Related Manuals for Hach POLYMETRON 8810
Summary of Contents for Hach POLYMETRON 8810
- Page 1 DOC024.52.93057 POLYMETRON Model 8810 ISE Analyzer User Manual 05/2015, Edition 19...
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Page 3: Table Of Contents
Table of Contents Section 1 Specifications ........................3 1.1 Dimensions..........................4 Section 2 General information ......................7 2.1 Safety information........................7 2.2 Use of hazard information......................7 2.3 Precautionary labels ........................7 2.4 EMC compliance statement (Korea).................... 8 Section 3 Product overview ...................... - Page 4 Table of Contents 6.7 Chemical cleaning (CLEANING option)..................30 6.8 Sample conditioning (SAMPLE COND option)................31 6.9 View calibration details (CAL PARAMETER option)..............31 6.10 Measurement cycle parameters (TIMING option)..............31 Section 7 Maintenance and Troubleshooting ................33 7.1 Maintenance..........................33 7.1.1 General..........................33 7.1.2 Maintenance schedule......................
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Page 5: Section 1 Specifications
Section 1 Specifications Specifications are subject to change without notice. Specification Details Ambient temperature 5 - 40 °C (41 - 104 °F) Relative humidity 10 to 80% Operating altitude From 0 to 2,000 m. (6,550 ft.) above sea level Mains power supply 110/220/240 VAC, 50/60 Hz, ±... -
Page 6: Dimensions
Specifications 1.1 Dimensions Figure 1 Panel dimensions (mm [inches]) - Page 7 Specifications Figure 2 Cabinet dimensions (mm [inches])
- Page 8 Specifications...
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Page 9: Section 2 General Information
Section 2 General information In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential damages resulting from any defect or omission in this manual. The manufacturer reserves the right to make changes in this manual and the products it describes at any time, without notice or obligation. -
Page 10: Emc Compliance Statement (Korea)
General information Products marked with this symbol indicates a risk of finger pinch. This symbol, when noted on the product, indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken to prevent damage to them. This symbol, when noted on a product, indicates the instrument is connected to alternate current. -
Page 11: Section 3 Product Overview
Section 3 Product overview 3.1 Analyzer overview Figure 3 Front and rear view (panel mount illustrated) 1 Electronic unit 7 Space for additional pump 13 Power supply connection 2 Measurement chamber (see 8 Input/Output connections 14 Rinse valve Figure 4 on page 10) 3 19 inch panel 9 Reagent pump cover... -
Page 12: Measurement Chamber
Product overview 3.2 Measurement chamber Figure 4 Measurement chamber components 1 Stirrer motor 4 Electrode cable 7 Drain tubing 2 Measurement chamber cover 5 Siphon 8 Overflow pipe 3 Electrode 6 Drain valve 9 Threaded fittings 3.3 Features The measurement chamber has mounting locations for: •... -
Page 13: Section 4 Installation
Section 4 Installation D A N G E R Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document. Mains power should only be connected once installation has been completed and checked. 4.1 Unpacking Carefully remove the analyzer and its accessories from the box and packing material, referring to the packing list included to confirm that everything has been delivered. -
Page 14: Hydraulic Connections
Installation 4.3 Hydraulic connections D A N G E R Chemical or biological hazards. If this instrument is used to monitor a treatment process and/or chemical feed system for which there are regulatory limits and monitoring requirements related to public health, public safety, food or beverage manufacture or processing, it is the responsibility of the user of this instrument to know and abide by any applicable regulation and to have sufficient and appropriate mechanisms in place for compliance with applicable regulations in the event of malfunction of the instrument. -
Page 15: Cable Preparation
Installation 4.5.1.1 Cable preparation W A R N I N G To conform with security standards and to respect the EMC compliancy of the analyzer, this procedure must be followed for all user supplied cables before connecting them to the electronic unit of the analyzer. -
Page 16: Connecting Peripherals
Installation 2. Remove 8 cm of the outer cabling to reveal the braided shielding. 1. Place the nut and metal seal of the cable gland onto the shielded cable. 3. Remove all but 12 mm of the shielding to reveal the interior wires, then roll the remainder of the shielding back over the cable. - Page 17 Installation 2. Take the cable, unscrew the threaded part and remove it. 1. Select an unused opening nearest to the cable connection on the electronic 3. Screw the threaded part into the board. Remove the screw and nut electronic unit opening selected in step combination and set aside the screw 1 using the nut removed in step 1 to for later use.
