Metrohm 900 Manuals

Metrohm 900 Manuals

Manuals and User Guides for Metrohm 900. We have 2 Metrohm 900 manuals available for free PDF download: Manual, Manual - Short Instructions

Metrohm 900 Manual

Metrohm 900 Manual (553 pages)

Touch Control

Brand: Metrohm | Category: Touch Panel | Size: 7 MB

Table of Contents

Table of Contents
5
1 Introduction

17
- Instrument Description
  17
- Titration and Measuring Modes
  17
- About the Documentation
  19
- Symbols and Conventions
  19
2 Safety Instructions

21
- General Notes on Safety
  21
- Electrical Safety
  21
- Tubing and Capillary Connections
  22
- Flammable Solvents and Chemicals
  22
- Recycling and Disposal
  23
3 Overview of the Instrument

24
- Figure 1 Front 900 Touch Control
  24
- Figure 2 Rear 900 Touch Control
  25
4 Installation

26
- Setting up the Instrument
  26
- Packaging
  26
- Checks
  26
- Location
  26
5 Titrations

27
6 Operation

32
- Switching the Instrument on and off
  32
- Fundamentals of Operation
  33
- Touch-Sensitive Screen
  33
- Display Elements and Controls
  34
- Status Display
  35
- Entering Text and Numbers
  36
7 System Settings

38
- General System Settings
  38
- Selecting the Dialog Language
  38
- Setting the Date, Time and Local Time
  39
- System-Specific Dialog Options
  40
- User Administration
  44
- Editing the User Configuration
  45
- Creating an Identification Profile
  49
- Defining Login Options
  49
- Password Options
  51
- Modification Options
  53
- Reasons
  54
- Audit Trail
  55
- Measured Value Display
  56
- Acoustic Signals
  56
8 Titrants

57
9 Reagents

77
- Editing Reagent Data
  78
- Reagent Monitoring
  78
10 Sensors

82
11 Device Manager

95
- Adding a New Device
  96
- Configuring the Instrument
  96
- Touch Control
  97
- E-Mail
  98
- PC/LIMS Report
  99
- Shared Memory
  100
- TCP/IP Settings
  102
- Metrohm Control Instruments
  103
- Properties - Control Instrument
  104
- Properties - Measuring Input
  104
- Properties - MSB Connector
  106
- Properties - Peripheral Devices
  107
- Sample Processor
  108
- Properties - Sample Processor
  109
- Properties - Tower
  109
- Properties - Swing Head
  111
- Sample Racks
  116
- Editing Rack Data
  118
- Rack Adjustment
  124
- Printer
  125
- PDF Settings
  126
- Network Printer
  127
- More Options
  129
- Balance
  129
- USB/RS-232 Adapter
  131
- PC Keyboard
  133
- Barcode Reader
  134
12 File Manager

137
- Managing Files
  137
- Copying a File
  139
- Renaming a File
  139
- File Properties
  140
- External Storage Medium
  141
- Figure 10 Directory Structure on the External Storage Medium
  142
- Creating Backups / Restoring Data
  143
- Restoring Data
  143
13 GLP Manager

145
- Automatic System Test
  146
- Test Tools
  146
- GLP Tests for Measurement and Titration
  147
- Parameter Description
  148
- System Validation
  151
- Parameter Description
  152
- System Monitoring
  155
- Service Interval
  155
- Backup Interval
  155
14 Common Variables

157
15 Templates

163
- Sample Data
  163
- Sample Identification List
  164
- Sample Assignment Table
  165
- Custom Result Templates
  167
- Editing Result Templates
  168
- Input Lines
  171
- Editing the Input Signal
  172
- Output Lines
  173
- Editing the Output Signal
  175
- Custom Calibration Buffers
  176
- Defining Calibration Buffers
  177
- Report Header
  178
- Custom Electrode Type
  179
- Limit Values for the Electrode Rating
  180
16 Methods

183
- Creating a New Method
  183
- Saving a Method
  184
- Loading a Method
  185
- Editing a Method
  186
- Inserting a Command
  187
- Method Options
  188
- Start Options
  189
- Stop Options
  191
- Sample Data
  192
- Method Properties
  196
- Note
  198
- Saving a Determination Automatically
  198
17 Electronic Signatures

200
- Signing Methods/Determinations Electronically
  200
- Deleting Electronic Signatures
  201
18 Control

202
19 Favorites

206
- Creating Favorites
  207
- Editing Favorites
  207
20 Sample Data

210
- Entering Sample Data in the Main Dialog
  210
- Requesting Sample Data at the Start of the Determina- Tion
  211
21 Sample Table

213
- General
  213
- Editing Sample Data
  216
- Properties
  218
22 Determination Run

221
23 Live Modifications

224
24 Results and more Determination Data

230
- More Determination Data
  231
- Details
  232
- Messages
  234
- Local Common Variables
  235
- Determination Properties
  235
- Loading a Determination
  238
- Determination List
  239
- Saving a Determination
  243
- Curves
  243
- Recalculation and Reevaluation
  245
25 Statistics

247
26 Result Table

252
- Properties
  253
- Saving the Result Table
  257
- Loading the Result Table
  257
27 Printing

