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SHOKO SCIENTIFIC Shodex RI-201H Operation Manual

Refractive index detector
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Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ Ｍ ａ ｎ ｕ ａ ｌ
Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ
Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ
Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ
Ｒｅｆｒａｃｔｉｖｅ Ｉｎｄｅｘ Ｄｅｔｅｃｔｏｒ
Shodex
READ this operation manual CAREFULLY
READ
READ
READ
8
RI-201H Refractive Index Detector.
Ｍ ａ ｎ ｕ ａ ｌ
Ｍ ａ ｎ ｕ ａ ｌ
Ｍ ａ ｎ ｕ ａ ｌ
R
ＲＩ-２０１Ｈ
CAREFULLY before using
CAREFULLY
CAREFULLY
ＳＴ１２-００３６７-Ａ

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Summary of Contents for SHOKO SCIENTIFIC Shodex RI-201H

  • Page 1 ＳＴ１２-００３６７-Ａ Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ Ｏ ｐ ｅ ｒ ａ ｔ ｉ ｏ ｎ Ｍ ａ ｎ ｕ ａ ｌ Ｍ...
  • Page 2 Copyright 2006-2013, SHOKO SCIENTIFIC CO.,LTD SHOKO SCIENTIFIC CO.,LTD SHOKO SCIENTIFIC CO.,LTD Printed in Japan. SHOKO SCIENTIFIC CO.,LTD All rights reserved. Contents of this publication may not be reproduced in any form or by any means(including electronic storage and retrieval or translation into a foreign language)
  • Page 3 Nothing contained in this manual shall be construed as giving any guarantee any license or immunity under any patent or other rights. Shodex RI-201H Refractive Index Detector must be used on user's own responsibility and in strict compliance with all applicable laws and regulations.
  • Page 4 Precautions Precautions Precautions Precautions 【 Important Important ! ! ! ! 】 Important Important Precautions are divided into three groups in this operation manual depending on the degree of danger. The three groups are Warning Warning Warning Warning Caution Caution Caution Caution Note...
  • Page 5 If the fuse is kept blown off after being replaced, power off Warning Warning the detector immediately and disconnect the power cord. Please consult out local representative in your area or SHOKO SCIENTIFIC. External input/output are for contact closure. Caution Caution Caution Caution Never apply voltage to those.
  • Page 6 Do not use any eluent which might corrode the material, such as Caution Caution Caution Caution stainless steel, that it comes into contact with. Use of such eluent might cause a base line drift and damage the detector. Caution Caution Use a dry cloth to wipe the detector.
  • Page 7 Contents Contents Contents Contents １ １ １ １ ･･･････････････････････････････････ ２ ２ ２ ２ ･･･････････････････････････････････････ ３ ３ ３ ３ ･････････････････････････････････ ４ ４ ４ ４ ････････････････････････････ ･･･････････････････････ ･････････････････････････････ ･･････････････････ ８ ８ ８ ８ ････････････････････ ･･････････････････････････ ･･･････････････････････････ ･･･････････････････････････ ･･･････････････････････････････ 14 14 14 14 ････････････････････...
  • Page 8 1. 1. 1. 1. Accessories Accessories Accessories Accessories 【 Details of Accessories Details of Accessories Details of Accessories Details of Accessories 】 Name Name Name Name Specifi Specifi Specifi Specification cation cation cation Quantity Quantity Quantity Quantity ２ 1-(1) 1-(2) ３...
  • Page 9 2. Features 2. Features 2. Features 2. Features Shodex 1) Stability The double temperature control system The double temperature control system The double temperature control system The double temperature control system 2) Safety 3) Integration - 2 -...
  • Page 10 3. Specifications 3. Specifications 3. Specifications 3. Specifications 1) Construction : Deflection type 2) Refractive Index Range : 1.00 ～ 1.75 3) Range : 0.25 ～ 512 μRIU 4) Linearity : 600 μRIU 5) Noise : 2.5 nRIU or less (Response : 1.5 seconds) : 200 nRIU／ｈ...
  • Page 11 4. Detection Principle 4. Detection Principle 4. Detection Principle 4. Detection Principle 4 4 4 4 - - - - 1 Optical System 1 Optical System 1 Optical System 1 Optical System 1 : Light beam : Refractive index of liquid in sample cell 2 : Sample cell 3 : Reference cell...
  • Page 12 1 : Photo Sensor A 2 : Photo Sensor B 3 : Image 4 4 4 4 - - - - 2 2 2 2 Flow Flow Flow L L L L ine Flow 316 stainless steel tubing Teflon tubing Connection by female nut Connection by flange （Panel）...
  • Page 13 4 4 4 4 - - - - 3 Electronics Circuitry 3 Electronics Circuitry 3 Electronics Circuitry 3 Electronics Circuitry Shodex 1 : Light source 8 : Null glass driver 15 : Solenoid Valve 2 : I/V converters Temperature sensor(internal) 16 : Integrator Output 3 : Keyboard...