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Page 18: Electrode Connections
Installation 4.5.1.3 Electrode connections W A R N I N G To conform with security standards and to respect the EMC compliancy of the analyzer, this procedure must be followed when connecting selective, reference, combined and temperature electrodes to the electronic unit of the analyzer. Before being connected to the terminal block of the measurement board, electrode cables must pass through ferrite blocks to minimize the risk of outside interferences that could cause erroneous measurement data. -
Page 19: Mains Power Supply
Installation Figure 6 Reference electrode and temperature sensor connections 4.5.2 Mains power supply D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before making electrical connections. The analyzer is factory configured to either 110, 220 or 240 VAC. -
Page 20: Input/Output Connections
Installation 4.5.3 Input/Output connections D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before making any of the connections in this section. W A R N I N G To conform with security standards and to respect the EMC compliancy of the analyzer, follow the procedures defined in Wiring procedures and cable preparation... - Page 21 Installation Table 2 Level detector and external commands (J1 - J8) Terminal Start / Standby External sample Not used Conditioning solution Titration solution Calibration solution Chemical cleaning Sample Table 3 Analog outputs (J9) Terminal Analog output 1 Analog output 2 Analog output 3 Analog output 4 9-10...
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Page 22: Alarms
Installation Table 6 Accessories 2 (J14) Terminal 1-11 (8-10) Automatic calibration or external sample pump (connect 8 and 10 and set jumper X4 at 2-3) Extra channel Chemical cleaning valve Dilution valve Not used 10-11 Pump 4 12-13 Pump 3 (X3 set at 1-2 and 3-4) 14-15 Pump 2 (X2 set at 1-2 and 3-4) 16-17... -
Page 23: Rs232 Connection
Installation J4, J5, J6 and J7 Terminal number Color Not used Not used Brown White 4.5.3.5 RS232 connection Refer also to Figure 8 on page 18 and Table 4 on page 19. Wire the connection to J10 as follows: J10 Terminal number DB9 Plug DB25 Plug 1 (TXD) -
Page 24: Additional Accessories
Installation SYSTEM ERRORS LEVEL SAMPLE Sample missing from measuring cell OVER TITR TIME Titration time is too long ERROR CALIB Automatic calibration error WARNINGS LEVEL REAGENT Titration reagent missing LEVEL COND Conditioning reagent missing LEVEL CALIB Calibration solution missing LEVEL CLEANING Cleaning solution missing RETURN PROCESS After an external sample measurement, this message indicates a return to process measurement... -
Page 25: Section 5 User Interface
Section 5 User interface 5.1 Front panel description The interface is via a 4-key keyboard, a 4-digit numeric display and an alphanumeric display of 2-lines of 16 characters. Figure 9 Front panel 1 Numeric display 4 Scroll up key 2 Select key 5 Enter key 3 Alphanumeric display 6 Scroll down key... - Page 26 User interface • Operating mode: The top line indicates units, measurement type and any activated alarms. The bottom line indicates the analyzer status, e.g. calibration, titration, etc. • Command mode: The top line indicates the main menu. The bottom line indicates submenus and data settings.
