Princeton Instruments IsoPlane SCT 320 Manual
  1. Manuals
  2. Brands
  3. Princeton Instruments Manuals
  4. Laboratory Equipment
  5. IsoPlane SCT 320
  6. Manual

Princeton Instruments IsoPlane SCT 320 Manual

Hide thumbs
Table of Contents

Advertisement

Quick Links

Download this manual
so lane
Manual
Download from Www.Somanuals.com. All Manuals Search And Download.

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the IsoPlane SCT 320 and is the answer not in the manual?

Questions and answers

Summary of Contents for Princeton Instruments IsoPlane SCT 320

  • Page 1 so lane Manual Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 2 4411-0143 Version 1.B May 8, 2013 www.princetoninstruments.com 15 Discovery Way, Acton, MA 10720 Phone: 978-263-3584 Fax: 978-263-5086 Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 3 FAX: 609-587-1970 www.princetoninstruments.com All rights reserved. No part of this publication may be reproduced by any means without the written permission of Princeton Instruments, a division of Roper Scientific, Inc. (“Princeton Instruments”). Printed in the United States of America. IntelliCal and SpectraSense are trademarks, and IsoPlane and LightField are registered trademarks of Roper Scientific, Inc.

  • Page 4: Table Of Contents

    Table of Contents ® Chapter 1 IsoPlane SCT 320 Description ..........7 1.1 Introduction ........................7 1.2 IsoPlane SCT 320 Description ..................7 Chapter 2 IsoPlane Setup ............... 9 2.1 Unpacking and Inspecting ....................9 2.2 Initial Setup Procedure......................9 2.2.1 Optional Software Packages .................9 2.2.2 Controlling the IsoPlane at the Command Level ..........10...
  • Page 5 Appendix H Certification and Warranty..........57 Index ....................... 59 Figures Figure 1-1. Light Path within the IsoPlane SCT 320 ..............7 Figure 2-1. Details of the RS-232, USB, and Power Connections on the IsoPlane......10 Figure 2-2. Power Supply ......................11 Figure 2-3. Turret Compartment Location..................12 Figure 2-4.
  • Page 6 Table of Contents Figure 2-18. Lift Turret up out of the Turret Compartment ............27 Figure 2-19. Location of Hole on Turret Grating Assembly ............27 Figure 2-20. Location of Post on Grating Spindle Assembly ............27 Figure 2-21. Turret Installed (Hole and Post Aligned) ..............28 Figure 3-1.
  • Page 7 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 8: Chapter 1 Isoplane Sct 320 Description

    ® 1.1 Introduction This manual is intended to help you set up and operate your new IsoPlane SCT 320 spectrograph. Even if you are an experienced user of spectroscopic equipment, we suggest that you follow the manual (at least initially) to insure proper setup and operation. If you have any...
  • Page 9 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 10: Chapter 2 Isoplane Setup

    LightField or WinSpec data acquisition and control software when operated with a Princeton Instruments detector. Connect the USB port of the IsoPlane to the USB port on the control computer using the USB cable provided. RS-2332 may also be used if a USB port is not available.

  • Page 11: Controlling The Isoplane At The Command Level

     CC-499-2 IBM AT or compatible 9-pin female (DB9S) connector to 9-pin male connector (DB9P). If neither of these cables is compatible with your system, consult Princeton Instruments for a custom cable. If you have facilities for constructing a custom cable, use the RS-232 pin assignments shown in Table 2-1.

  • Page 12: Terminal Or Rs-232 Port Settings

    Sections 2.13.1 and 2.13.2, respectively. 2.6 Mounting Accessories to an IsoPlane Slit Assembly All Princeton Instruments spectroscopy accessories come with their own set of instructions for proper mounting and operation. The instructions below are only general information. Please refer to the individual instructions for detailed information.

  • Page 13: Turret Installation

    Note: In some instances with light sources, there is limited access to the bottom two screw holes. In this case, Princeton Instruments provides special slotted holes in the light source housing to facilitate mounting the source to the slit.

  • Page 14: Figure 2-4. Center Torque Screw

    Chapter 3 SCT 320 Operation 7. Locate the vertical post on the Grating Spindle Assembly (see Figure 2-6). 8. Position the grating turret on the grating spindle so the hole in the turret assembly aligns with the post in the turret assembly as shown in Figure 2-8. 9.

  • Page 15: Figure 2-6. Location Of Post On Grating Spindle Assembly

    ® IsoPlane SCT 320 Manual Version 1.B Post Figure 2-6. Location of Post on Grating Spindle Assembly Figure 2-7. Lower Turret into the Turret Compartment Aligned Hole and Post Figure 2-8. Turret Installed (Hole and Post Aligned) Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 16: Array Detector Mounting Instructions

    Chapter 3 SCT 320 Operation 2.8 Array Detector Mounting Instructions 2.8.1 Introduction The standard mounting plate for CCDs, FPAs, and diode arrays accommodates detectors with a slotted flange or mounting holes aligned on a 3.60” bolt circle pattern. There are six (6) equally spaced #10-32 tapped holes on a 3.60”...

  • Page 17: Mounting An Array Detector To The Isoplane

    ® IsoPlane SCT 320 Manual Version 1.B 2.8.2 Mounting an Array Detector to the IsoPlane The array detector mounting plate is mounted to the entrance port of the IsoPlane. 1. Remove the shipping cover from the mounting plate. 2. If the detector has a three-slotted flange (3.60” bolt circle): a.

