EYELA SD-1000 Instruction Manual

EYELA SD-1000 Instruction Manual

Spray dryer

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WARRANTY
EYELA products are warranted against defects in materials and
workmanship for a period of year following the date of shipments.
EYELA will make repairs or replacements free of charge upon return to
the factory, transportation paid, of the detective item except following
cases. This warranty does not cover finishes nor does it cover damage
resulting from accident, misuse, abuse, tampering, servicing performed
or attempted by unauthorized service agency.
FOREWORD
Thank you very much for your kind patronage of EYELA. Get to know
your EYELA products, but before using, to be sure to read this manual
well. EYELA cannot be held responsible for the malfunction resulting
from the use of EYELA products other than as specified in this manual.
Nihonbashi Honcho Bldg. 6F, 3-4, 3-chome
Honcho Nihonbashi, Chuo-ku, Tokyo, Japan
Phone: 81/3-5201-6462
Fax:
81/3-3241-0177
Liability Disclaimer
Liability to Tokyo Rikakikai Co., Ltd. for any defect in this instrument is
limited to the invoiced price of the defective instrument. Tokyo
Rikakikai Co., Ltd. has no control over the set-up, use, connection to
other equipment, or data generated by means of EYELA products.
Therefore, in no event shall Tokyo Rikakikai Co., Ltd. be liable for any
incidental or consequential damages, losses, or liability which may result
from improper use of its products, either in connections with other
equipment or in the generation, reporting, or application of data and
results.

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Summary of Contents for EYELA SD-1000

  • Page 1 FOREWORD Thank you very much for your kind patronage of EYELA. Get to know your EYELA products, but before using, to be sure to read this manual well. EYELA cannot be held responsible for the malfunction resulting from the use of EYELA products other than as specified in this manual.
  • Page 2 Instruction Manual Spray Dryer SD-1000 This manual is designed to use this unit safely with the best performance. Read carefully the chapter [For safety operation] before operating this unit. Important Keep this instruction manual beside the unit. Tokyo Rikakikai Co., Ltd.
  • Page 3 Precautions for your safety 1. Warning signal words account function They are classified and defined according characteristic, some parts of this unit will to their risk, and indicated with an alert be heated to high temperature. mark and a signal word. This manual shows precautions for your Please follow these instructions.
  • Page 4 2. Warning label A warning label is attached to the unit to refer the most important clause. The attached position is shown as below. Be careful to use the unit referring warning messages. * When the warning label is worn and hardly show the message, change it with a new one. Please order us a new label.
  • Page 5: Table Of Contents

    Thank you for choosing products. Introduction This instruction manual describes the procedure of installation, operation, trouble shooting, maintenance / check-up, and disposal for Spray dryer model SD-1000. Read this manual carefully before operation. Table of contents 1. For safety operation 2.
  • Page 6: For Safety Operation

    For safety operation This unit is heated to high temperature. This unit is not explosion-proof structure. Be careful to handle safely depending on characteristics of sample. Do not use flammable materials such as organic solvent. Do not use this unit to dry flammable materials such as organic solvent. This unit has a built in heater, so it may ignite.
  • Page 7: Outline

    Outline 2-1 Application Warning Dangerous Do not remodel. Do not use flammable materials Do not use out of applications. such as organic solvent. Do not use this unit to dry flammable materials Remodeling or using out of applications such as organic solvent. may occur electric shock hazard or This unit has a built-in heater, so it may ignite.
  • Page 8: Specifications

    2-3 Specifications Spray dryer SD - 1000 Model Max 1500ml/h Evaporating rate 40 ~ 200°C Inlet temp. control range ±1°C Inlet temp. control accuracy 0.2 ~ 0.75 m /min ( Flow rate is changeable by control knob) Drying air flow rate control range Spraying air press.
  • Page 9: Descriptions

    2-4 Description Pressure sensor Pump for sample Sample flowing tubing (ø3.15 x ø5.2) Sample stirring plate (Magnetic stirrer) Sample flowing tubing (Silicone ø3.7 x ø6.1) Air tubing (ø4 x ø6) Spray nozzle Duct Outlet temperature sensor Connecting tube Cyclone Maintenance port Protection cover (Inlet filter) Evaporation tube...
  • Page 10: Descriptions And Functions Of Control Panel

    Descriptions and functions of the control panel 3-1 Control panel Outlet temp. Drying air Spraying pressure indicator indicator flow rate indicator TEMP. CONTROLLER BLOWER ATOMIZING PUMP  POWER Pump line alarm lamp OUTLET  TEMP. ℃ ;/min ×10 kPa PUMP LINE ALARM Pump operation lamp Inlet temp. indicator Measured value indication Pump switch INLET  TEMP.
  • Page 11 Description Function Drying air flow rate To control drying air volume. ⑩ control knob ⑪ Drying air flow It illuminates when the drying air volume is lower than a alarm lamp certain value. ⑫ RUN/STOP key To start and stop temperature controlling or blower operation. It illuminates while temperature is controlled or blower Temp.
  • Page 12: Safety And Alarm Functions

