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NMR 600'89 Ascend DNP
Bruker NMR 600'89 Ascend DNP Manuals
Manuals and User Guides for Bruker NMR 600'89 Ascend DNP. We have
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Bruker NMR 600'89 Ascend DNP manual available for free PDF download: User Manual
Bruker NMR 600'89 Ascend DNP User Manual (102 pages)
Brand:
Bruker
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
3
Contact
7
1 Introduction
9
General Information
9
Limitation of Liability
9
Customer Service
9
Warranty
9
Copyright
9
General View
10
Figure 1.1: General View of a Magnet System with 2Helium Turrets
10
2 Safety
11
Approved Persons
11
Customer Responsibilities
12
Key Words
13
Danger
13
Residual Risks
15
Persons
15
Intended Use
15
Safety Devices
16
Spare Parts
16
Signs and Labels
17
Technical Risks
17
Warning
18
Cryogenic Agents
18
Electricity
18
Gas under Pressure
19
Low Temperatures
20
Personal Protective Equipment
23
Description of Signs and Labels
24
Safety Devices
25
Figure 2.1: Safety Devices of the Cryostat with 2 Helium Turrets
25
Behavior in Danger and Emergency Situations
26
Fire Department Notification
26
3 Transportation
27
Safety
27
Packaging
27
Figure 3.1: Packaging (Without Surrounding Panels)
27
Disposal
28
Transport Inspection
28
Transportation by Fork Lift / Pallet Jack
29
Figure 3.2: Transportation by Fork Lift - Front View
29
Figure 3.3: Transportation by Fork Lift - Rear View
29
Transportation with a Crane
30
Figure 3.4: Attachment Points for Lifting Equipment
30
Figure 3.5: Instruction Label for Lifting Equipment
30
Storing
31
Disposal
31
4 Assembling
33
5 Operation
35
Safety
35
Magnetic Field
35
Persons
35
Set into Operation
36
Figure 5.1: Start the Magnet Stand
36
Figure 5.2: Stop the Magnet Stand
36
6 Troubleshooting
37
Safety
37
Spontaneous Ignition and Explosion
37
Problem
38
During Transportation
38
During Assembling
38
During Cooling Procedure
40
During Energizing and Shimming
44
During Operation of the Magnet Stand
47
During Standard Operation
49
During De-Energizing and Warming
51
Troubleshooting Work
52
After a Quench
52
Figure 6.1: Magnet System During a Quench
52
7 Maintenance
53
Safety
53
Cleaning
53
Maintenance Timetable
54
Maintenance-Free Components
54
Table 7.1: Maintenance Timetable
54
Table 7.2: Maintenance-Free Components of the Magnet System
54
8 Disassembling
55
9 Technical Data MS 600'89 D359 Ascend DNP
57
Environmental Conditions
57
Identification Plate
57
Table 9.1: Environmental Conditions
57
Dimensions
58
Weights
58
Dimensions for Transportation
58
Table 9.2: Weight of the Magnet System
58
Table 9.3: Dimensions for Transportation of the Magnet System
58
Dimensions Cryostat
59
Figure 9.1: Dimensions of the Cryostat (Front View)
59
Table 9.4: Dimensions of the Cryostat - Front View
60
Figure 9.2: Dimensions of the Cryostat (Top View)
61
Table 9.5: Dimensions of the Cryostat - Top View
61
Safety Valves
62
Figure 9.3: Safety Valves of the Cryostat
62
Table 9.6: Opening Pressure of the Safety Valves of the Magnet System
62
Nitrogen Level Sensor
63
Figure 9.4: Nitrogen Level Sensor
63
Table 9.7: Nitrogen Level Sensor
63
Helium Level Sensor
64
Figure 9.5: Helium Level Sensor
64
Table 9.8: Helium Level Sensor
64
Temperature Sensors
65
Figure 9.6: Characteristic Curve of PT 100 Sensor
65
Table 9.9: Characteristic Values of PT 100 Sensor
65
Figure 9.7: Characteristic Curve of IBT Carbon Sensors
66
Table 9.10: Characteristic Values of IBT Carbon Sensor
66
Technical Data Magnet
67
Table 9.11: Specification of the Magnet
67
Fringe Field Plot
68
Figure 9.8: Fringe Field Plot of the Magnet System at Maximum Field
68
Table 9.12: Fringe Field Data of the Magnet System at Maximum Field
68
Technical Data Sweep Coil
69
Table 9.13: Specification of the Sweep Coil
69
Filling Volume, Evaporation Rate and Hold Time
70
Table 9.14: Cryogenic Agents Consumption During Installation
70
Table 9.15: Cryogenic Agents
70
Nitrogen Level Graph
71
Figure 9.9: Nitrogen Level Graph
71
Helium Level Graph
72
Figure 9.10: Helium Level Graph
72
Resistance at Room Temperature
73
Table 9.16: Resistance at Room Temperature
73
Sweep Current Lead Resistance
74
Heater Currents
74
Sweep Power Supply Settings
74
Table 9.17: Sweep Current Lead Resistance at Room Temperature
74
Table 9.18: Heater Currents
74
Table 9.19: Sweep Power Supply Settings
74
Shim Switch Heater
75
Table 9.20: Shim Switch Heater Operation
75
Energizing Assignment and Currents
76
Table 9.21: Energizing Assignment and Currents
76
Magnetic Center
77
Figure 9.11: Magnetic Center and Shimsystem Offset (SO)
77
Table 9.22: Magnetic Center
77
Cycling Assignment and Shim Currents
78
Table 9.23: Cycling Assignment and Shim Currents
78
Cryo Shim Currents
79
Deenergizing Assignment and Currents
79
Table 9.24: Cryo Shim Currents
79
Table 9.25: Deenergizing Assignment and Currents
79
Current Lead
81
Figure 9.12: High Current Lead, 55 Pin
81
Sweep Current Lead
82
Figure 9.13: Sweep Current Lead 55 Pin
82
Shorting Plug
83
Figure 9.14: Shorting Plug 55 Pin
83
Sweep Current Lead Mounting Device
84
Figure 9.15: Sweep Current Lead Mounting Device M 16 Socket
84
Wiring Diagram Magnet
85
Figure 9.16: Wiring Diagram Magnet
85
Wiring Diagram Magnet Control and Shims
86
Figure 9.17: Wiring Diagram Magnet Control and Shims
86
Wiring Diagram Magnet Diagnostic and Temperature Sensors
87
Figure 9.18: Wiring Diagram Magnet Diagnostic and Temperature Sensors
87
Nitrogen Refill Report
88
Helium Refill Report
90
Appendix A
93
Warning Signs
93
List of Figures A.2 Figures
95
Figures
95
Tables
97
Index
99
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