Bruker D2 PHASER Manuals

Bruker D2 PHASER Manuals

Manuals and User Guides for Bruker D2 PHASER. We have 1 Bruker D2 PHASER manual available for free PDF download: User Manual

Bruker D2 PHASER User Manual

Bruker D2 PHASER User Manual (120 pages)

Brand: Bruker | Category: Laboratory Equipment | Size: 43 MB

Table of Contents

Table of Contents
3
Introduction
7
Basics and Principle of Operation
9
Design of the Diffractometer
10
Goniometer
10
X-Ray Tube
10
Slit Systems, Slit and Soller Modules and Other Passive Optics
12
Primary Divergence Slit Systems
12
Secondary Detector Slit Systems
12
Slit Module
12
K Filter Module
13
Absorber Module
13
Soller Slit Module
13
Airscatter Screen Modules
13
Sample Holder
14
Sample Changer
14
Detectors
14
Silicon Strip Detector LYNXEYE
15
Xflash Detector
15
Operation of the D2 PHASER
16
Transport and Positioning of the Instrument
16
Switching on the Instrument
16
Switching off the Instrument
17
Warning and Status Lamps
17
Operational Controls and Connection Plugs
17
Front Door of the Instrument
17
Measurement with the D2 PHASER
17
Configuration and Settings of Primary Section
18
Configuration and Settings of Sample Section
18
Configuration and Settings of Secondary Section
19
Start Measurement with Commander
19
Start Measurement with Joblist
20
Start Element Analyses with the Program SPECTRA
20
Alignment of the Diffractometer
21
Introduction
21
Philosophy of Alignment for D2 PHASER Systems
21
Functional Principle of the Goniometer
22
Zero Definition of the  Scale
22
Setting the Parameters of the Detector Unit
23
Avoiding Collisions with the D2 PHASER Goniometer
25
Maintenance of the Diffractometer
26
Introduction
26
Maintenance of the Internal Cooling Unit
26
Cooling Cycle
26
Thermomodule
26
Checking the Cooling Fluid Level
26
Refilling the Cooling Fluid Tank
27
Replacement of the Fan Filter
27
X-Ray Safety Precautions
28
Introduction
28
Detailed Description of the X-Ray Safety System
28
Radiation Protection Enclosure
28
Safety System
28
Radiation Protection and Leakage Levels
30
Resetting the D2 PHASER Safety System
30
Important Information for Canadian Users
31
General Safety Precautions of the D2 PHASER
31
Biological Effects
31
Mechanisms of Damage
31
Tissue Sensitivity
32
Prompt and Delayed Effects
32
Delayed Effects of Radiation Exposure
32
General Physical Principles
32
Production of X-Rays
32
Continuous Spectrum
33
Characteristic Spectrum
34
X-Ray Safety Precaution
36
Troubleshooting
37
Resetting the Safety System
37
Overtemperature Safety Shutdown
37
Trouble with the Internal Cooling Unit
37
Generator Arcing
37
Drive Error
37
DSP Error with Xflash Detector
38
Other Problems
38
Maintenance Parts and Consumables
39
Maintenance Parts
39
Maintenance Kit for D2 PHASER Systems
39

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