Thermo Scientific Orbitrap Exploris GC Manuals

Manuals and User Guides for Thermo Scientific Orbitrap Exploris GC. We have 1 Thermo Scientific Orbitrap Exploris GC manual available for free PDF download: Operating Manual

Thermo Scientific Orbitrap Exploris GC Operating Manual (192 pages)

Mass Spectrometers

Brand: Thermo Scientific | Category: Measuring Instruments | Size: 16 MB

Legal Notices
4
Table of Contents
5
Using this Manual
11
About this Manual
11
Typographical Conventions
12
Signal Words
12
Viewpoint Orientation
12
Data Input
12
Topic Headings
13
Reference Documentation
14
Contacting Us
15
Scope of Delivery
17
Functional Description
19
General Description
20
Layout of the Orbitrap Exploris GC and Orbitrap Exploris GC 240 Mass Spectrometer
20
Operating Modes of the Orbitrap Exploris GC and Orbitrap Exploris GC 240 MS
21
Performance Specifications
22
Instrument Front Side
23
System Status Leds
23
Left Instrument Side
25
Forepump Connection Ports
25
Gas Inlets
25
Right Instrument Side
27
Control Panel
27
Digital-In
28
Ion Optics
32
Source Ion Optics
32
Curved Linear Trap
36
Orbitrap Analyzer
38
Extraction of Ion Packets
38
Measuring Principle
39
Ion Detection
39
HCD Cell
41
Vacuum System
41
Forepump
42
Turbomolecular Pump
43
Vent Valve
43
System Bakeout
43
Electronic Assemblies
44
Cooling Fans
44
Safety
46
Safety Symbols and Signal Words in this Manual
46
Observing this Manual
46
Safety Symbols on the Instrument
47
Rating Plate
48
Intended Use
49
Qualification of the Personnel
50
Permitted Materials
50
Electric Safety Precautions
52
In Case of Emergency
53
Residual Hazards
55
Personal Protective Equipment
56
Installation
57
Placing the Instrument
58
Instrument Dimensions
58
Front View
59
Side View
59
Workbench for Instrument
59
Moving the Instrument
61
Placing the GC
63
Placing the Forepump
67
Laboratory Conditions
70
Power Supply
70
Gas Supply
72
Connecting the Orbitrap Exploris GC and Orbitrap Exploris GC 240 CI Gas Supply
74
Laboratory Temperature
75
Humidity
76
Ventilation and Fume Exhaust
76
Vibration
77
Airborne Noise Emission
77
Setting up Instrument Hardware and Adjusting System Parameters
78
User I/O Connections
79
Output Specifications
79
Input Specifications
80
Troubleshooting Instrument Connection
81
Operation
83
Safety Guidelines for Operation
84
Before Operating the Mass Spectrometer
85
Checking the Forepump
85
Checking the Nitrogen Supply
85
Checking the System Vacuum Levels
86
Checking the Disk Space on the Data System
86
Checking the Mass Accuracy of the Instrument
87
Checking the CI Reagent Gas
87
Setting the System in Standby Condition
88
Shutting down the System
89
Starting up the System after a Shutdown
91
Checks for an Instrument that was Vented
93
Resetting the System
94
Installing the Column
96
Nut and Ferrule Combinations
98
Troubleshooting
107
Safety Guidelines for Troubleshooting
108
Fault Table
109
Main Power Failure
110
Vacuum Leak
111
Failure of UHV Chamber Heating Control
113
Turbomolecular Pump Is Not Running
113
Failure of Source Heaters / Transfer Line Heaters
114
Maintenance
115
Safety Guidelines for Maintenance
116
Guidelines for Maintenance
117
Inspection- and Servicing Plan
118
Cleaning the Surface of the Instrument
120
Checking the Warning Labels
120
Leak-Checking the Gas Lines
120
Checking the Condition of Tubings and Hoses
121
Tools and Supplies
122
Maintaining the Vacuum System
124
Maintenance of the Forepump
124
Maintenance of the Turbomolecular Pump
125
Baking out the System
125
Maintenance of the Fan Filters
127
EI/CI Source Maintenance
129
Removing the Ion Source Cartridge from the Orbitrap Exploris GC and Orbitrap Exploris GC 240 System
129
Reinserting the Ion Source Cartridge
145
Cleaning the Orbitrap Exploris GC and Orbitrap Exploris GC 240 Ion Source Cartridge and Durable Components
152
Spectrometer
156
Replacing a Dual Filament in the Orbitrap
157
Spectrometer
157
Maintenance of the Ion Optics
161
Cleaning the Quadrupole
161
Cleaning the Bent Flatapole
166
Consumables
173
Thermo Fisher Scientific Service
174
Returning Parts
174
Services to be Performed by Thermo Fisher Scientific Service Only
174
Chapter 9 Replaceable Parts
177
Instrument Parts
177
Appendix 10 Legal Documents
180
Fcc Compliance Statement
180
WEEE Compliance
181
Declaration of Conformity
183
Index
187

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