Metrohm 848 Titrino plus Manuals

Metrohm 848 Titrino plus Manuals

Manuals and User Guides for Metrohm 848 Titrino plus. We have 1 Metrohm 848 Titrino plus manual available for free PDF download: Manual

Metrohm 848 Titrino plus Manual

Metrohm 848 Titrino plus Manual (148 pages)

Brand: Metrohm | Category: Laboratory Equipment | Size: 2 MB

Table of Contents

Table of Contents
5
1 Introduction

11
- Instrument Description
  11
- Titration and Measuring Modes
  11
- Connectors
  12
- Intended Use
  12
- About the Documentation
  12
- Symbols and Conventions
  13
- Safety Instructions
  14
- General Notes on Safety
  14
- Electrical Safety
  14
- Tubing and Capillary Connections
  15
- Flammable Solvents and Chemicals
  15
- Recycling and Disposal
  15
2 Overview of the Instrument

17
- Figure 1 Front 848 Titrino Plus
  17
- Figure 2 Rear 848 Titrino Plus
  18
3 Installation

19
4 Titrations

27
5 Operation

29
- Switching the Instrument on and off
  29
- Fundamentals of Operation
  30
- The Keypad
  30
- Figure 18 Keypad 848 Titrino Plus
  30
- Structure of the Dialog Windows
  31
- Navigating in the Dialog
  31
- Entering Text and Numbers
  32
- Selecting from a Selection List
  33
- Formula Editor
  33
- Methods
  35
- Creating a New Method
  35
- Saving a Method
  36
- Loading a Method
  37
- Exporting a Method
  38
- Control
  39
- Sample Data
  40
- Entering Sample Data in the Main Dialog
  40
- Requesting Sample Data at the Start of the Determination
  41
- Sample Table
  42
- General
  42
- Editing the Sample Data
  43
- Sending the Sample Size from a Balance
  45
- Carrying out a Determination
  45
- Live Modifications
  47
- Editing the Sample Data of the Running Determination
  47
- Editing the Sample Table While a Determination Is Running
  48
- Editing the Live Parameters
  49
- Results
  50
- Statistics
  51
- Printing a Report Manually
  53
- Manual Control
  54
- Dosing
  55
- Measuring
  59
- Stirring
  60
6 System Settings

62
- Basic Settings
  62
- Managing Sensors
  66
- General
  66
- Editing the Sensor Data
  66
- Managing Solutions
  68
- General
  68
- Editing the Solution Data
  68
- Managing Common Variables
  70
- General
  70
- Editing Common Variables
  71
- File Management
  72
- Figure 19 Directory Structure on the USB Flash Drive
  72
- Configuring External Devices
  73
- Instrument Diagnosis
  76
- Loading Program Versions and Language Files
  76
- Diagnosis Functions
  77
7 Parameters

78
- Dynamic Equivalence Point Titrations (DET)
  78
- Start Conditions
  78
- Titration Parameters
  79
- Stop Conditions
  85
- Evaluation
  86
- Calculation
  89
- Figure 20 Tubbs Method for Determining the Equivalence Point
  89
- Statistics
  91
- Reports
  91
- Monotonic Equivalence Point Titrations (MET)
  93
- Start Conditions
  93
- Titration Parameters
  94
- Stop Conditions
  99
- Evaluation
  100
- Calculation
  103
- Statistics
  105
- Reports
  105
- Endpoint Titrations (SET)
  107
- Conditioning
  107
- Start Conditions
  108
- Titration Parameters
  110
- Control Parameters EP1
  112
- Control Parameters EP2
  115
- Stop Conditions
  115
- Calculation
  116
- Statistics
  118
- Reports
  118
- Ph Calibration (CAL)
  120
- Calibration Parameters
  120
- Buffers
  122
- Reports
  123
8 Operation and Maintenance

124
- Quality Management and Qualification with Metrohm
  124
9 Troubleshooting

125
- SET Titration
  125
- Miscellaneous
  126
10 Appendix

127
- Exchange Unit
  127
- Maximum Dosing and Filling Rate
  127
- Parameters for the Preparing (PREP)
  127
- Stirring Rate
  128
- Balance
  128
- Figure 21 Rotational Speed Depending on Stirring Rate
  128
- USB Devices
  129
- 6.2147.000 Numerical USB Keypad
  129
- Key Assignment of a USB Keyboard
  130
- PC Mouse
  130
- Printer
  131
- System Initialization
  131
- Remote Interface
  132
- Pin Assignment of the Remote Interface
  132
- Figure 22 Pin Assignment of Remote Socket and Remote Plug
  132
- Status Diagram of the Remote Interface
  134
- Figure 23 Remote Status Diagram DET/MET
  134
- Figure 24 Remote Status Diagram SET
  134
- Remote Control Via an RS-232 Connection
  135
- Figure 25 Remote Status Diagram CAL
  135
- Figure 26 Connecting the RS-232/USB Box to the PC
  135
- Commands and Variables
  136
- Arithmetic Algorithms in the 848 Titrino Plus
  137
11 Technical Specifications

140
- Measuring Inputs
  140
- Potentiometry
  140
- Polarizer
  140
- Temperature
  141
- Dosing Drive
  142
- Interfaces
  142
- Power Connection
  142
- Safety Specifications
  142
- Electromagnetic Compatibility (EMC)
  143
- Ambient Temperature
  143
- Reference Conditions
  144
- Dimensions
  144
12 Accessories

145
Index

147

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