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Page 27: Section 6 Menu Overview
Select the unit of concentration from the list available. Selecting USER allows you to define your own, and requires a 5 character description. Adjust ADC This option is reserved for Hach Lange service technicians. Two-point temperature calibration. Use a temperature simulator for TEMPERATURE each of the two points. -
Page 28: Calibration (Calibration Option)
Menu overview Option Description OPTION From the list available, select YES for those additional options that have been installed and NO for those not installed. For correct operation of the analyzer, any hardware installations must have been completed before setting the option to YES. AUTOMAT.CAL - Automatic calibration. -
Page 29: Process Calibration
Menu overview 4. FILL BUFFER 2 is displayed. Pour the second calibration solution into the measurement chamber and press Enter. 5. CONC 2 XX.XXEXX is displayed. Enter the calibration solution concentration and press Enter. The solution is then measured before the measurement chamber is then cleaned. -
Page 30: Calibration Results
Menu overview Option Description C. Ini Adjust the concentration of the solution before the addition if necessary. C. End Adjust the concentration of the solution after the addition if necessary. 6. If the CAL PUMP NO or the Use Default Parameters option has been selected: Option Description ADD C... -
Page 31: Set The Alarms And Thresholds (Alarm Option)
Menu overview 1. Select ANALOG-OUT with the scrolling keys and press Enter. Select the type of analog output: Option Description LINEAR Linear output LOGARITHMIC Logarithmic output DUAL RANGE Bilinear output 2. If linear output is selected: Option Description START XX.XXEXX Define the concentration corresponding to the 0 or 4 mA current for the start of output scale 1. -
Page 32: Measurement Mode (Sequence Option)
Menu overview Option Description WARNING/R1 YES/NO Define the alarm allocation (see table above). ALARM 1/2 ON/OFF Activate or deactivate alarms 1 and 2. ALARM 1/2 HIGH/LOW If activated, define if the trigger is a high or low measurement value. ALARM 1/2 XXX Enter the threshold value. -
Page 33: Sample Conditioning (Sample Cond Option)
Menu overview Option Description REAG. INJ Define the duration (in seconds) that the cleaning solution is injected into the measurement chamber. RESIDENC. Define the duration (in seconds) that the cleaning solution remains in the measurement chamber. 6.8 Sample conditioning (SAMPLE COND option) This option is displayed only if the SAMPLE COND option has been activated. - Page 34 Menu overview...
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Page 35: Section 7 Maintenance And Troubleshooting
Section 7 Maintenance and Troubleshooting 7.1 Maintenance D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before carrying out any maintenance on the analyzer. 7.1.1 General For periodic maintenance, all the elements are freely accessible on the front panel. For installation of accessories and specialized service work the analyzer is easily accessible from all sides with some simple manipulations. -
Page 36: Shutdown
Maintenance and Troubleshooting If needed, clean the exterior of the instrument with a moist cloth and a mild soap solution. Never use cleaning agents such as turpentine, acetone or similar products to clean the instrument, including the display and any accessories. 7.1.5 Shutdown Stopping the measurement cycle Select STOP in the main menu and press Enter. - Page 37 Maintenance and Troubleshooting Malfunction Possible cause Corrective action Check sample flow > 40 L/minute Sample flow or no sample Check air pressure 4 - 7 bars flow in the measurement cell Check the valves are working Electrode connections Check all electrode connections Check measurement cycle No analysis results parameters...
- Page 38 Maintenance and Troubleshooting...
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Page 39: Section 8 Additional Options
Section 8 Additional options The following options can be added to the analyzer to increase performance: • Reagent pump - 2 point automatic calibration • Reagent pump - 1 point automatic calibration • Reagent pump - Sample conditioning 1 • Reagent pump - Sample conditioning 2 •... -
Page 40: Automatic Calibration
Additional options 8.1 Automatic calibration This option allows the analyzer to perform an automatic calibration at programmed intervals and with a known calibration solution. Three different kits are available, each including a 10 liter canister equipped with level detector and strainer: 1. -
Page 41: Two Point Calibration With A Micro Piston Pump
Additional options 8.1.2 Two point calibration with a micro piston pump D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before installing this option. To install the pump, refer to Micro piston pump on page 47. -
Page 42: Conditioning
Additional options ® 5. Connect the other end of the Tygon tubing to the connector marked OUT on the pump box. 6. Remount the transparent cell to its cover. ® 7. Connect Tygon tubing (4) between the connector marked IN on the pump box and the canister of cleaning solution. - Page 43 Additional options Figure 13 Rinsing and dilution assembly In the above illustration the rinsing system is shown on the left and the dilution system on the right. 1 Input block (already installed on the 8 PE tubing 4/6 15 PE tubing 3.2/6.4 analyzer) 2 Sample valve (already installed on 9 Outlet tubing 3/5...
- Page 44 Additional options Note: For optimal performance, the minimum rinse water pressure should be 2.5 bar. Install the dilution assembly as follows (the numbers in brackets refer to Figure 13): 1. Install the control valve on the panel (position 4 in Figure 10 on page 37).
