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Instruction Manual
CoolSafe100-9 PRO Superior XS
CoolSafe 95-15 PRO Superior XL
© Copyright 2012
LaboGene ApS
Industrivej 6-8
Vassingerød
DK-3540 Lynge.
Tel: +45 3940 2566; Mobil: +45 3016 0990;
Fax: +45 4498 1741
Mail: info@labogene.com;
Internet: www.labogene.com ,
CVR-No.: DK32259154
1/19
Code 9 9.900.900.763
XS XL
U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe
Usermanual-Rev A5.docx
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Summary of Contents for LaboGene SCANVAC CoolSafe100-9 PROSuperior XS
- Page 1 CoolSafe 95-15 PRO Superior XL © Copyright 2012 LaboGene ApS Industrivej 6-8 Vassingerød DK-3540 Lynge. Tel: +45 3940 2566; Mobil: +45 3016 0990; Fax: +45 4498 1741 Mail: info@labogene.com; Internet: www.labogene.com , CVR-No.: DK32259154 1/19 Code 9 9.900.900.763 XS XL U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe Usermanual-Rev A5.docx...
- Page 2 In case you have any comments about this manual we will appreciate receiving them at the address below. Warranty and Liability LaboGene ApS guarantees that the product delivered has been thoroughly tested to ensure that it meets its published specifications. The warranty included in the conditions of delivery is valid only if the product has been installed and used in accordance with the instructions supplied by LaboGene Aps..
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Page 3: Table Of Contents
7.2. Vacuum pump -------------------------------------------------------------- 7.3. Cleaning ---------------------------------------------------------------------- 7.4 Checking for Leaks---------------------------------------------------------- 8. The Freeze-drying process--------------------------------------------------- 8.1 Hints & Tips------------------------------------------------------------------- 8.2 Bibliography------------------------------------------------------------------- 8.3 Pressure Table---------------------------------------------------------------- 9.0 Factory fitted options-------------------------------------------------------- Enclosure: Declaration of conformity 3/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 4: Introduction
Do not handle, move or service the vacuum pump whilst in operation or if it is switched Off, until has cooled down to ambient.(see 7.2 p 13 regarding maintenance & changing of oil) 4/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 5: Installation
CoolSafe via the connection on the rear of the CoolSafe in order to allow cryo pumping. The vacuum pump can be located on the rear panel of the CoolSafe by means of a shelf support. This is located by using the thumb screws provided-see below. 5/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... - Page 6 Check the oil level on the pump and fill it if necessary. The oil level sight glass should be 1/2 - 3/4 full. LaboGene recommends that when the pump is running the gas ballast valve is in the open position.
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Page 7: Functional Description
Browse between the possible variables related to the actual process with the UP-key. The browser is reset to its start position when pressing one of the numerical keys. 7/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... - Page 8 END MENU WITH SAVE AND START (all selections will be saved and activated on start-up and all other modes will be automatically cancelled). Complete the programming sequence by pressing the RIGHT-key. 8/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx...
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Page 9: Operation
It is important to remember following factors when trying to obtain efficient utilization of the freeze dryer system. The efficiency of the freeze drying process depends upon: 9/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 10: Computer Control Option
Entering a zero value for pressure, no pressure regulation is applied, this can be used in the secondary drying phase or if no regulation is required. This protocol also applies when entering values using the PRO controller.. 10/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 11: Preparation
The electronic vacuum valve remains closed until you enter the freeze drying modes (either opened via key pad in manual mode or via programme sequence in automatic mode). 11/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 12: Pre-Freezing & Freeze Drying
“ice-plug”. NB. Always wear cryo-protective gloves when carrying out this procedure If the electric de-icing option is not fitted : 12/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 13: Stopping Vacuum Pump
Keep a Log book of the usage periods. Drain the oil mist filter if the oil level is more than 10 mm. Drain, clean and eventually change the filter insert if vapours are emitted 13/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... -
Page 14: Cleaning
6. Check that the lid of the chamber is located correctly, again check that the seal is OK as previous. 8. The Freeze-drying process 14/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... - Page 15 The heating will initiate sublimation of the moisture from the product to the surrounding environment. The vapour will move to the condenser surface because of the lower vapour pressure in the condenser. 15/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx...
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Page 16: Hints & Tips
Here is list of books & papers that may assist you in your work: Books. An Introduction to Freeze Drying by James M.Flink& Henning Knudsen (ISBN 87-872- 0084-8)1983 Freeze Drying of Food Products by J.C.Harper& A.L.Tappel- Advances in Food Research Vol.7 Academic Press 1957. 16/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... - Page 17 Freeze Drying Foodstuffs; CRC Critical Reviews; Food Technology; Vol.1 issue 3; pages 379-451;September 1970. Freeze Drying Velum Archival Materials; Journal of the Society of Archivists; Vol.14; issue 2; pages 175-188; September 1993. 17/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx...
- Page 18 8.3 Pressure of Aqueous Vapour 18/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx...
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Page 19: Factory Fitted Options
7.001.300.096 PC Control. This includes Mini-PC and software for full control, visual display and operation of the CoolSafe. Also enabling full documentary presentation all the parameters of the freeze drying cycle, including downloading and visualization in a Windows Excel™ . 19/19 Code 9 9.900.900.763 U:\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Manualer-WORD\ScanVac\CoolSafe XL Usermanual-Rev A5.docx... - Page 20 Directive 2006/95/EEC, per August 2007 (Electrical equipment designed for use within certain voltage limits) Directive 2004/108/EEC EMC Electromagnetic compatibility Lynge, December 2011 Finn Kokholm Managing Director LaboGene ApS, Industrivej 6-8, Vassingerød, 3540 Lynge, Denmark \\Server1\data\QA\Manualer\Arkiv\Manuals- Labogene-Origio-GKO\Declarations\WORD-ex- ScanLaf\Declaration-CoolSafe 110-9-95-15 XS & XL-rev.5.docx...
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