User Manuals: Bruker Ascend 400'54 NMR Spectrometer

Manuals and User Guides for Bruker Ascend 400'54 NMR Spectrometer. We have 3 Bruker Ascend 400'54 NMR Spectrometer manuals available for free PDF download: User Manual

Bruker Ascend 400'54 User Manual (98 pages)

Brand: Bruker | Category: Industrial Equipment | Size: 1 MB

Table of Contents

3
- Contact
  
  7
- 1 Introduction
  
  9
  - General Information
    9
  - Limitation of Liability
    9
  - Customer Service
    9
  - Warranty
    9
  - Copyright
    9
  - General View
    10
  - Figure 1.1: General View of a Magnet System with 2 Helium Turrets
    10
- 2 Safety
  
  11
  - Approved Persons
    11
  - Customer Responsibilities
    12
  - Key Words
    13
  - Danger
    13
  - Residual Risks
    14
  - Persons
    14
  - Intended Use
    14
  - Safety Devices
    15
  - Spare Parts
    15
  - Signs and Labels
    16
  - Technical Risks
    16
  - Warning
    17
    
    Cryogenic Agents
    17
    
    Electricity
    17
    
    Gas under Pressure
    18
    
    Low Temperatures
    19
  - Personal Protective Equipment
    22
  - Description of Signs and Labels
    23
  - Safety Devices
    24
  - Figure 2.1: Safety Devices of the Cryostat with 2 Helium Turrets
    24
  - Behavior in Danger and Emergency Situations
    26
  - Fire Department Notification
    26
- 3 Transportation
  
  27
- 4 Assembly
  
  33
  - Safety
    33
- 5 Operation
  
  35
  - Safety
    35
    
    Magnetic Field
    35
    
    Persons
    35
  - Set into Operation
    36
  - Figure 5.1: Start the Magnet Stand
    36
  - Figure 5.2: Stop the Magnet Stand
    36
- 6 Troubleshooting
  
  37
  - Safety
    37
    
    Spontaneous Ignition and Explosion
    37
  - Problem
    38
  - During Transportation
    38
  - During Assembly
    38
  - During Cooling Procedure
    40
  - During Energizing and Shimming
    44
  - During Operation of the Magnet Stand
    47
  - During Standard Operation
    49
  - During De-Energizing and Warming
    51
  - Troubleshooting Work
    52
  - After a Quench
    52
  - Figure 6.1: Magnet System During a Quench
    52
- 7 Maintenance
  
  53
  - Safety
    53
  - Cleaning
    53
  - Maintenance Timetable
    54
  - Maintenance-Free Components
    54
  - Table 7.1: Maintenance Timetable
    54
  - Table 7.2: Maintenance-Free Components of the Magnet System
    54
- 8 Disassembly
  
  55
  - Safety
    55
- 9 Technical Data MS 400'54 Ascend
  
  57
- Appendix A
  
  89
  - Warning Signs
    89
List of Figures A.2 Figures

91
- Figures
  91
- Tables
  93
- Glossary / Abbreviations
  95

Bruker Ascend 400'54 User Manual (98 pages)

