERATURE” on the Main screen. 4. When the bath temperature has been reached the unit will display the message: BATH_NAME VESSEL TEMP HAS BEEN REACHED. PLEASE FOLLOW INSTRUCTIONS ON THE 6100/6300.
  • Page 58 Chapter 3: Operation Figure 3-16: Map Screen To display the map screen: 1. Highlight the MAP menu from the main screen and press ENTER. 3-28 Operation Manual: Evolution 4300...

  • Page 59: Serial Port Control Of Evolution 4300

    Chapter 3: Operation Serial Port Control of Evolution 4300 For PC control, monitoring and reporting, the Evolution 4300 has a serial RS-232 port. Test commands carefully. Improper PC control of remote instruments may lead to unexpected operation. Collector Serial Command Reference...
  • Page 60 NN.N ml for B Sample liquid (NN.N [AA_M:F:A NNN] [NNN] ml) from A Sample liquid (NN.N [AA_M:F:B NNN] [NNN] ml) from B Sample liquid (NN.N [AA_M:F:S NNN] [NNN] ml) from Sampler Set up unit address [AA_Z_NN] [NN] 3-30 Operation Manual: Evolution 4300...
  • Page 61 Chapter 3: Operation Command Function Command Format Response Format Get Serial Number [AA_R] [SPXXXXXX ] [0] = Ready Check Unit Status [AA_S:S] [9] = Not Home AA represents the unit address. 3-31 Operation Manual: Evolution 4300...

  • Page 62: Maintenance

    This chapter gives a very brief overview of properly maintaining the Evolution 4300. To ensure consistent performance a Preventive Maintenance/Operational Qualification (PM/OQ) should be conducted periodically. Contact Distek for more information. General Information ..............4-2 Replacement of Tubing Lines............4-2 Operation Manual: Evolution 4300...

  • Page 63: General Information

    Distek recommends a six month Preventative Maintenance/Operational Qualification (PM/OQ). Contact Distek's Service Department for more information. The only tubing that Distek recommends to be replaced by the customer is the waste tubing lines. All other media lines should be replaced by a trained professional.
  • Page 64 Chapter 4: Maintenance Contact Distek to obtain a tubing replacement kit. The following procedure describes how to change the waste tubing lines. Figure 4-1: Waste Tubing Replacement Diagram 1. Remove the recycle bin and the rinse tank by lifting the bin upward to disengage the two metal posts located on each side.

  • Page 65: Troubleshooting

    Chapter 5: Troubleshooting Troubleshooting This chapter provides troubleshooting information to identify the most common problems and their solution. Troubleshooting ...............5-2 Error Messages .................5-3 Warning Messages ..............5-6 General Messages..............5-7 Operation Manual: Evolution 4300...
  • Page 66 Pump not responding. Communication with This is usually related the pump is not to the incorrect correct. address set for the pump. See Setting up Communication section on page 2-9or Configuring the Syringe Pump Address (Dual Bath System). Operation Manual: Evolution 4300...

  • Page 67: Error Messages

    Trying to modify It is not possible to NOT MODIFY IT. parameters while the modify parameters pump is busy. while the pump is running. Wait until the pump is not active (idle) and modify the parameters. Operation Manual: Evolution 4300...
  • Page 68 (replacement & recycle). SAMPLING TIME Sampling time Modify the sample INTERVALS ARE intervals are set time point list. INCORRECT. CANNOT smaller than the SAVE IT! minimum allowable interval. Operation Manual: Evolution 4300...
  • Page 69 Make sure the pump is RESPONSE. to detect Pump A. powered on (light power switch). Check the 485 connect from the pump to the samplers. See Setting Up the Power and Communication Connections on page 2-8. Operation Manual: Evolution 4300...

  • Page 70: Warning Messages

    Verification of user deletion. CONFIRM DELETION OF THIS USER. METHOD NAME: “METHOD_NAME” Verification to save method changes. DO YOU WANT TO SAVE THIS METHOD? BATH A/B: “BATH_NAME” Verification to save parameter modifications. DO YOU WANT TO SAVE PARAMETERS? Operation Manual: Evolution 4300...

  • Page 71: General Messages

    Confirmation to overwrite existing _NAME” method. WOULD YOU LIKE TO OVERWRITE BATH_NAME If the Evolution 4300 is configured BATH A/B IS RUNNING. to control an Evolution 6100 or ABORT TEST? 6300 this message will be display when trying to start a method on...
  • Page 72 TERMINATED! BATH TEMP REACHED, CHECK If the instrument is configured to VESSEL TEMP, INTRODUCE DOSAGE control a Distek Model 2100 (B or FORM AND START TEST? C) system the Evolution 4300 will display this prompt when bath temperature has equilibrated. The...
  • Page 73 PUMP X. ACCEPT NEW ADDRESS: change. METHOD “METHOD_NAME” IS This message will appear when a DONE. PUT PROBES INTO DI WATER test has completed giving the user SOURCE, START SYS_WASH! the option to run a SYS_WASH. Operation Manual: Evolution 4300...

  • Page 74: Appendix A : Spare Parts And Accessories

    2910-1801 Sampling Probe, 1800ml for Paddles -Lower 2910-1802 Portion Only Sampling Probe, 1800ml for Baskets-Lower 2910-1803 Portion Only Sampling Probe, 1800ml for Paddles -Solid 2910-1806 Housing Sampling Probe, 1800ml for Baskets-Solid 2910-1807 Housing Return Probe 2910-0001 Operation Manual: Evolution 4300...
  • Page 75 (In the United States, suitable receptacles are supplied by Hubbell, Inc. Alternately, a sized computer-grade Although the Distek Model 4300 is designed with internal surge protection, failure to follow these recommendations may compromise the operation of the system and, should the system be damaged by power surges, lightning or other significant power fluctuations, such system damage is not covered by Distek’s warranty.
  • Page 76 ♦ For those sites whose power quality is compromised either by the nature of the generation source or imposed fluctuations and pulses, an isolation transformer or an on-line UPS may be needed. Operation Manual: Evolution 4300...