258
- General Report Options
  260
- Settings of the Individual Reports
  261
- List of All Printable Reports
  262
28 Manual Control

266
- Opening and Closing the Manual Control
  267
- Measuring
  268
- Parameter Description
  269
- Dosing
  272
- Continuous Dosing
  274
- Dosing Fixed Volumes
  276
- Preparing
  278
- Emptying
  279
- Figure 11 Live Display "Preparing the Dosing Unit
  279
- Figure 12 Live Display "Preparing the Exchange Unit
  279
- Filling
  280
- Replacing Reagent
  280
- Stirring
  281
- Conditioning a Titration Cell
  282
- Parameter Description
  283
- Remote
  283
- Sample Processor
  284
- Moving the Lift
  286
- Moving to a Rack Position
  288
- External Positions
  290
29 Parameters

294
- Dynamic Equivalence Point Titrations (DET)
  294
- Start Conditions
  294
- Titration Parameters
  297
- Stop Conditions
  301
- Potentiometric Evaluation
  302
- Figure 13 Equivalence Point Recognition and Equivalence Point Numbering Within
  306
- Windows
  306
- Control Instrument
  307
- Figure 14 Tubbs Method for Determining the Equivalence Point
  307
- Sensor
  308
- Dosing Device
  309
- Stirrer
  310
- Monotonic Equivalence Point Titrations (MET)
  311
- Start Conditions
  311
- Titration Parameters
  314
- Stop Conditions
  317
- Potentiometric Evaluation
  318
- Figure 15 Equivalence Point Recognition and Equivalence Point Numbering Within
  322
- Windows
  322
- Control Instrument
  323
- Sensor
  324
- Dosing Device
  325
- Stirrer
  326
- Endpoint Titrations (SET)
  327
- Start Conditions
  327
- Control Parameters
  328
- Titration Parameters
  332
- Stop Conditions
  333
- Conditioning
  334
- Cell
  336
- Control Instrument
  336
- Sensor
  336
- Dosing Device
  338
- Stirrer
  339
- Volumetric Karl Fischer Titrations (KFT)
  339
- Start Conditions
  339
- Control Parameters
  341
- Titration Parameters
  344
- Stop Conditions
  345
- Conditioning
  346
- Cell
  348
- Control Instrument
  348
- Sensor
  349
- Dosing Device
  350
- Stirrer
  351
- Coulometric Karl Fischer Titrations (KFC)
  352
- Control Parameters
  352
- Titration Parameters
  354
- Stop Conditions
  355
- Conditioning
  355
- Cell
  358
- Control Instrument
  359
- Sensor
  359
- Stirrer
  360
- Bromine Index Determination (BRC)
  361
- Control Parameters
  361
- Titration Parameters
  364
- Stop Conditions
  365
- Conditioning
  365
- Cell
  367
- Control Instrument
  368
- Sensor
  368
- Stirrer
  369
- STAT Titrations (STAT)
  370
- Start Conditions
  370
- Control Parameters
  372
- Titration Parameters
  374
- Stop Conditions
  376
- Monitoring
  377
- Figure 16 Action "Exit Method" or "Cancel Command
  381
- Figure 17 Action "Pause
  381
- Figure 18 Action "Wait
  381
- Control Instrument
  384
- Sensor
  384
- Dosing Device
  385
- Stirrer
  388
- Manual Titrations (MAT)
  389
- Dosing Parameters
  390
- Control Instrument
  391
- Sensor
  391
- Dosing Device
  392
- Stirrer
  395
- Measurements (MEAS)
  395
- Measuring Parameters
  395
- Standard Addition
  400
- Control Instrument
  404
- Sensor
  404
- Stirrer
  406
- Calibration of Sensors (CAL)
  407
- Calibration Parameters (CAL Ph)
  407
- Calibration Parameters (CAL Conc)
  410
- Calibration Parameters (CAL Cond)
  413
- Control Instrument
  416
  - Sensor
    416
  - Stirrer
    417
  - Electrode Test for Ph Electrodes (ELT)
    418
  - Electrode Test Parameters
    419
  - Control Instrument
    420
  - Sensor
    421
  - Stirrer
    422
  - Additional Information
    422
  - Evaluations (EVAL)
    424
  - Fixed Endpoint Evaluation (EVAL FIX-EP)
    426
  - Pk Value and Half Neutralization Potential Evaluation (EVAL Pk/Hnp)
    428
  - Figure 19 Evaluation of Pk Value / Half Neutralization Potential
    428
  - Minimum and Maximum Evaluation (EVAL MIN/MAX)
    429
  - Figure 20 Evaluation of Minimum and Maximum
    429
  - Break Point Evaluation (EVAL BREAK)
    430
  - Figure 21 Evaluation of a Break Point
    430
  - Rate Evaluation (EVAL RATE)
    433
  - Calculations
    434
  - Calculations (CALC)
    434
  - Calculations (CALC LIVE)
    441
  - Formula Editor
    443
  - Reports (REPORT)
    449
  - General Report Options
    449
  - Settings of the Individual Reports
    450
  - List of Reports
    451
  - Dosing and Liquid Handling
    454
  - Preparing an Exchange or Dosing Unit (PREP)
    454
  - Emptying a Dosing Unit (EMPTY)
    455
  - Dosing a Specified Volume (ADD)
    456
  - Liquid Handling (LQH)
    461
  - Monitored Dosing (DOS)
    464
  - Figure 22 Dosing Criterion "Volume/Dosing Rate
    465
  - Figure 23 Dosing Criterion "Volume/Dosing Time
    465
  - Figure 24 Dosing Criterion "Dosing Rate/Dosing Time
    466
  - Figure 25 Action "Exit Method" or "Cancel Command
    474
  - Figure 26 Action "Pause
    474
  - Figure 27 Action "Wait
    474
  - Communication
    481
  - Scanning Remote Lines (SCAN)
    482
  - Setting Remote Lines (CTRL)
    483
  - Scanning the RS-232 Interface (SCAN RS)
    485
  - Defining RS-232 Commands (CONTROL RS)
    486
  - Automation
    486
  - Rotating Sample Rack (MOVE)
    486
  - Moving the Lift (LIFT)
    489
  - Controlling Pumps (PUMP)
    490
  - Resetting the Rack (RACK)
    491
  - Defining the Sample Variable (SAMPLE)
    491
  - Creating a Subsequence (SUBSEQ)
    492
  - Miscellaneous Commands
    495
  - Controlling a Stirrer (STIR)
    495
  - Pausing the Method Run (WAIT)
    496
  - Scan Data (REQUEST)
    496
  - Defining an Acoustic Signal (BEEP)
    497
  - Signing a Determination (SIGN)
    498
  - Canceling the Method Run (END)
    498
30 Operation and Maintenance

