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Agilent Technologies 16452A Operation And Service Manual
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Agilent Technologies 16452A Operation And Service Manual

Liquid test fixture
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Agilent 16452A Liquid Test Fixture
Operation and Service Manual
Agilent Part No. 16452-90000
Printed in JAPAN January 2000
Third Edition

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Summary of Contents for Agilent Technologies 16452A

  • Page 1 All manuals and user guides at all-guides.com Agilent 16452A Liquid Test Fixture Operation and Service Manual Agilent Part No. 16452-90000 Printed in JAPAN January 2000 Third Edition...
  • Page 2 All manuals and user guides at all-guides.com Notice...
  • Page 3 All manuals and user guides at all-guides.com Manual Printing History : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : :...
  • Page 4 All manuals and user guides at all-guides.com Safety Summary WARNINGS The Agilent Technologies assumes no liability for the customer's failure to comply with these requirements. DO NOT Operate In An Explosive Atmosphere Keep Away From Live Circuits DO NOT Service Or Adjust Alone...
  • Page 5 All manuals and user guides at all-guides.com Operating Precaution Caution Certi cation Warranty Instrument Speci cations...
  • Page 6 All manuals and user guides at all-guides.com Limitation Of Warranty No other warranty is expressed or implied. Agilent Technologies speci cally disclaims the implied warranties of merchantability and tness for a particular purpose. Exclusive Remedies The remedies provided herein are buyer's sole and exclusive remedies. Agilent Technologies shall not be liable for any direct, indirect, special, incidental, or consequential damages, whether based on contract, tort, or any other legal theory.
  • Page 7 All manuals and user guides at all-guides.com Safety Symbols Warning Caution Note...
  • Page 8 All manuals and user guides at all-guides.com Typeface Conventions Italics copy lename copy file1 Computer HARDKEYS NNNNNNNNNNNNNNNNNNNNNNNNNN NNNNN SOFTKEYS viii...
  • Page 9 All manuals and user guides at all-guides.com Contents 1. General Information 2. Initial Inspection 3. Operation Contents-1...
  • Page 10 All manuals and user guides at all-guides.com 4. Service A. Liquids that Corrode the Test Fixture Contents-2...
  • Page 11 All manuals and user guides at all-guides.com Figures Tables Contents-3...
  • Page 12 All manuals and user guides at all-guides.com...
  • Page 13 All manuals and user guides at all-guides.com General Information Introduction Manual Summary Product Description Applicable Instrument General Information...
  • Page 14 Accessories Furnished Accessories Recommended Measurement Cables These cables are not furnished with the 16452A. Order according to your measurement requirements. Speci cations Electrode Size : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : ...
  • Page 15 All manuals and user guides at all-guides.com Operating Frequency : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : :...
  • Page 16 All manuals and user guides at all-guides.com Supplemental Performance Characteristics Electrode gap repeatability : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : Necessary liquid volume : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : : :...
  • Page 17 All manuals and user guides at all-guides.com Figure 1-2. Fixture Error (A) Figure 1-3. Fixture Error (B) Figure 1-4. Fixture Error (A+B) General Information...
  • Page 18 All manuals and user guides at all-guides.com...
  • Page 19 All manuals and user guides at all-guides.com Initial Inspection Introduction Initial Inspection...
  • Page 20 All manuals and user guides at all-guides.com Product Overview Figure 2-1. 16452A Product Overview Initial Inspection...
  • Page 21 Part Number Quantity Designator The O-rings are assembled in the 16452A. The 1.3 mm spacer is assembled in the 16452A. The cap is on the SMA-BNC adapter. Operation and Service Manual The carrying case and the are not shown in the Figure 2-1.
  • Page 22 All manuals and user guides at all-guides.com Repackaging the Test Fixture For Shipment FRAGILE Initial Inspection...
  • Page 23 All manuals and user guides at all-guides.com Operation Introduction " Measurement Sequence " Measurement Requirements Operation...
  • Page 24 All manuals and user guides at all-guides.com Preparation of Test Fixture for Use Connecting the SMA-BNC Adapters to the 16452A Figure 3-1. Connecting the SMA-BNC Adapter Operation...
  • Page 25 All manuals and user guides at all-guides.com Separating the Test Fixture into High and Low Electrodes Figure 3-2. Separating the Test Fixture into High and Low Electrodes Cleaning and Drying the Electrodes Caution Operation...
  • Page 26 All manuals and user guides at all-guides.com Assembling the Test Fixture Figure 3-3. Assembling the Test Fixture for a SHORT Compensation Putting the Lid On the Liquid Outlet Figure 3-4. Putting the Lid On Operation...
  • Page 27 All manuals and user guides at all-guides.com Connecting the Test Fixture Using the 4194A Figure 3-5. Cable length switch (4194A) Figure 3-6. Connecting the Test Fixture (4194A) Operation...
