Anton Paar TTK 600 Manuals

Manuals and User Guides for Anton Paar TTK 600. We have 1 Anton Paar TTK 600 manual available for free PDF download: Reference Manual

Anton Paar TTK 600 Reference Manual (85 pages)

Low Temperature Chamber with CCU 100 Control Unit

Brand: Anton Paar | Category: Climate chamber | Size: 6 MB

Table of Contents
4
Safety Instructions
7
General Safety Instructions
7
Conventions for Safety Messages
8
Safety Signs on the Instrument
9
TTK 600 - an Overview
10
Intended Use of the Instrument
10
Operating Principle
11
TTK 600 Sample Chamber
12
Chamber Main Parts
12
Chamber Housing with Connectors
12
Chamber Lid
13
Internal Parts
13
Sample Holders
14
Standard Sample Holder
14
Standard Sample Holder Heating Environment
14
Capillary Sample Holder
14
Transmission Sample Holder
15
Antechamber for TTK 600
15
Battery Sample Holder
15
Sample Cooling
16
Liquid Nitrogen Cooling Equipment
16
Compressed-Air Cooling Equipment
17
CCU 100 Combined Control Unit
18
CCU 100 Front Panel
18
CCU 100 Rear Panel
18
Control of the Sample Cooling
19
Overheat Protection
19
Water Flow Controller
19
Checking the Supplied Parts
20
Installation
21
Installation Overview
21
Installation Requirements
22
X-Ray Diffractometer Requirements
22
Electrical Requirements
23
Cooling Water Requirements
23
Requirements for Liquid Nitrogen Cooling
23
Requirements for Compressed-Air Cooling
23
Vacuum Equipment Requirements (Optional)
23
Mounting the Adapter on the Sample Chamber
24
Mounting the Chamber on the Goniometer
25
Installing CCU 100
25
Connecting CCU 100 with a Computer
25
Installing the Cooling Water Circuit
26
Installing the Liquid Nitrogen Equipment
26
Installing the Air-Cooling Equipment
27
Cooling Mode Switching Valve (Optional)
29
Mounting the Gas/Vacuum Connector
29
Installing the Gas Supply (Optional)
29
Installing the Vacuum Equipment (Optional)
30
Installing the Gas/Vacuum System for Using the Antechamber
31
Convection Heater
31
Mounting the Electrode Connector and the Connector Box
32
Putting TTK 600 into Operation
34
Alignment of the Standard Sample Holder
34
Height Alignment with Rigid Adapter
34
Height Alignment with Motorized Alignment Stage
35
Alignment of the Chamber Rotation
35
Alignment of the Standard Sample Holder
35
Preparing the Cooling Equipment
36
Preparing the Liquid-Nitrogen Cooling
36
Preparing the Compressed-Air Cooling
36
Checking the Instrument Condition
36
Turning on the Instrument
37
Operating CCU 100
38
Front Panel of the Instrument
38
Keypad
38
Status Leds
39
Display
39
Navigation Diagram of CCU 100
40
Turning the Heater on and off
41
Controlling the Cooling Device
41
Controlling the Liquid Nitrogen Cooling
41
Controlling the Compressed-Air Cooling
42
Manual Control of CCU 100
42
Remote Control of CCU 100
42
Operating the LN2 Cooling Equipment
43
LN2 Consumption and Operating Time
43
Typical Cooling Curves
43
Performing a Measurement
44
Adjusting the Knife Edge
44
Preparing the Sample
44
Additional Information for the Standard Sample Holder
44
Additional Information for the Transmission Sample Holder
45
Samples for the Capillary Sample Holder
45
Taking out the Sample Holder
46
Standard Sample Holder
46
Transmission Sample Holder
46
Battery Sample Holder
47
Applying the Sample
48
Powder Samples for the Standard Sample Holder
48
Bulk Samples for the Standard Sample Holder
48
Powders and Pastes for the Transmission Sample Holder
48
Foils for the Transmission Sample Holder
50
Coin Cells for the Battery Sample Holder
50
Guideline for the Correct Choice of Conditions and Foil Materials
51
Temperature Range
51
Temperature Accuracy and Influence of Convection Heater
51
Background of the Foil Materials
52
Foil Materials for the Battery Sample Holders
52
Mounting the Sample Holder
53
Mounting the Standard Sample Holder
53
Mounting the Standard Sample Holder Heating Environment
53
Mounting the Capillary Sample Holder
54
Mounting the Transmission Sample Holder
55
Mounting and Use of the Antechamber for TTK 600
56
Mounting and Use of the Battery Sample Holders
57
Creating a Gas/Vacuum Environment
58
Operation with Air
58
Operation under Vacuum
58
Operation with Gases Other than Air
59
Heating and Cooling the Sample
60
Carrying out the Measurement
60
Temperature Control Information
61
Sample Temperature Accuracy
61
Effective Heating and Cooling Rate
61
Standard Sample Holder
61
Putting TTK 600 out of Operation
62
Troubleshooting
63
Error Messages
63
General Messages on Display
63
Error Analysis
63
Technical Support
66
Maintenance
67
Routine Maintenance
67
Check the Functioning of the Flow Controller
67
Exchanging of Parts
67
Switching off the Instrument
67
Exchanging the Graphite Foil
67
Replacing the Window Foil
69
Replacing the O-Rings
69
Checking and Replacing Mains Fuses
70
Appendix A: Technical Data
71
Appendix B: Sample Chamber Dimensions
74
Appendix C: Declaration of Conformity
75
Appendix D: Spare Parts and Accessories
76
Appendix E: Safety Data Sheet for Liquid Nitrogen
78
Appendix F: Warranty
85

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