499
- System Initialization
  499
31 Troubleshooting

500
- Editing Methods
  500
- Sample Table
  500
- Results/Statistics
  500
- Printing
  501
- Manual Control
  501
- Miscellaneous
  502
- SET Titration
  502
- Volumetric Karl Fischer Titration
  503
- Coulometric Karl Fischer Titration
  505
- STAT Titration
  507
32 Appendix

508
- Manual Dosing Controller, Optional Accessory for Manual Titration
  508
- Figure 28 Manual Dosing Controller 6.2107.120 - Overview
  508
- Dosing Unit
  509
- Maximum Dosing and Filling Rate
  509
- Default Parameters for Preparing (PREP) and Emptying (EMPTY)
  509
- Exchange Unit
  510
- Maximum Dosing and Filling Rate
  510
- Default Parameters for Preparing (PREP)
  510
- Stirring Rate
  510
- Balance
  511
- Figure 29 Rotational Speed Depending on the Stirring Rate
  511
- Result Variables as Parameter Setting
  512
- Electrode Calibration with Sample Processors
  513
- Stored Buffer Series for Ph Calibration
  515
- Metrohm
  515
- NIST (According to DIN Standard 19266, 2015)
  516
- DIN (According to DIN Standard 19267, 2012)
  517
- Fisher
  518
- Fluka
  519
- Mettler Toledo
  520
- Beckmann
  521
- Radiometer Analytical
  522
- Baker
  523
- Hamilton DURACAL
  524
- Precisa
  525
- Merck Certipur 20 / Titrisol
  526
- Merck Certipur 25
  527
- Using Audittrailviewer
  529
- Installing Audittrailviewer
  529
- Opening the Audit Trail
  530
- Contents of the Audit Trail
  531
- Filtering the Audit Trail
  532
- Exporting the Audit Trail
  533
- Diagnosis
  533
- LCD Test
  534
- Temperature Monitoring
  535
- Formatting an External Storage Medium
  535
- Removing an External Storage Medium
  535
- Adjusting the Touch Screen
  535
- Testing the Touch Screen
  536
- Software Update (Loading Program Versions and Language Files)
  537
- Simulating Titration Curves
  541
- Service
  543
- Arithmetic Algorithms in the Titrando
  543
33 Technical Specifications

545
- Touch Screen
  545
- Interfaces
  546
- Power Supply
  546
- Declarations of Conformity
  546
- Ambient Temperature
  547
- Dimensions
  547
- Storage Capacity
  547
34 Accessories

548
Index

549

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Metrohm 900 Manual - Short Instructions

Metrohm 900 Manual - Short Instructions (26 pages)

Touch Control

Brand: Metrohm | Category: Control Unit | Size: 0 MB

Table of Contents

Table of Contents
5
1 About These Short Instructions

7
2 Introduction

8
3 Safety Instructions

12
- General Notes on Safety
  12
- Electrical Safety
  12
- Tubing and Capillary Connections
  13
- Flammable Solvents and Chemicals
  13
- Recycling and Disposal
  14
4 Overview of the Instrument

15
5 Installation

17
- Setting up the Instrument
  17
- Packaging
  17
- Checks
  17
- Location
  17
6 Operation

18
- Switching the Instrument on and off
  18
- Fundamentals of Operation
  20
- Touch-Sensitive Screen
  20
- Display Elements and Controls
  21
- Status Display
  22
- Entering Text and Numbers
  23
7 Maintenance

25
Index

26

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