Varian Saturn 2000 GC/MS Manuals

Varian Saturn 2000 GC/MS Manuals

Manuals and User Guides for Varian Saturn 2000 GC/MS. We have 2 Varian Saturn 2000 GC/MS manuals available for free PDF download: Hardware Manual, Pre-Installation Instructions

Varian Saturn 2000 GC/MS Hardware Manual

Varian Saturn 2000 GC/MS Hardware Manual (200 pages)

Ion Trap Mass Spectrometry

Brand: Varian | Category: Laboratory Equipment | Size: 4.35 MB

Table of Contents

Varian, Inc
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Varian, Inc
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Table of Contents
34
Functional Description

40
- Introduction
  40
- Technical Specifications
  42
  - Saturn 2000 GC/MS System Performance Specifications
    42
  - Physical Specifications
    42
- The Gas Chromatograph
  42
- The Mass Spectrometer
  43
- Mechanical Assemblies
  43
  - Controls and Indicators
    43
  - Cooling Fans
    44
  - Turbomolecular Pump Vacuum System
    46
  - Turbomolecular Pump Vacuum Manifold
    46
  - Diffusion Pump Vacuum System
    48
  - The Pneumatics Manifold
    51
  - The Transfer Line
    52
  - Ion Trap Assembly
    53
  - Ion Gauge
    57
- Foreline Pump
  58
- Electronic Assemblies
  58
- The Data System
  65
- Computer/Instrument Interface
  65
- The Computer
  65
- The Autosampler
  65
Chemical Ionization Options

66
System Start-Up and Shutdown

108
- Diffusion Pump Shutdown
  108
- Diffusion Pump Startup
  110
Mass Spectrometer Maintenance

112
- Periodic Maintenance
  112
- Checking Foreline Pump Oil Level and Condition
  112
- Purging Foreline Pump Oil
  113
- Changing Foreline Pump Oil
  114
  - Flushing
    115
- Check Cooling Fans Turbomolecular Pump System
  115
- How to Replace the Turbomolecular Pump
  117
- Check Cooling Fans Diffusion Pump System
  119
- Checking the Diffusion Pump Fluid Level and Condition
  120
- Turning off the Diffusion Pumped Mass Spectrometer
  121
- Replacing the Diffusion Pump Thermocouple Gauge
  122
- Replacing the Diffusion Pump Peltier Baffle
  123
- Cleaning the Diffusion Pump Peltier Baffle
  124
- Removing the Diffusion Pump
  125
- Topping off the Diffusion Pump Fluid Level
  126
- Cleaning the Diffusion Pump
  127
- Changing the Diffusion Pump Heater
  129
- Reinstalling the Diffusion Pump
  130
- Turning on the Mass Spectrometer
  132
- How to Service the Ion Trap
  133
- Turn off the Mass Spectrometer
  134
- Retract/Remove the Transfer Line
  134
- Remove the Analyzer Assembly
  135
- Replace the Electron Multiplier
  137
- Replace the Filament(S)
  138
- Remove the Ion Trap Oven
  139
- Cleaning the Trap Components
  139
  - Disassemble the Trap Components
    139
  - Clean the Trap Components
    140
  - Clean Silchrom Ion Trap Electrodes
    142
  - Clean the Two Quartz or Silica Coated Spacers
    142
  - Reassemble the Trap
    142
- Re-Install the Trap Oven
  143
- Reposition the Electron Multiplier
  144
- Re-Install the Analyzer Assembly
  144
- Install the Transfer Line
  144
- Close the Vent
  145
- Turn on the Mass Spectrometer
  145
- Bake out the Trap
  145
- Check Ion Trap Operation
  146
- Fill the Calibration Compound Vial
  146
GC Maintenance

148
- Overview
  148
- General GC Maintenance
  149
  - Check and Renew Gas Supplies
    149
  - Leak Check
    149
  - Gas Purifier Replacement
    150
  - Injector Maintenance
    152
- 1079 Injector
  153
  - Remove the Glass Insert
    154
  - Replace the Glass Insert
    155
  - Clean the Glass Insert
    156
  - Deactivate the Glass Insert
    157
- How to Remove the Capillary Column from the System
  158
- How to Install a New Capillary Column in the System
  160
Troubleshooting

162
Troubleshooting of Diffusion Pump System

184
- Overview
  184
- Problems During Startup
  184
- Problems During Routine Operation
  185
Miscellaneous Procedures and Instructions

188
- Other Documents
  188
- Site Requirements
  188
  - Site Preparation
    188
  - Power
    188
  - Quality of Power
    190
- Operating Environment
  191
  - Temperature
    191
  - Humidity
    191
  - Exhaust System
    192
- Gas Requirements
  192
  - Helium - GC Carrier Gas
    192
  - Methane, Isobutane - CI Reagent Gases (with CI Option Only)
    192
  - Ammonia - CI Reagent Gas (with CI Option Only)
    192
  - Cryogenics
    192
  - Other Gases
    193
- How to Install Saturn
  193
- How to Move Saturn
  193
- Parts and Supplies
  194
  - Kits, Assemblies, Boards, and Cables
    194
  - Trap Components
    195
  - Pump Spares, Pumps, Pump Conversion Parts
    195
  - Diffusion Pump Spares
    196
  - GC Spares
    197
  - Tools, Test Samples, Etc
    197
  - Additional Saturn Spares
    198
  - CI Parts/Spares
    198
  - Multiple CI Module Parts Lists
    198
  - MCI Module Accessory Kit
    199
  - Open Split Interface
    199
- Calling Varian Service
  200

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Varian Saturn 2000 GC/MS Pre-Installation Instructions

Varian Saturn 2000 GC/MS Pre-Installation Instructions (9 pages)

Brand: Varian | Category: Laboratory Equipment | Size: 0.33 MB

Table of Contents

Table of Contents
1
Space and Weight Requirements
2
Power Requirements
3
Operating Environment
5
- Temperature/Humidity
  5
- Particulate Matter
  6
- Vibration
  6
- Exhaust System
  6
Gas Requirements
6
- GC Carrier Gases
  6
- CI Reagent Gases (with CI Option Only)
  6
- Other Gases
  7
- Gas Lines
  7
Capillary Columns
7
Solvents
7
Network Requirements
7
Computer/Printer Requirements
7
- Specifications
  7
- Qualified Pcs
  8
- Qualified Printers
  8
Inspection
8
Unpacking and Installation
9
Parts and Supplies
9
Preventive Maintenance
9
Trademark Acknowledgment
9

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