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Daedalus RM Manuals
Manuals and User Guides for Daedalus RM. We have
1
Daedalus RM manual available for free PDF download: User Manual
Daedalus RM User Manual (40 pages)
Brand:
Daedalus
| Category:
Synthesizer
| Size: 0.83 MB
Table of Contents
Table of Contents
3
List of Figures
4
Warnings / Information
5
Items Included with the Rm Synthesizer
6
Items to be Supplied by the End-User
7
Figure 1: Possible Bench-Top Setup
8
Instrument Site Considerations
8
Figure 2: Possible Fume Hood Setup
9
Connection Details
9
Figure 3: Cleaning Manifold Assembly Diagram
10
Figure 4: Piston Position During Operation
12
Theory of Operation
12
Figure 5: RM Synthesizer Operational Description
14
Figure 6: RM Synthesizer Flow Diagram
15
Figure 7: Example Valve Actuation Progression
16
Conventions Used in this Manual
16
Valve Descriptions
16
Figure 8: Back Panel Port Connections
18
Back Panel Connections
18
Figure 9: Front Panel Controls
19
Front Panel Control
19
Preparing the Instrument for Use
19
Figure 10: Mixing Chamber Components: Poston, Reagent Plate, and Main Seal
21
The Mixing Chamber / Adding Reagents
21
Figure 11: View Showing Internal Placement of the Mixing Chamber Components
22
Figure 12: Progression of Steps for Assembling and Sealing the Mixing Chamber Prior to Sample Preparation
23
Sealing the Mixing Chamber
23
Protocol for Making Samples
24
Figure 13: Increasing the Sample Chamber Pressure Using the Piston
26
Transferring Samples from the Mixing Chamber to the Nmr Cell
27
Figure 14: Progression of Valve Actuation for the Sample Transfer Steps
28
Cleaning the Mixing Chamber
28
Figure 15: Removing the Piston
30
Resetting the System for the Next Sample
30
Tips
31
Calibrating the System
33
Replacing the Window Seals
34
Figure 16: Replacing the Mixing Chamber Windows
35
Figure 17: Reassembly of the Window Plug
35
Figure 18: Reinserting the Window Plug
36
Figure 19: Face Plate Tightening Pattern
36
Figure 20: Removing the Light Housing
37
Specifications
38
Figure 21: Internal Control Board Schematic
39
Further Information
40
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