Hanna Instruments HI 904 Karl Titrator Manuals

Manuals and User Guides for Hanna Instruments HI 904 Karl Titrator. We have 2 Hanna Instruments HI 904 Karl Titrator manuals available for free PDF download: Uick Start Manual, Quick Start Manual

Hanna Instruments HI 904 Uick Start Manual (180 pages)

KARL FISCHER COULOMETRIC TITRATOR

Brand: Hanna Instruments | Category: Laboratory Equipment | Size: 7 MB

Quick Start Guide

3
- Table of Contents
  3
- Safety Measures
  6
- Titrator Connections
  7
- User Interface
  8
- How to Select Your Language
  9
- How to Use the Contextual Help
  9
- Methods
  9
- Before Performing the First Titration
  10
- How to Perform the First Titration
  10
Table of Contents

19
- Chapter 1. INTRODUCTION
  
  21
Setup Chapter 2.

23
- Chapter 2 SETUP
  
  23
  - Setup
    24
  - Unpacking
    25
  - Safety Measures
    26
  - Installation
    27
  - Titrator Top View
    27
  - Titrator Rear View
    28
  - Titrator Left-Side View
    28
  - Titrator Assembly
    29
    
    Connecting the Air Pump
    29
    
    Connecting the Reagent Adapter Holder
    30
    
    Titration Vessel
    31
    
    Titration Vessel Components
    32
    
    Electrical Connections
    34
  - Reagent, Waste Bottle Assembly
    35
  - Reagent Exchange Adapter
    36
User Interface Chapter 3.

37
- User Interface
  38
- Start up
  39
  - User Interface
    39
- Description
  40
- Keypad
  40
  - Function Keys
    40
  - Option Keys
    40
  - Arrow Keys
    41
  - Numeric Keys
    41
  - Enter Key
    41
- Display
  41
- The Idle Screen
  42
- The Process Screen
  43
- Entering Text
  44
- Menu Navigation
  44
- Selecting a Menu Item
  44
- Selecting an Option
  44
- Saving Modifications
  45
General Options Chapter 4.

47
- General Options
  48
- Date and Time Setting
  49
- Display Settings
  50
- Beeper
  51
- Stirrer
  51
- Language
  52
- Reagent Exchange Reminder
  52
- Save Files to USB Storage Device
  53
- Restore Files from USB Storage Device
  54
- Calibration Check
  55
- USB Link with PC
  55
- Setup Balance Interface
  56
- Printer Mode
  57
- Reset to Default Settings
  58
- Update Software
  58
Methods Chapter 5.

59
- Methods
  61
- Selecting Methods
  61
- Deleting Standard Methods
  62
- Standard Methods
  62
- Upgrading Standard Methods
  62
- Creating User Methods
  63
- Restoring the Standard Methods to the Manufacturer's Settings
  63
- User Methods
  63
- Chapter 3 . USER INTERFACE
  
  64
- Chapter 4 . GENERAL OPTIONS
  
  64
- Chapter 5. METHODS
  
  64
  - Deleting User Methods
    64
  - View / Modify Method
    64
  - Method Options
    65
  - Naming the User Method
    65
  - Method Revision
    66
  - Method Type
    66
  - Pre-Analysis Stir Time
    67
  - Stirring Speed
    67
  - Stirbar Type
    68
  - Drift Entry
    68
  - Reagent Name
    69
  - Sample Parameters
    70
    
    Sample Determination
    70
    
    Sample Name
    71
    
    Sample Type
    71
    
    Sample Density
    72
    
    Sample Size
    72
    
    Dissoluted Sample Size
    73
    
    External Solvent Size
    73
    
    Extracted Sample Size
    73
  - Control Parameters
    74
    
    Titration Speed
    74
    
    Standby Duration
    75
    
    Standby Mode
    75
    
    End Point Value
    76
    
    Imposed Current
    76
    
    Generator Current Mode
    77
    
    Signal Averaging
    77
  - Termination Parameters
    78
    
    Maximum Duration
    78
    
    Maximum Titrated Water
    79
    
    Termination Criterion
    79
    
    End Point Stability Time
    80
  - Result Unit
    80
  - Printing
    80
  - Bromine Index
    81
Methods

83
- Chapter 6. TITRATION
  
  85
  - Idle
    85
  - Pre-Titration
    85
  - Drift Analysis
    86
  - Standby
    87
  - Sample Analysis
    88
Auxiliary Functions

95
- Chapter 7. AUXILIARY FUNCTIONS
  
  97
  - Air Pump
    97
  - Filling the Vessel
    97
  - Emptying the Vessel
    97
  - Stirrer
    98
  - Results
    99
  - Review Last Titration Report
    99
  - Review Available Reports
    100
  - GLP Data
    100
  - Meter Information
    101
  - Setup Titration Report
    102
Maintenance, Peripherals Chapter 8.