  • Page 28 All manuals and user guides at all-guides.com Using the 4284A/4285A NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN CORRECTION MEAS SETUP CABLE : NNNNNNNN 4284A/4285A Operation Manual Figure 3-7. Connecting the Test Fixture (4284A/4285A) The 16452-61601 cable can be used in the same manner as the 16048A cable with 4284A/4285A. Operation...
  • Page 29 All manuals and user guides at all-guides.com Fixture Stand Usage Figure 3-8. Fixture Stand Usage Operation...
  • Page 30 All manuals and user guides at all-guides.com Checking the SHORT Residual Using the 4194A NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN OPEN OFS on/off COMPEN NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN SHRT OFS on/off COMPEN NNNNNNNNNNNNNNNNNNNNNNNNNNNNN NNNNNNNNNNNNNNNNN IMPEDANCE Ls-Rs FUNCTION NNNNNNNNNNNNNN NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN menu AUTO SCALE A DISPLAY NNNNNNNNNNNNNNNNNNNNNNNNNN NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN more 1/3 AUTO SCALE B REPEAT <...
  • Page 31 All manuals and user guides at all-guides.com If the SHORT Residual is Out of Range Setting the Instrument for Capacitance Measurement " " Using the 4194A NNNNNNNNNNNNNNNNNNNNNNNNNNNNN NNNNNNNNNNNNNNNNNNNNNNNNNN NNNNNNNNNNNNNNNNNNNNNNNNNN NNNNNNNNNNNNNNNNN IMPEDANCE more 1/3 more 2/3 Cp-Rp FUNCTION Using the 4284A/4285A FUNC NNNNNNNNNNNNNNNNN Cp-Rp...
  • Page 32 All manuals and user guides at all-guides.com Performing a SHORT Compensation Note Using the 4194A NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN ZERO SHORT COMPEN ENTER/EXECUTE NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN SHRT OFS ON Note REPEAT Using the 4284A/4285A NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN CORRECTION MEAS SETUP SHORT NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN MEAS SHORT NNNNNNNN 3-10 Operation...
  • Page 33 All manuals and user guides at all-guides.com Air Capacitance (C ) Measurement Figure 3-9. Separating the Test Fixture into High and Low Electrodes Figure 3-10. Test Fixture Assemble for Measurement Operation 3-11...
  • Page 34 All manuals and user guides at all-guides.com Note Liquid Capacitance and Resistance (Cp, Rp) Measurement Warning Be careful when dealing with liquids (especially volatile and/or ammable liquid such as oil or organic solvents) that can cause an accident. Accidents such as an explosion, ignition, emission of poison gas, scalding (by heat or chemicals), and so on, are possible To prevent any accidents, establish a strict process for the measurements.
  • Page 35 DO NOT enclose the liquid in the 16452A. Carburetion of the liquid enclosed in the 16452A can cause an explosion of the 16452A. Warning DO NOT apply a dc test signal to the 16452A. The dc signal can cause electrolysis of the liquid. Operation...
  • Page 36 All manuals and user guides at all-guides.com Drain the Liquid (After Measurement) Figure 3-12. Taking the Lid O 3-14 Operation...
  • Page 37 All manuals and user guides at all-guides.com Data Processing|Calculate Dielectric Parameter from Measurement Data " " " Measurement Theory " " " " " " " 0 j" 00 " " 00 " 0 " 0 " 00 Capacitive Measurement Method "...
  • Page 38 All manuals and user guides at all-guides.com Correction Coecient Figure 3-13. Stray Capacitance " " Figure 3-14. Correction Coecient " " " 3-16 Operation...
  • Page 39 All manuals and user guides at all-guides.com Performing Temperature Measurements Figure 3-15. Soaking the 16452A in the Oil Tank Warning DO NOT touch the heated test xture, cable, and xture stand with your naked hand. Use gloves to prevent scalding.
  • Page 40 All manuals and user guides at all-guides.com...
  • Page 41 All manuals and user guides at all-guides.com Service Introduction Warning These servicing instructions are for use by quali ed personnel only. Do NOT perform any servicing (other than that contained in the operating section) unless you are quali ed to do so. Assembly Replacement Service...
  • Page 42 All manuals and user guides at all-guides.com Figure 4-1. 16452A Replaceable Parts (Major Parts) Table 4-1. Replaceable Parts (Major Parts) Ref. Agilent Part Desig. Number Qty. Description Assembling procedure of the electrode is described later in this chapter. Service...
  • Page 43 All manuals and user guides at all-guides.com Table 4-2. Replaceable Parts (Other parts) Agilent Part Number Qty. Description Service...
  • Page 44 All manuals and user guides at all-guides.com Electrode Assembly Figure 4-2. 16452A Replaceable Parts (Around SMA Connector) Table 4-3. 16452A Replaceable Parts (Around SMA Connector) Ref. Agilent Part Desig. Number Qty. Description Service...
  • Page 45 All manuals and user guides at all-guides.com Figure 4-3. Inside of the Electrode Assembly Assembling Procedure for Electrode Service...
  • Page 46 All manuals and user guides at all-guides.com Troubleshooting Caution Service...
  • Page 47 All manuals and user guides at all-guides.com Liquids that Corrode the Test Fixture Nickel Corrosive Liquid Corrosive liquid Little-corrosive liquid Non-corrosive liquid In the case of high temperature and air-mixed. Liquids that Corrode the T est Fixture...
  • Page 48 All manuals and user guides at all-guides.com Ceramic (alumina : Al ) Corrosive Liquid Viton (Fluoro rubber) Corrosive Liquid Silver-copper and gold-copper Liquids that Corrode the T est Fixture...