  • Page 14 - 7 -...
  • Page 15 5 5 5 5 ..N N N N o o o o me men n n n clature clature and Fu and Func nc nc nct t t t i i i i on on on on clature clature and Fu...
  • Page 16 Name of parts Function □ □ Cancel Cancel Cancel Cancel Cancel Cancel Cancel Cancel □ Enter Enter Enter Enter □ Enter Enter Enter Enter □ □ 5 5 5 5 - - - - 2 2 2 2 Side Panel Side Panel Side Panel Side Panel...
  • Page 17 5 5 5 5 - - - - 3 3 3 3 Back Panel Back Panel Back Panel Back Panel □ □ □ □ □ □ □ □ □ Shodex Name of parts Function □ □ □ □ □ □ □...
  • Page 18 5 5 5 5 - - - - 4 Displ 4 Displ 4 Display ay ay ay 4 Displ - 123.4μRIU 40℃ RD + 2 * PARAMETERS TEMP. UNSTABILIZE * SETTING □ □ □ □ □ Function µ □ □ □...
  • Page 19 - 12 -...
  • Page 20 Enter Enter Enter Enter Enter Enter Enter Enter Table 5 Table 5- - - - 1 Settable Table 5 Table 5 1 Settable 1 Settable parameters 1 Settable parameters parameters parameters Parameter Selectable value Unit Default - 13 -...
  • Page 21 6 6 6 6 ..I I I I n n n n stallation stallation and Co and Con n n n ne ne ne nec c c c t t t t i i i i on on on on stallation stallation and Co...
  • Page 22 6 6 6 6 - - - - 2 Signal cable Connections 2 Signal cable Connections 2 Signal cable Connections 2 Signal cable Connections ) driver ) driver External input/output (Auto Zero-In, Marker-In, Purge-In, Ready-Out, Caution Caution Caution Caution Leak-Out, and Error-Out) are for contact closure. Never apply voltage to those.
  • Page 23 6 6 6 6 - - - - 3 Tube Connections 3 Tube Connections 3 Tube Connections 3 Tube Connections □ □ □ Caution Caution Do not connect any tube other than the provided OUT TUBE to the Caution Caution Eluent outlet joint of the detector.
  • Page 24 6 6 6 6 - - - - 4 Operation Procedures 4 Operation Procedures 4 Operation Procedures 4 Operation Procedures ç Pur r r r ge ge ge ge Pur r r r ge ge ge ge Zero Zero Zero Zero When using organic solvent, wear safety goggles.
  • Page 25 Use a thoroughly degassed eluent. Note Note Note Note It is recommended that a degassing device be used to degas the eluent as it is easy to use and permits continuous degassing. If an eluent is replaced with another eluent in which it is insoluble, Note Note Note...
  • Page 26 Warning immediately and disconnect the power cord. Please consult our local representative in your area or SHOKO SCIENTIFIC CO.,LTD. 7 7 7 7 - - - - 3 3 3 3 Cleaning of detector exterior Cleaning of detector exterior Cleaning of detector exterior Cleaning of detector exterior Use a dry cloth to wipe the detector.
  • Page 27 8 8 8 8 ..Troubleshoot Troubleshooti i i i ng ng ng ng Troubleshoot Troubleshoot Problem Possible cause Solution No power 1. Power cable is not 1. Connect power cable to power socket. connected. (Lamps and displays do not go on when 2.
  • Page 28 Problem Possible cause Solution Large baseline drift 1. Insufficient solvent 1. Replace the solvent thoroughly. replacement. (Refer to the notes in 6-4.) 2. Room temperature 2. Use detector in places where changes fluctuates greatly. in room temperature are small. 3. Bubbles are present in 3.
  • Page 29 9 9 9 9 ..WEEE Instruction WEEE Instruction WEEE Instruction WEEE Instruction ＷＥＥＥ Ｍａｒｋ Please contact your Shodex office or Shodex distributor when Please contact your Shodex office or Shodex distributor when Please contact your Shodex office or Shodex distributor when Please contact your Shodex office or Shodex distributor when the instrument the instrument has reached the end of its life.
  • Page 30 Appendix 1 1 1 1 Appendix Appendix Appendix P P P P r r r r oper opert t t t y y y y Data Data of Solvents of Solvents oper oper Data Data of Solvents of Solvents Flash Boiling Fire Point Polarity...
  • Page 31 Appendix Appendix 2 2 2 2 Appendix Appendix Shodex RI RI RI RI- - - - 2 2 2 2 01 01 01 01H H H H Components and Subassemblies Components and Subassemblies Components and Subassemblies Components and Subassemblies Part Number Part Number Item / / / / Description Item...
  • Page 32 SHOKO SCIENTIFIC CO., LTD. SHOKO SCIENTIFIC CO., LTD. SHOKO SCIENTIFIC CO., LTD. SHOKO SCIENTIFIC CO., LTD. Ｓ Ｓ Ｓ Ｓ ｃｉｅｎｔｉｆｉｃ ｃｉｅｎｔｉｆｉｃ ｃｉｅｎｔｉｆｉｃ Ｉｎｓｔｒｕｍｅｎｔｓ ｃｉｅｎｔｉｆｉｃ Ｉｎｓｔｒｕｍｅｎｔｓ Ｉｎｓｔｒｕｍｅｎｔｓ Ｄ Ｄ Ｄ Ｄ ｉｖｉｓｉｏｎ Ｉｎｓｔｒｕｍｅｎｔｓ ｉｖｉｓｉｏｎ ｉｖｉｓｉｏｎ ｉｖｉｓｉｏｎ Ｆａｃｔｏｒｙ Ｄｅｐａｒｔｍｅｎｔ 1-3-3, Azamino-Minami, Aoba-ku, Yokohama City, Kanagawa 225-0012, Japan...