103
- Maintenance, Peripherals
  104
- Detector Electrode Maintenance
  105
- Generator Electrode Maintenance
  105
- Reagent Adapter Holder Maintenance
  106
- Reagent Exchange Adapter Maintenance
  106
- Connecting an External Display
  107
- Peripherals
  107
- Connecting an External PC Keyboard
  108
- Connecting a Printer
  110
- Connecting to a Computer
  111
Methods Optimization

113
- Chapter 8 . MAINTENANCE, PERIPHERALS
  
  115
- Chapter 9. OPTIMIZATION
  
  115
  - Titrator Settings
    115
  - Control Parameters
    115
    
    Endpoint Potential and Polarization Current
    115
    
    Signal Averaging
    116
    
    Titration Speed
    116
  - Termination Parameters
    117
    
    Drift Stop Termination Criteria
    117
    
    Relative Drift Stop
    117
    
    Stability Time
    117
    
    Absolute Drift Stop
    118
  - Method Options
    118
    
    Background Drift Rate Entry
    118
    
    Pre-Analysis Stir Time
    118
    
    Stirring Speed
    118
  - The Sample
    119
  - Proper Sampling Procedure
    119
  - Determining the Optimal Sample Size
    119
  - Solid Samples
    119
  - Liquid Samples
    120
  - Sample Preparation Techniques
    121
    
    Dilutions
    121
    
    External Dissolution
    121
    
    External Extractions
    121
    
    Heating
    122
    
    Homogenization
    122
  - Karl Fischer Reagent System
    123
  - Water Standards
    123
- Appendix 1. TECHNICAL SPECIFICATIONS
  
  129
- Appendix 2. RECOMMENDED REAGENTS
  
  131
- Appendix 3. TITRATOR COMPONENTS
  
  137
Titration Theory

151
- Introduction
  153
  - General Review of Titration Theory
    153
  - Introduction to Titrations
    153
  - Uses of Titrations
    153
- Advantages and Disadvantages of Titrations
  154
- Amperometric Titrations
  155
- Potentiometric Titrations
  155
- Titrations According to the Measurement Method
  155
- Types of Titration
  155
- Spectrophotometric Titrations
  156
- Karl Fischer Titrations
  157
- Titrations According to the Reaction Type
  157
- Acid-Base Titrations
  161
- Argentometric Titrations
  162
- Complexometric Titrations
  163
- Ion Selective Titrations
  163
- Non-Aqueous Solvent Acid-Base Titrations
  163
- Precipitation Titrations
  164
- Redox Titrations
  164
- Back Titrations
  165
- Multiple End Point Titrations
  165
- Titrations According to the Titration Sequence
  165
- Introduction to Titration Apparatus and Typical Titration Procedure
  167
- Manual Titration
  167
- Automatic Titration
  168
- Accuracy
  169
- Errors with Titrant and Standard
  169
  - Preparation Errors
    169
- Repeatability
  169
- Sampling Errors
  169
- Sources of Error
  169
- Titration Results
  169
- Chemical Reaction Errors
  170
- Dispensing Errors
  170
- End Point Determination Errors
  170
- Calculation of Water Content as % Mass from Samples Measured by Mass
  171
- Calculation of Water Content as % Mass from Samples Measured by Volume
  171
- Calculation of Water Content as % Mass Subtracting Background Drift Rate
  171
- Calculation of Water Content as % Volume from Samples Measured by Volume
  171
- Calculations
  171
- Equations Used in Karl Fischer Titrations
  171
- Calculation of Titer (Water Equivalent of the Titrant) Using Sodium Tartrate Dihydrate Containing 15.66% Water by Mass
  172
- Calculation of Water Content in External Dissolution Samples
  172
- Calculation of Water Content in External Extraction Samples
  172
- Calculation of Water Content in Gaseous Samples
  172
- Calculation of Titer (Water Equivalent of the Titrant) Using Water Standards
  173
- Equations Used in Titrations
  173
- Sample Calculation
  173
- Standardize Titrant
  173
- Blank Titration
  174
- Multiple End Point Titration
  174
- Back Titration
  175
- Glossary
  176

Hanna Instruments HI 904 Quick Start Manual (180 pages)

Karl Fischer Coulometric Titrator

Brand: Hanna Instruments | Category: Laboratory Equipment | Size: 4 MB

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Hanna Instruments HI 904 Karl Titrator Manuals

Hanna Instruments HI 904 Uick Start Manual (180 pages)

Table of Contents

Quick Start Guide

Table of Contents

Chapter 1. INTRODUCTION

Setup Chapter 2.

Chapter 2 SETUP

User Interface Chapter 3.

General Options Chapter 4.

Methods Chapter 5.

Chapter 3 . USER INTERFACE

Chapter 4 . GENERAL OPTIONS

Chapter 5. METHODS

Methods

Chapter 6. TITRATION

Auxiliary Functions

Chapter 7. AUXILIARY FUNCTIONS

Maintenance, Peripherals Chapter 8.

Methods Optimization

Chapter 8 . MAINTENANCE, PERIPHERALS

Chapter 9. OPTIMIZATION

Appendix 1. TECHNICAL SPECIFICATIONS

Appendix 2. RECOMMENDED REAGENTS

Appendix 3. TITRATOR COMPONENTS

Titration Theory

Hanna Instruments HI 904 Quick Start Manual (180 pages)

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