    3-2 Safety and alarm functions When an abnormal operation occurs, solve it This unit has safety and alarm functions referring to [Trouble shooting] on P.18. as below. Safety function Safety device Function Cause It detects excess current or electric leakage Mains switch Electric leakage or excess (Power breaker)
  • Page 13: Installation

    Installation 4-1 Installed place Warning Do not install at a dangerous circumstance As this unit equips a heater, there is the fear of fire in the dangerous circumstance. Place to be installed. Horizontal flat low humid place where is not exposed to direct sun light, not vibrated, no explosive gas, no corrosive gas or chemical.
  • Page 14: Connection Of Utility

    (1) Check the voltage, phase, current capacity Model Current Voltage of this unit. It is shown in the right table. SD-1000 AC 200V single phase Mains cable (2) Mains plug is not supplied. Connect directly to the switch board. (Do not connect yet .) AC200V single phase AC200V single phase...
  • Page 15: Operation

    Operation 5-1 Preparation Caution Main unit Handle glass wares carefully. Handle glass wares carefully not to ① break down. marking Rectification plate 1. Attaching evaporating tube (1) Loosen screw of lock knob. (2) Place the rectification plate to the Lock knob evaporating tube.
  • Page 16 4. Attaching separator and receiving flask (1) Attach receiving flask cap to the evaporating tube and cyclone. evaporating (2) Attach separator and receiving flask tube to each receiving flask cap. cyclone * Put upper and lower packings to each side of receiving flask cap.
  • Page 17 Pressure sensor (3) Cut 30cm of silicone tubing [ID3.7mm x OD6.1mm, supplied part], and connect it between the pressure sensor and the spray nozzle. Connect the tubing Connect the tubing Spray nozzle 6. Ground for static electricity When you use statical material such as sodium chloride, calcium chloride or other chlorides, connect the cyclone and the receiving flask to the ground terminal with...
  • Page 18: Exhaust Hose

    8. Connecting air tubing (1) Prepare a compressor referring to the section 2-2 Optional accessories. (2) Connect the supplied air tubing to the air tubing connecting port on the right surface of the unit. Insert the tubing completely until it stops. Pull the tubing softly to check whether pull softly the tubing attach completely.
  • Page 19 5-2 Operation Caution Caution While operating unit, When some troubles occur, stop operating immediately. do not touch heated parts. While operating unit, and after operating, When some troubles occur, turn off mains switch immediately, and check the unit the evaporating tube and cyclone are very referring to the chapter [Trouble shooting].
  • Page 20 TEMP. CONTROLLER 4. Temperature controlling and blower operation OUTLET  TEMP. ℃ Press RUN/STOP key for 1 second. Outlet temperature indicator Temp. control and blower operation lamp INLET  TEMP. ℃ illuminates, and temperature controlling and blower operation start. Inlet temperature indicator To stop operation, press RUN/STOP key again HEATING (for 1 sec.).
  • Page 21 TEMP. CONTROLLER 9. Setting outlet temperature OUTLET  TEMP. ℃ (Control of sample flow rate) Outlet temperature indicator (1) Control sample flow rate by control knob INLET  TEMP. ℃ with checking the outlet temperature indicator. Inlet temperature indicator Increase slowly the sample flow rate little by little.
  • Page 22 5-3 Quitting operation Distilled water When the sample vessel is empty, apply immediately another sample, or follow the below procedure. 1. Cleaning of flow line Fill the empty sample vessel with distilled water (about 100ml), and run the pump continuously to clean the silicone tubing and the spray nozzle.
  • Page 23 Trouble shooting Problem Cause Remedy Turn on the breaker on Electric power is not supplied. Indicators do not show switch board. anything, even if the power switch is turned Stop operation immediately Mains switch or power switch and call service. breaks down.
  • Page 24 Problem Cause Remedy The power breaker turns Excess current or electric Stop operation immediately off while operating. leakage. and call service. Control air volume, or clean or Temperature of heater rises The over temperature protector functions while change the filter. If it is not solved extremely because drying air operating, and the heater further, stop operation immediately...
  • Page 25 Maintenance and Check-up 7-1 Cleaning and changing filter Warning Caution Turn off the power before Clean or care the unit cleaning or changing filter. after it is cooled enough. You must turn off the power switch and the mains switch (power breaker) before cleaning Clean or care the unit after it is cooled or changing filter to prevent electric shock enough to avoid burning your hands.
  • Page 26 7-2 Cleaning spray nozzle Caution  、 Take care of tip of needle. Body The tip of needle is very sharp. Be careful Needle not to injure or not to bend or break down it when you drop. Gasket for field cap Body adapter 1.
  • Page 27 7-4 Cleaning and Care Warning Caution Do not take the unit apart. Clean or care the unit after it is cooled enough. There are heating part and electric parts inside of the unit. Clean or care the unit after it is cooled Do not take the unit apart to prevent enough to avoid burning your hands.
  • Page 28 Disposal of unit To dispose the unit, follow the disposal standard of your country. Model Overall dimensions Net weight Main SD-1000 110kg 700W x 620D x 1500H mm unit −23−...

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