Dynisco ViscoIndicator Operation Manual

Rheological sensing for the masses
Hide thumbs Also See for ViscoIndicator:

Advertisement

Quick Links

ViscoIndicator
Rheological Sensing for the Masses
Operations Manual
P/N: 974175
|
Rev: 092019
|
ECO: 50719
www.dynisco.com
-1-

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the ViscoIndicator and is the answer not in the manual?

Questions and answers

Summary of Contents for Dynisco ViscoIndicator

  • Page 1 ViscoIndicator Rheological Sensing for the Masses Operations Manual P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com...
  • Page 2: Table Of Contents

    Rules Screen ..........................31 Wi-Fi Screen..........................32 Overflow Protection Settings ..................... 34 Rules screen (Configurable Machine Protection/Safety Settings) ..........36 Using Activation Energy with the ViscoIndicator ............... 41 ViscoIndicator calibration ......................42 Laboratory Correlation of Results ....................44 Troubleshooting ......................... 45 Warranty ............................
  • Page 3: Safety

    After assembling the stand, install the RCU on the stand before installing the RSU. Installing the RSU to the stand before installing the RCU can make the stand unstable. Take care to follow this assembly order unless the stand has been properly secured. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com...
  • Page 4 1.2 Obligation of the operator to exercise due care The Dynisco component conforms to the state of the art technology and ensures a maximum of safety. In practical operation, this safety can, however, be achieved only if all necessary measures are taken. The obligation of the plant operator to exercise due care includes planning these measures and supervising their execution.
  • Page 5 1.3 Obligation of the personnel to exercise due care The ViscoIndicator melt rheometer may only be operated by persons trained, instructed and authorized to do so. These persons must know the operating instructions and act accordingly. The respective competences of the staff must be clearly determined.
  • Page 6: How To Use This Manual

    How to use this manual Read this manual (Dynisco part number 974175) to understand how to operate the ViscoIndicator. For information on assembly, installation & service of the ViscoIndicator, please see the Assembly, Installation & Service manual (Dynisco part number 975389).
  • Page 7: Abbreviations And System Description

    RCU - Rheometer Control Unit PIV - Process Isolation Valve System Description The ViscoIndicator can provide continuous measurement of melt flow rate, apparent viscosity, or intrinsic viscosity directly on an extruder. Process Connection Material is sampled through a connection port in the extruder and travels up through one (Aux1) or two (Aux1 &...
  • Page 8 General VI System Outline P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com...
  • Page 9: Vi Start Guide

    3-4 minutes, shut off motor and follow step 9. 5.1 One time/infrequent steps 1. If you purchased a cloud account, register at iot.dynisco.com 2. Setup Manager Account pass code 3. Configure Wi-Fi 4.
  • Page 10: Turning The Viscoindicator On/Off

    ON. It may take several minutes for the HMI to fully power up and get to the PV software screen (see following sections describing software function). Turning the ViscoIndicator OFF The ViscoIndicator can be turned off by turning the RCU Power Knob back to the OFF position. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com...
  • Page 11: Operating The Vi Using The Hmi Software

    5. Alarms / Events – History of alarms and variable deviations 6. Permissions – Allows different levels of machine access depending on operator level 7. Help – VI Help information 8. Settings – Machine specific settings P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -11-...
  • Page 12: Pv Screen

    – denotes heat is on, but at least one temp zone is outside the limits in the recipe. · green - denotes heat is on, and all temp zones are within the limits in the recipe P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -12-...
  • Page 13 · Field Service - 4 digit login code required - Used by Dynisco field service personnel only. 4. Current Recipe – Displays name of recipe that is currently running. A recipe consists of material specific parameters that are followed (temperatures, motor speed, etc.) while running a...
  • Page 14: Plot Screen

    The lower and upper values displayed on the Y axis are fixed and are shown as red lines. They are equal to the lower and upper limits in the current recipe for the plotted variable. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -14-...
  • Page 15: Machine State

