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930 Compact IC Flex Oven/ChS/Deg
Metrohm 930 Compact IC Flex Oven/ChS/Deg Manuals
Manuals and User Guides for Metrohm 930 Compact IC Flex Oven/ChS/Deg. We have
1
Metrohm 930 Compact IC Flex Oven/ChS/Deg manual available for free PDF download: Manual
Metrohm 930 Compact IC Flex Oven/ChS/Deg Manual (108 pages)
Brand:
Metrohm
| Category:
Laboratory Equipment
| Size: 8 MB
Table of Contents
Table of Contents
5
Introduction
9
Instrument Description
9
Intended Use
11
Safety Instructions
11
General Notes on Safety
11
Electrical Safety
11
Tubing and Capillary Connections
13
Flammable Solvents and Chemicals
13
Recycling and Disposal
13
Symbols and Conventions
14
Overview of the Instrument
15
Front
15
Figure 1 Front
15
Rear
17
Figure 2 Rear
17
Feed-Throughs for Capillaries and Cables
18
Figure 3 Feed-Throughs on the Door
19
Figure 4 Openings for Capillaries and Cables
20
Figure 5 Ducts for Capillaries
21
Installation
22
Setting up the Instrument
22
Packaging
22
Checks
22
Location
22
Capillary Connections in the IC System
22
Removing Transport Locking Screws
25
Figure 6 Removing the Transport Locking Screws
25
Connecting the Drainage Tubing and Leak Sensor
26
Installing the Drainage Tubing
26
Connecting the Leak Sensor
28
Column Oven
28
Connecting the Eluent Bottle
29
Figure 7 Installing the Eluent Bottle Cap
29
Figure 8 Installing Tubing Weighting and Aspiration Filter
31
Connecting the Eluent Degasser
33
Installing the High-Pressure Pump
33
Figure 9 High-Pressure Pump with Purge Valve
33
Installing an Inline Filter
34
Installing the Pulsation Absorber
34
Figure 10 Inline Filter
34
Injection Valve
35
Figure 11 Pulsation Absorber
35
Figure 12 Exchanging the Sample Loop
36
Metrohm Suppressor Module (MSM)
37
Inserting the Rotors
38
Connecting the Metrohm Suppressor Module (MSM)
41
Figure 13 Metrohm Suppressor Module (MSM) - Connection Capillaries
41
Installing the Conductivity Detector
45
Installing the Amperometric Detector
46
Connecting the Sample Degasser (Optional)
47
Connecting the Instrument to a Computer
48
Connecting the Instrument to the Power Grid
49
Initial Start-Up
50
Connecting and Rinsing the Guard Column
52
Connecting the Separation Column
54
Conditioning
58
Operation
60
Operation and Maintenance
61
IC System
61
Operation
61
Care
61
Maintenance by Metrohm Service
61
Shutting down and Recommissioning
62
Capillary Connections
63
Servicing the Door
63
Column Oven - Replacing the Capillaries
63
Figure 14 Column Oven
64
Handling the Eluent
65
Manufacturing Eluent
65
Changing the Eluent
66
Servicing the Eluent Degasser
66
Notes on Operating the High-Pressure Pump
67
Servicing the High-Pressure Pump
68
Figure 15 High-Pressure Pump - Parts
68
Figure 16 High-Pressure Pump - Cross-Section
75
Figure 17 Tool for Piston Seal (6.2617.010)
76
Figure 18 Removing the Piston Cartridge from the Pump Head
76
Figure 19 Inserting the Piston Seal into the Tool
77
Figure 20 Parts of the Piston Cartridge
78
Servicing the Inline Filter
81
Figure 21 Inline Filter - Removing the Filter
82
Servicing the Pulsation Absorber
84
Injection Valve
84
Metrohm Suppressor Module (MSM)
84
Notes for Operating the Metrohm Suppressor Module (MSM)
84
Taking Care of the Suppressor Housing
85
Servicing the Metrohm Suppressor Module (MSM)
85
Figure 22 Parts of the Metrohm Suppressor Module (MSM)
85
Servicing the Detector
93
Rinsing the Sample Path
93
Separation Column
95
Separating Efficiency
95
Protecting the Separation Column
95
Storing the Separation Column
95
Regenerating the Separation Column
95
Quality Management and Qualification with Metrohm
96
Troubleshooting
97
Technical Specifications
101
Reference Conditions
101
Instrument
101
Ambient Conditions
101
Housing
102
Weight
102
Leak Sensor
102
Column Oven
102
Eluent Degasser
103
High-Pressure Pump
103
Injection Valve
104
Metrohm Suppressor Module (MSM)
104
Detector
104
Sample Degasser
104
Power Connection
104
Interfaces
105
Accessories
106
Index
107
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