  • Page 77: Appendix C : Ce Declaration Of Conformity

    Declared Compliance & Test EMC Directives 89/336/EEC/93/68/EEC Standards: IEC 61326:2002 EN 61000-3-2 EN 61000-3-3 EN 61010-1:2001 (2 Edition) IEC 1010-2-010:92 (as applicable) UL 61010A-1 CAN/CSA 1010.1-92 Jeff Brinker Engineering Manager November 11, 2003 Operation Manual: Evolution 4300...

  • Page 78: Appendix D : Sample Printouts From Parallel Printer

    Appendix D Appendix D : Sample Printouts from Parallel Printer Actual printouts may vary from samples shown. Method Printout DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 01:41:19PM Autosampler Serial Number: 4300001 METHOD USER NAME : DISTEK METHOD NAME: DISTEK METHOD WAS CREATED ON: 08/14/02...
  • Page 79 Appendix D Saved Report Printout DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 01:41:19PM Autosampler Serial Number: 4300001 REPORT USER NAME : DISTEK METHOD NAME: DISTEK DATE: 08/14/02 START TEST AT: 11:48:27AM BATH: 399 SAMPLING: 20.0ml/min AUTO INCLUDES: PASS FILTER: 18.0ml/min FLUSH SAMPLE...
  • Page 80 Appendix D Saved Report Printout – With Distek Premiere 5100 Control DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 01:41:19PM Autosampler Serial Number: 4300001 REPORT USER NAME : DISTEK METHOD NAME: DISTEK DATE: 08/14/02 START TEST AT: 11:48:27AM PUMP PARAMETERS BATH PARAMETER SAMPLING: 20.0ml/min...
  • Page 81 Appendix D Saved Report Printout – With Distek Premiere 5100 Control (continued) ----------------------------------------------------- BATH REPORT DURING THIS TEST: BATH A: 399 RPM RESULTS --------------------- DELTA (MAX-MIN) TEMPERATURE PROFILES -------------------------------------- VES # MAX TEMP. MIN TEMP. DELTA (MAX-MIN) 37.06 37.04 0.02 37.06...
  • Page 82 Appendix D Saved Report Printout – With Distek Model 2100C Control DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 01:41:19PM Autosampler Serial Number: 4300001 REPORT USER NAME : DISTEK METHOD NAME: DISTEK DATE: 08/14/02 START TEST AT: 11:48:27AM PUMP PARAMETERS BATH PARAMETER SAMPLING: 20.0ml/min...
  • Page 83 Appendix D Real Time Test Printout – Single Pump Configuration DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 04:58:19PM Autosampler Serial Number: 4300001 USER NAME : DISTEK METHOD NAME: DISTEK BATH 398 PUMP SERIAL NUMBER: SP00001 SAMPLING: 20.0ml/min PASS FILTER: 18.0ml/min OTHER RATES: 20.0ml/min FLUSH VOL: 03.0ml...
  • Page 84 Pump B on one printout. The information will be divided by the left and right halves of the printout, the left containing Pump A results and the right side will have Pump B results. DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 04:58:19PM Autosampler Serial Number:...
  • Page 85 Appendix D Real Time Test Printout – Single Bath Configuration with Distek Model 2100 Control DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 04:58:19PM Autosampler Serial Number: 4300001 USER NAME : DISTEK BATH: 399 START TEST AT: 04:58:15PM METHOD NAME: DISTEK SAMPLE VOL: 02.0ml...
  • Page 86 Appendix D Real Time Test Printout – Single Bath Configuration with Distek Premiere 5100 Control DISTEK AUTOSAMPLER Firmware V1.3 8/14/02 04:58:19PM Autosampler Serial Number: 4300001 USER NAME : DISTEK BATH: 399 START TEST AT: 04:58:15PM METHOD NAME: DISTEK SAMPLE VOL: 02.0ml...
  • Page 87 Appendix D Real Time Test Printout – Single Bath Configuration with Distek Premiere 5100 Control (Continued) TEMPERATURE PROFILES VES # DELTA TEMP. TEMP. (MAX- MIN) 37.06 37.04 0.02 37.06 37.01 0.05 37.03 37.01 0.02 37.10 37.05 0.05 37.07 37.04 0.03 37.07...
  • Page 88 Appendix D Real Time Test Printout – Dual Bath Configuration with Distek Premiere 5100 and Model 2100 Control In a dual bath configuration the printout will contain data from both Pump A and Pump B on one printout. The information will be divided by the left and right halves of the printout, the left containing Pump A results and the right side will have Pump B results.
  • Page 89 Appendix D Real Time Test Printout – Dual Bath Configuration with Distek Premiere 5100 and Model 2100 Control (continued) METHOD NAME: DISTEK BATH 399 PUMP SERIAL NUMBER: SP00002 SAMPLING: 20.0ml/min PASS FILTER: 18.0ml/min OTHER RATES: 20.0ml/min FLUSH VOL: 03.0ml OFFSET VOL: 02.0ml LINE1 VOL: 02.0ml...
  • Page 90 Appendix D Real Time Test Printout – Dual Bath Configuration with Distek Premiere 5100 and Model 2100 Control (continued) BATH REPORT DURING THIS TEST: BATH A: 398 RPM RESULTS DELTA (MAX- MIN) RPM: TEMPERATURE PROFILES DELTA TEMP. TEMP. (MAX- MIN) TEMP: 36.9...