    NOTE: motor speed set point only controls the motor speed in speed control mode 4- Current pressure / pressure set point NOTE: pressure set point only controls the pressure in pressure control mode 5- PIV temperature / set point P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -15-...
  • Page 16 7- Auxiliary 2 temperature / set point (if Auxiliary 2 zone is enabled) 8- Flow block temperature / set point 9- Die characteristics (Length and Inner Diameter) NOTE: The Length and inner diameter of the die can only be changed in the machine settings P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -16-...
  • Page 17: Recipes Screen

    5- New Recipe button- Makes a copy of the selected recipe. The new recipe name will have the same name as the selected recipe except several random digits will be appended to the name. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -17-...
  • Page 18 8- Export Recipes button – If a USB memory stick is attached to the HMI housing, pressing this button will export all recipes to the memory stick. 9- Import Recipes button – Imports recipes from a memory stick into the ViscoIndicator’s memory.
  • Page 19 VI process connection location · Temperature set points control the temperature of the polymer during VI rheological measurements and therefore can affect calculated IV/MFR values. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -19-...
  • Page 20 Default value equal 190C for typical ASTM MFR test Activation energy - Please see "Using Activation Energy with the ViscoIndicator" section later in this guide for a description on how activation energy is used in to correct for differences in melt flow and viscosity due to temperature differences between the ViscoIndicator and laboratory equipment.
  • Page 21 IV coefficient - Value of the IV coefficient term used is IV calculation (Default value = 0.2157) IV exponent - Value of IV exponent term used in IV calculation. (Default value = 0.2147) P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -21-...
  • Page 22 If while the motor is on the VI pressure falls below 12psi for more than 1 minute the motor will shut off. See troubleshooting section if rule 10 occurs repeatedly making it difficult to run the VI. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -22-...
  • Page 23: Alarms / Events

    1- Events List - Scrollable list of past events since last time list was cleared (the most recent events are at the bottom of the screen) 2- Clear button - current list of events 3- Exports events button - to memory stick connected to HMI enclosure P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -23-...
  • Page 24: User Permissions

    User Permissions The user permissions screen is used to change access to the ViscoIndicator’s functions. There are three access levels - Operator, Manager and Field Service. Various functions are only accessible to manager or field service access levels. The VI system will automatically logout of manager level access after 60 minutes if the display is not touched 1.
  • Page 25: Help

    Help The help screen contains information on operation of the ViscoIndicator in a HTML format. Please refer to the Operation manual, not the Help screen, for the most current information on operating the VI. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com...
  • Page 26: Settings Screen

    2. Calibration Screen – Access to and pressure calibration and Rules, as well as temperature calibration and Field Service screens only used by Dynisco Field Service personnel 3. WIFI – Screen for configuring the VI WIFI/Ethernet connection required for cloud data 4.
  • Page 27: Machine Screen

    NOTE - only values inside a text box can be changed (some machine settings are fixed at the factory) Company Name – Owner of the ViscoIndicator Machine Name - Descriptive name of machine Serial Number –...
  • Page 28 Pressure PID P, I, D - PID parameters for driving pressure control (Factory Set) Simulation Mode – Reads data from internal file instead of taking active measurements Leave in OFF position Calibration Mode – Displays raw sensor readings without scaling Leave in OFF position P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -28-...
  • Page 29: Calibration Screens

    This screen gives access to the Pressure calibration and the Rules screens, as well as Temperature calibration and Field Service screens, which are used only by Dynisco Field Service Personnel. To access the Pressure or Rules screens, touch the text at the top of the screen...
  • Page 30: Pressure Screen (Calibrating The Pressure Transmitter)

    5. Press the green text Rcal button again (the button text color should change back to red) 6. Press the Save Values button (this must be done or the measured values will be lost) P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -30-...
  • Page 31: Temperature And Field Service Screens

    Temperature and Field Service Screens These screens give access to temperature calibration and Field Service functions. Temperature calibration and Field Service should only be carried out by Dynisco field service personnel. Rules Screen See separate rules section later in this manual...
  • Page 32: Wi-Fi Screen

