Page 3
Operate the Series 5200 Binary Gas Analyzer according to the operat- ing procedures stated herein. Any questions concerning the safe and proper use of your instrument should be addressed to: Mail: GOW-MAC Instrument Co. 277 Brodhead Road Bethlehem, PA 18017 Tel:...
GENERAL PRECAUTIONS FOR HANDLING AND STORING HIGH PRESSURE GAS CYLINDERS Compressed gases gave properties that can cause serious accidents, injuries, and even death if proper precautions and safety practices are not followed. Therefore, during handling and use of these gases, be certain to use applicable safety precautions described by your local compressed gas sup- plier, the Compressed Gas Association, and/or O.
Section 1 Safety This section contains information to promote safety in the operation and main- tenance of this equipment. It is not intended to supersede, replicate, or replace any safety documentation or procedures provided from or established by official safety sources. All persons involved with the operation of this equipment including plant engineering, operations, and management must understand the potential hazards involved, and know and observe all required safety precautions.
Page 10
Series 5200 beyond the scope of these instructions or by anyone other than GOW-MAC or a GOW-MAC Representative could cause the product to fail to perform as de- signed, and persons who rely on this product for their safety could sustain severe bodily injury or death.
Section 2 Principle of Operation A. Detectors 1. Thermal Conductivity Detector (TCD) The thermal conductivity detector (TCD) consists of a relatively large mass of metal to pro- vide a stable heat sink. Stainless steel is generally used because of its compatibility with most sample gases and its high thermal conductivity.
Page 12
(gas pair and relative concentra- tions). Detector current is provided by a solid state constant current power supply. The TCD is tem- perature-controlled in an insulated enclosure. Temperature is set and monitored on the screen. GOW-MAC Instrument Co.
Section 3 Specifications Detector Diffusion Type -Thermal Conductivity (TCD) User selectable nominal ranges. Upper limits are function of signal. Ranges Ranges 1-4 limits are subject to change with varying current for different gas pairs. 100 °C (default) Detector Temperature User programmable in range 0-100 °C Operating Temperature 15°C –...
1. When unpacking the instrument, check it carefully for evidence of shipping damage or rough handling. Check to ensure that all components ordered have either been supplied or backor- dered. Report any damage or discrepancies immediately to GOW-MAC Instrument Com- pany.
Page 16
The height and width of the front panel are designed to fit into an EIA standard 19-inch rack. The 7-inch touchscreen is the display and user interface. The only instrument power switch is on the back panel. Model 5200 Binary Gas Analyzer front panel, dimensions in inches GOW-MAC Instrument Co.
Page 17
3. Gas Connections Gas connections are on the back panel. All are 1/8” diameter stainless steel compression fit- tings. Gas parameters for the Series 5200 Binary Gas analyzer are specified in the following table. Model 5200 Binary Gas Analyzer back panel and connections, dimensions in inches Series 5200 Binary Gas Analyzer, 0724, Rev.0...
Page 18
DO NOT USE soap or other organic substances to check for leaks. If there are leaks, the soap and/or organic substances will be aspirated into the leak and contaminate the system. The easiest way to locate leaks is with the GOW-MAC model 21-080 Mini Gas Leak Detector if the tubing can be pressurized with helium.
Page 19
5. Instrument Communication Connection Descriptions a. 25-pin user I/O connection. D-SUB female receptacle with 25 positions described in the following table. POS.# POSITION NAME SPECIFICATION READY (NC) Contact 30 VDC @ 300 mA ALARM 1 (NO) Contact 30 VDC @ 300 mA ALARM 1 (COM) Contact 30 VDC @ 300 mA ALARM 2 (NC)
Page 20
9-pin serial connection. D-SUB male receptacle with 9 positions described in the follow- ing table. POS. # POSITION NAME NOT USED RS-232 RECEIVE DATA RS-232 TRANSMIT DATA NOT USED RS-232 GROUND SIGNAL NOT USED NOT USED NOT USED NOT USED GOW-MAC Instrument Co.
Communications 1. USB Connection The USB port can be used for data logging storage and future GOW-MAC software updates. A thumb drive or external hard drive can be connected here to save the data log text files. It is important to keep track of how much space is used when collecting data. Once the storage is full, the data log will STOP collecting data.
Page 22
Rating: output protection 240V RMS, 1000 Ohm maximum load Connections: Pin 11 (4-20mA) Lo Pin 24 (4-20mA) Hi ii. 0-5 Volt analog output Rating. Analog Signal Output: 5V compliance w/ 10K Ohm minimum load Connections: Pin 12 (0-5V) Lo-(ground) Pin 25 (0-5V) Hi GOW-MAC Instrument Co.
Page 23
b. Status Relay Outputs Description: For monitoring system status Ratings: 30 VDC @ 300 mA i. High/Low alarms Connections: Pin 2 Alarm 1 N.O. Pin 16 Alarm 1 N.C. Pin 3 Alarm 1 Common Connections: Pin 4 Alarm 2 N.C. Pin 17 Alarm 2 N.O.