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Page 45: External Sample
Additional options 8.5 External sample D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before installing this option. This option allows the analyzer to measure an external sample without modifying the process parameters. -
Page 46: Heating System
Additional options To invoke the external sample measurement, use the switch provided. At the end of the measurement, if the switch has not been reset to its initial status, a warning message is displayed. 8.6 Heating system D A N G E R Electrocution hazard. -
Page 47: Reagent Pumps
Additional options Figure 16 Extra channel option 1 First sample input 4 Second sample valve 7 Tubing to link the two channels 2 First sample valve (already mounted 5 Second sample input 8 Electric cable for second sample on the analyzer) valve 3 T-bar connection for both sample 6 Compressed air inlet connector... -
Page 48: Peristaltic Pump
Additional options 8.8.1 Peristaltic pump D A N G E R Electrocution hazard. Always make sure the analyzer is turned off and power is disconnected before installing this option. The peristaltic pump is a compact tubular pump with a constant output. The flow rate is determined by the diameter of the tube being used (see Table 8). -
Page 49: Micro Piston Pump
Additional options 1. Remove the pump cover. 2. Mount the pump on the front of the panel in one of the available slots (see Figure 10 on page 37) using the 2 screws. 3. Replace the cover on the back of the panel using the 4 screws. ®... -
Page 50: Pulse Pump
Additional options ® 4. Connect Tygon tubing from the pump (2) to the measuring cell. ® 5. Connect Tygon tubing from the pump (1) to the reagent canister. 6. Connect the pump cable (4) to the electronic unit according to the pump function (refer to Table 6 on page 20 and... -
Page 51: Section 9 Spare Parts
Section 9 Spare parts Note: Where mentioned in the following tables, Version 1 refers to any 8810 analyzer delivered before June 2012 and Version 2 to any 8810 analyzer delivered after 1 June 2012. Controller Description Item no. Version 1 complete controller 359110,30000 Version 2 complete controller (110V) 359110,50000... - Page 52 Spare parts Reagent pumps (continued) Description Item no. Grey pump tubing 359090,70015 Green pump tubing 359090,70020 Violet pump tubing 359090,70021 24 VAC 50 Hz micro pump equipped (batch, level detector, reagent tubing) 368810,71050 24 VAC 60 Hz micro pump equipped (batch, level detector, reagent tubing) 368810,71060 24 VAC 50 Hz micro pump only 08810=A=7150...
- Page 53 Spare parts Connections (continued) Description Item no. E-fitting G3/8 6/8 359103,10050 E-fitting 1:8 NPT 6/8 359103,10132 Screw in socket G3/8 PP 359110,02300 Fitting 359500,11106 E-fitting G3/8 10/12 359103,10077 Teflon tape 502614,66121 Complete tubing level detector 359110,05000 Electrodes Description Item no. Pt 100 for temperature measurement, fixed cable Z_368495,10000 Reference electrode...
- Page 54 Spare parts 2 Years spare parts kit (368810,9X00X) Description Quantity Item no. Complete stirrer 359110,01650 Tubing holder cassette 359090,80000 Siphon 359110,01400 Flow tubing 359110,01500 Threaded sleeve PG 13.5 red 359015,20035 Viton O-ring 11 x 4 429=110=040 Teflon tubing 359012,00070 Fitting 1/4 DN 6/8 587=008=002 E-fitting G 1/4 DN 6 587=108=002...
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Page 55: Section 10 User Configuration
Section 10 User configuration User configuration Default value User value Date ELECTRODE NAME Name GLASS Slope Slope +059.16 Uiso Isothermal potential +0000.0 mV Reference potential +0000.0 mV Reference concentration 10E-8 OPTION AUTOMAT. CAL YES/NO Automatic calibration AUTO. CAL 1PT/2PTS Type of automatic calibration 2 PTS With sample / With rinse water Calibration with sample or rinse water... - Page 56 User configuration User configuration Default value User value Date SAMPLE COND: sample conditioning REAGENT 1: XXX Conditioning activated by reagent 1 REAGENT 2: XXX Conditioning activated by reagent 2 INJ. REAG. 1: XXXs Duration of reagent 1 injection 10 seconds INJ.
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