    The VI is an industrial machine that connects a computing device and embedded sensors. The VI is able to efficiently collect and send sensor and rheological data. It utilizes Microsoft Azure services to collect and archive data in the cloud platform (across a global network of Microsoft-managed datacenters). P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -32-...
  • Page 33 Windows IoT, only one application can run at a time. Communication is only in one direction from the ViscoIndicator to the server (the VI doesn't accept data from the network), and all data that is sent out is encrypted and compressed, using Microsoft APIs. Server-side security is administered by Microsoft.
  • Page 34: Overflow Protection Settings

    2- Overflow Protection Toggle - Turns overflow protection on or off (any change is also reflected in the Rules screen) 3- email address box - When the timer expires, the ViscoIndicator can send an email to the specified address (NOTE: this feature is not active in the current software version)
  • Page 35 4- Receive System emails toggle - Turns Receiving emails on/off (NOTE: this feature is not active in the current software version) P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -35-...
  • Page 36: Rules Screen (Configurable Machine Protection/Safety Settings)

    These rules exist to help prevent unsafe conditions or machine damage. When triggered, each rule can change the state of the ViscoIndicator or simply display an informational message on the status screen. Rules can be individually enabled/disabled with a user permission level of manager.
  • Page 37 Stop motor when clear extrudate Motor running Please confirm that you reminder is for 10 minutes change of have cleared extrudate ignored Motor on after warning Yes? state before restarting motor P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -37-...
  • Page 38 RCU is provided with a 2-wire 24V signal when the screw is turning, which changes to a 0V signal when the screw is not turning. Please consult Dynisco for more details. If this signal cannot be provided/isn't setup, rules 6 thru 8 must be turned off to operate the VI.
  • Page 39 10 seconds is too viscous (pump damage) Protect Pressure Motor Pressure No change Invalid Pressure transmitter from above recipe of state reading overpressure upper limit (Pressure transmitter damage) P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -39-...
  • Page 40 RTD malfunction or just Heat zone Protect machine Motor off, Motor off Heat shut off from polymer heat on for 16 hours due to inactivity degradation if at temperature but not operating P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -40-...
  • Page 41: Using Activation Energy With The Viscoindicator

    Using Activation Energy with the ViscoIndicator Often, the temperature at which the polymer is being processed at is not the same as the test temperature used in the lab to verify the melt flow index. A polymer’s melt flow index is dependent upon its temperature. Therefore, if the polymer is processed at a different temperature from the lab, there can be a difference in melt flow indexes.
  • Page 42: Viscoindicator Calibration

    ViscoIndicator calibration Dynisco recommends the following steps: 1- Run the VI in “Pressure Mode” setting the pressure set point equal to the standard pressure from ASTM standard weight for the material. 2- Once the pressure on the PV screen matches the set point, read the value of pump speed from the screen.
  • Page 43 . The expected extrudate weight would be: = 0.663 ∗ 7 ∗ .5 = 2.32 Deviation from this value, by more than a couple of percent can be caused by errors in the melt density value. P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -43-...
  • Page 44: Laboratory Correlation Of Results

    The ViscoIndicator allows for this with a correlation factor which is a simple scalar that can be used for individual materials, if needed. It’s difficult to predict whether this factor will be needed or not. A material’s elasticity may show the need for using a correlation factor but sometimes it doesn’t affect the...
  • Page 45: Troubleshooting

    0 psi, speed mode, and run at 1/4 normal speed, recipe time period carefully watch pressure build up for 3-4 minutes. If pressure begins to build up, then switch back to original recipe P/N: 974175 Rev: 092019 ECO: 50719 www.dynisco.com -45-...
  • Page 46 Fault Possible Cause Resolution Lab Results vs. See Section 27—Laboratory Correlation of Results ViscoIndicator Results may need correlated. Result on See Section 25--Using Activation Energy with the ViscoIndicator ViscoIndicator. doesn’t correlate Activation energy needs to with LMI. be entered into the recipe.
  • Page 47: Warranty

    As the guarantee period, DYNISCO grants a 12-month guarantee from the date of delivery, when the ViscoIndicator is used in single-shift operation. If it is used in multiple-shift operation, the duration of the guarantee is reduced to 6 months.

Table of Contents