Quick Start Guide 1. Connect zero/reference, span/calibration and sample gases to back panel. The allowable range for gas pressures is 10 to 100 psig. If installing the 5200P (purgeable housing), one additional connec- tion needed is purge gas (see addendum). 2.
Page 26
To view % impurity or purity, navigate to the TCD screen and select desired display units on the right-hand side. The Analyze screen displays measured ppm or % for whichever gas is selected on the Control screen. GOW-MAC Instrument Co.
Section 6 Operating Controls User Interface Screens The Series 5200 uses a touchscreen for user interface controls. Tabs along the bottom are to navigate between screens. NOTE ABOUT UNITS USED ON THE SCREENS – When not labeled on the screen, default units are: Gas Flow = ccpm Temperature = °C...
Page 28
• Date, time, and range of current calibration. • During calibration, a “Stabilization Timer” will appear in the calibration message box and count down the remaining seconds. • Buttons to manually start zero, span, and span check cycles. GOW-MAC Instrument Co.
Page 29
o Zero: Switches to zero (reference) gas to determine the actual signal offset for the zero gas provided. The process takes two minutes, and the software will as- sign a “zero” value to that specific detector signal. o Span: Switches to span gas to determine the actual detector signal for the cali- bration gas provided.
Page 30
• Display units can be selected on the right-hand side. Selected units will appear through- out the program and the options included are ppm (impurity), % impurity, and % purity. Please note that you cannot calibrate with % purity selected. GOW-MAC Instrument Co.
Page 31
For binary mixes, maximum currents lie between the two curves for pure gases. This chart applies to TCDs with GOW-MAC W, WX, W2, AuW, and Ni filaments. Detector. The detector signal is based on thermal conductivity of the flowing gases as well as the bridge current.
Page 32
• The active range is displayed in the Status Bar as R1, R2, R3, or R4. • Polarity Button. If the instrument is displaying a negative signal, the polarity switch can be used to flip the signal in the positive direction. GOW-MAC Instrument Co.
Page 33
6. Output Screen features • The values displayed on the output screen will reflect the selection made on the TCD page. For example, if you select “% Impurity”, the values on the output screen will be in % impurity. • 4-20 mA Output. Enter the 4 to 20 mA output concentrations based on the desired range of measurement.
Page 34
Press key #7. A message in the Status Bar indicates the update is in progress. Follow prompt to reboot the system. The installed software revision is displayed on the Menu Screen after the reboot. GOW-MAC Instrument Co.
Section 7 Instrument Operation 1. Select gases on the Gas Screen. a. Select sample gas. i. This is the matrix gas of the sample, also described as the balance or main com- ponent of a gas mixture. The selected sample gas is communicated to a sample flow meter that corrects from a stored gas list.
Page 36
Date and time of the last successful calibration will appear in the status bar and in the calibration message box. GOW-MAC Instrument Co.
Page 37
7. Span Check. To check validity of the span value at any point in the analysis, hit the check span button to initiate a span check process. The 5200 performs a verification of the saved span value. The span gas is sent to the detector and the resulting signal must be within 2% of the saved value to be considered good.
Section 8 Troubleshooting All Models Not Calibrating. There are three known causes of a failure to calibrate the 5200. First, the instrument might not calibrate if set to the wrong range. Ensure the range is correct for the span gas. Second, the voltage signal shown on the control screen may be too low to calibrate.
Section 9 Replacement Parts Description Part Number TCD detector, 10-454 with WX filaments............10-5200-00 Platinum probe for detector heater..............124-175 Heater, 3/8 in OD X 3 in L, 100W, 120V............124-181 Heater, 3/8 in OD X 3 in L, 100W, 240V............124-182 Fuse, 10A, Power Inlet module..............121-162 Gas selection manifold shut-off valve.............180-1032 Series 5200 Binary Gas Analyzer, 0724, Rev.0...
Recommended flow rates for the 5200 are 200 ccpm for both reference and sample gas. These flow rates are essential for an accurate calculation. Please refers to GOW-MAC’s Gen- eral Service Bulletin to get more information on choosing a safe current for your analysis.
Hydrogen Palladium Tubes are not covered by this warranty. All requests for service or repair under this warranty must be received within the warranty period by GOW-MAC or its authorized representative. All repairs are made at GOW-MAC plants or at the ® office of authorized representatives.
City: State/Country: Zip : E-mail address: BEFORE item can be shipped, fax completed form to: (610) 954-0599 or e-mail it to: repairs@gow-mac.com For GOW-MAC Use Only: Signed: Date Passed Safety Inspection. OK to proceed to Repair Dept. Chemical Safety Officer...
Need help?
Do you have a question about the 5200 Series and is the answer not in the manual?
Questions and answers