Brand: Bruker | Category: Laboratory Equipment | Size: 1 MB

Table of Contents
3
Contact
7
Introduction
9
General Information
9
Limitation of Liability
9
Customer Service
9
Warranty
9
Copyright
9
General View
10
Figure 1.1: General View of a Magnet System with 2 Helium Turrets
10
Safety
11
Approved Persons
11
Customer Responsibilities
12
Key Words
13
Danger
13
Residual Risks
14
Persons
14
Intended Use
14
Safety Devices
15
Spare Parts
15
Signs and Labels
16
Technical Risks
16
Warning
17
Cryogenic Agents
17
Electricity
17
Gas under Pressure
18
Low Temperatures
19
Personal Protective Equipment
22
Description of Signs and Labels
23
Safety Devices
24
Figure 2.1: Safety Devices of the Cryostat with 2 Helium Turrets
24
Behavior in Danger and Emergency Situations
26
Fire Department Notification
26
Transportation
27
Safety
27
Packaging
27
Figure 3.1: Packaging (Without Surrounding Panels)
27
Disposal
28
Transport Inspection
28
Transportation by Fork Lift / Pallet Jack
29
Figure 3.2: Transportation by Forklift - Front Side
29
Figure 3.3: Transportation by Forklift - Rear Side
29
Transportation with a Crane
30
Figure 3.4: Attachment Points for Lifting Equipment
30
Figure 3.5: Instruction Label for Lifting Equipment
30
Storing
31
Disposal
31
Assembly
33
Safety
33
Operation
35
Safety
35
Magnetic Field
35
Persons
35
Set into Operation
36
Figure 5.1: Start the Magnet Stand
36
Figure 5.2: Stop the Magnet Stand
36
Troubleshooting
37
Safety
37
Spontaneous Ignition and Explosion
37
Problem
38
During Transportation
38
During Assembly
38
During Cooling Procedure
40
During Energizing and Shimming
44
During Operation of the Magnet Stand
47
During Standard Operation
49
During De-Energizing and Warming
51
Troubleshooting Work
52
After a Quench
52
Figure 6.1: Magnet System During a Quench
52
Maintenance
53
Safety
53
Cleaning
53
Maintenance Timetable
54
Maintenance-Free Components
54
Table 7.1: Maintenance Timetable
54
Table 7.2: Maintenance-Free Components of the Magnet System
54
Disassembly
55
Safety
55
Technical Data MS 400'54 Ascend ULH
57
Environmental Conditions
57
Identification Plate
57
Table 9.1: Environmental Conditions
57
Dimensions
58
Weights
58
Dimensions for Transportation
58
Table 9.2: Weight of the Magnet System
58
Dimensions Cryostat
59
Figure 9.1: Dimensions of the Cryostat (Front View)
59
Table 9.4: Dimensions of the Cryostat - Front View
60
Figure 9.2: Dimensions of the Cryostat (Top View)
61
Table 9.5: Dimensions of the Cryostat - Top View
61
Safety Valves
62
Figure 9.3: Safety Valves of the Cryostat
62
Table 9.6: Opening Pressure of the Safety Valves of the Magnet System
62
Nitrogen Level Sensor
63
Figure 9.4: Nitrogen Level Sensor
63
Table 9.7: Nitrogen Level Sensor
63
Helium Level Sensor
64
Figure 9.5: Helium Level Sensor
64
Table 9.8: Helium Level Sensor
64
Temperature Sensors
65
Figure 9.6: Characteristic Curve of PT 100 Sensor
65
Table 9.9: Characteristic Values of PT 100 Sensor
65
Figure 9.7: Characteristic Curve of IBT Carbon Sensor
66
Table 9.10: Characteristic Values of IBT Carbon Sensor
66
Technical Data Magnet
67
Table 9.11: Specification of the Magnet
67
Fringe Field Plot
68
Figure 9.8: Fringe Field Plot of the Magnet System at Maximum Field
68
Table 9.12: Fringe Field Data of the Magnet System at Maximum Field
68
Filling Volume, Evaporation Rate and Hold Time
69
Table 9.13: Cryogenic Agents Consumption During Installation
69
Table 9.14: Cryogenic Agents
69
Nitrogen Level Graph
70
Figure 9.9: Nitrogen Level Graph
70
Helium Level Graph
71
Figure 9.10: Helium Level Graph
71
Resistance at Room Temperature
72
Table 9.15: Resistance at Room Temperature
72
Heater Currents
73
Shim Switch Heater
73
Table 9.16: Heater Currents
73
Table 9.17: Shim Switch Heater Operation
73
Energizing Assignment and Currents
74
Table 9.18: Energizing Assignment and Currents
74
Magnetic Center
75
Figure 9.11: Magnetic Center and Shimsystem Offset (SO)
75
Table 9.19: Magnetic Center
75
Cycling Assignment and Shim Currents
76
Table 9.20: Cycling Assignment and Shim Currents
76
Energizing Currents
77
Deenergizing Assignment and Currents
77
Table 9.21: Energizing Currents
77
Table 9.22: Deenergizing Assignment and Currents
77
Current Lead
79
Figure 9.12: Current Lead 55 Pin
79
Wiring Diagram Magnet
80
Figure 9.13: Wiring Diagram Magnet
80
Wiring Diagram Magnet Control and Shims
81
Figure 9.14: Wiring Diagram Magnet Control and Shims
81
Wiring Diagram Magnet Diagnostic and Temperature Sensors
82
Figure 9.15: Wiring Diagram Magnet Diagnostic and Temperature Sensors
82
Shorting Plug
83
Figure 9.16: Shorting Plug 55 Pins
83
Nitrogen Refill Report
84
Helium Refill Report
86
Warning Signs
89
Figures
91
Tables
93
Abbreviations
95

Bruker Ascend 400'54 User Manual (102 pages)

Brand: Bruker | Category: Laboratory Equipment | Size: 4 MB

Table of Contents
3
Contact
9
Introduction
11
- General Information
  11
- Limitation of Liability
  11
- Customer Service
  11
- Warranty
  11
- Copyright
  11
- General View
  12
Safety
13
- Approved Persons
  13
- Customer Responsibilities
  14
- Key Words
  15
- Residual Risks
  16
- Persons
  16
- Intended Use
  16
- Safety Devices
  17
- Spare Parts
  17
- Signs and Labels
  18
- Technical Risks
  18
- Personal Protective Equipment
  24
- Description of Signs and Labels
  25
- Safety Devices
  26
- Behavior in Danger and Emergency Situations
  28
- Fire Department Notification
  28
Transportation
29
- Safety
  29
- Packaging
  29
- Disposal
  30
- Transport Inspection
  30
- Transportation by Fork Lift / Pallet Jack
  31
- Transportation with a Crane
  32
- Storing
  33
- Disposal
  33
Assembling
35
- Safety
  35
Operation
37
- Safety
  37
- Set into Operation
  38
Troubleshooting
39
- Safety
  39
- Problem
  40
- During Transportation
  40
- During Assembling
  40
- During Cooling down
  42
- During Energizing and Shimming
  46
- During Operation of the Magnet Stand
  48
- During Standard Operation
  50
- During De-Energizing and Warming up
  52
- Troubleshooting Work
  53
- After a Quench
  53
Maintenance
55
- Safety
  55
- Cleaning
  56
- Maintenance Timetable
  56
Disassembling
57
- Safety
  57
A Appendix
59
- Warning Signs
  61
- Figures
  63
- Tables
  65
- Glossary / Abbreviations
  67
- Technical Data MS 400'54 Ascend
  69
- Index
  99

Bruker Categories

Laboratory Equipment Measuring Instruments Industrial Equipment Security Sensors Analytical Instruments

More Bruker Manuals

User Manuals: Bruker Ascend 400'54 NMR Spectrometer

Bruker Ascend 400'54 User Manual (98 pages)

Table of Contents

Table of Contents

Contact

1 Introduction

2 Safety

3 Transportation

4 Assembly

5 Operation

6 Troubleshooting

7 Maintenance

8 Disassembly

9 Technical Data MS 400'54 Ascend

Appendix A

List of Figures A.2 Figures

Bruker Ascend 400'54 User Manual (98 pages)

Table of Contents

Bruker Ascend 400'54 User Manual (102 pages)

Table of Contents

Related Products

Bruker Categories