  • Page 18: Rotational Alignment

    Chapter 3 SCT 320 Operation 2.8.3 Rotational Alignment This general procedure assumes that you have already mounted the array detector to the exit port of the spectrograph and that there is a light source at the entrance port. The basic actions are listed below.

  • Page 19: Focusing The Spectrometer

    ® IsoPlane SCT 320 Manual Version 1.B 2.8.4 Focusing the Spectrometer The basic actions for focusing the spectrometer are listed below. This general procedure assumes that you have already mounted the array detector to the exit port of the spectrograph and that there is a light source at the entrance port.

  • Page 20: Height Adjustment Of Image Plane

    Chapter 3 SCT 320 Operation 2.8.5 Height Adjustment of Image Plane Note: This procedure should only be attempted by someone experienced in aligning optical components and assemblies. 2.8.5.1 Overview During the manufacturing process, the IsoPlane focal plane is factory-aligned so that it is precisely centered on the optical axis.

  • Page 21: Single Point Detector Mounting Instructions

    ® IsoPlane SCT 320 Manual Version 1.B 2. Adjustments to the Cap and Set Screws should be small, approximately 1/8 -turn or less. 3. If the Cap Screw is adjusted 1/8 -turn in a counter-clockwise direction, then the Set Screw should be adjusted 1/8 -turn in a clockwise direction.

  • Page 22: Spectrometer Calibration

    Chapter 3 SCT 320 Operation 2.10 Spectrometer Calibration Refer to the application software manual or the software help for information on calibrating the data pixels with wavelengths. 2.11 Slit Width Adjustments in the Model 716-1 Manual Bilateral Slit and the 716-MS Kinematic Slit The slit width of each bilateral slit assembly (716 type) is adjustable from 0.010 millimeters to 3 millimeters (10 to 3,000 µm) by a micrometer knob located on the top of the slit housing.

  • Page 23: Slit Width Adjustments In The Model 718-1 Motorized 3Mm Slit

    This shutter is controlled either by a detector via a shutter cable from the detector’s Shutter connector to the Shutter connector on the IsoPlane or by an Shutter Control box (Model SHC-EXT) available from Princeton Instruments. 2.13.1 Installing an Internal Shutter 1.

  • Page 24: Removing An Internal Shutter

    IsoPlane has an internal shutter, you will either have to remove the shutter or control the shutter via a Princeton Instruments SHC-EXT external shutter control box if one is available. This is because there is no way for these detectors to keep the shutter open or to open the shutter during an acquisition.

  • Page 25: Turret Removal

    ® IsoPlane SCT 320 Manual Version 1.B 2.14 Turret Removal CAUTION 1. The optical surfaces in the spectrograph are extremely delicate and can be permanently damaged by contact with solid objects as well as with most liquids and aerosols. 2. DO NOT TOUCH optical surfaces with anything. Wear thin protective powderless gloves to minimize damage from body oils if you accidentally touch any optical surface, especially the grating.

  • Page 26: Turret Interchange

    Chapter 3 SCT 320 Operation Figure 2-16. Lift Turret up out of the Turret Compartment 6. If you are not installing/removing a shutter assembly or installing a different turret, replace and secure the Turret Compartment cover. 2.15 Turret Interchange Read and follow the instructions in this section only if you have ordered more than one turret for the IsoPlane.

  • Page 27: Figure 2-17. Center Torque Screw

    ® IsoPlane SCT 320 Manual Version 1.B 6. Use extreme care so as not to touch the grating surfaces. Grasp the Center Torque Screw and lift the grating turret straight up off the grating spindle assembly (see Figure 2-18). If the turret cannot be lifted up, you may need to loosen the Center Torque Screw more.
  • Page 28 Chapter 3 SCT 320 Operation Figure 2-18. Lift Turret up out of the Turret Compartment Hole Figure 2-19. Location of Hole on Turret Grating Assembly Post Figure 2-20. Location of Post on Grating Spindle Assembly Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 29 ® IsoPlane SCT 320 Manual Version 1.B Aligned Hole and Post Figure 2-21. Turret Installed (Hole and Post Aligned) Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 30: Chapter 3 Operation

    Chapter 3 Operation 3.1 Introduction This chapter reviews how to enable the control of an IsoPlane and Princeton Instruments detector by either the LightField (64-bit) or WinSpec (32-bit) software. This chapter also points out how to perform alignment using the software. Further information about operating the system can be found in the appropriate software manual or help file.

  • Page 31: Lightfield

    ® IsoPlane SCT 320 Manual Version 1.B 3.4 LightField Start LightField after making sure the detector and IsoPlane are connected to the computer and are turned on. When LightField boots it will look for available devices and will load their icons in the Available Devices panel.
  • Page 32 Chapter 3 SCT 320 Operation Figure 3-2. LightField Experiment Settings stack and Experiment Devices panel 3. Note that the stack on the left now displays several expanders. Experiment Settings Because this is a new experiment, the default settings for the detector will be active. The bar (at the bottom of the window) displays an icon for temperature status.

  • Page 33: Perform Alignment

    Micrometer Compartment, and the locking set screw. If not, refer to earlier sections of this manual. 1. Mount a light source such as a Princeton Instruments Hg and Ne/Ar Dual Switchable light source in front of the entrance slit.
  • Page 34 Chapter 3 SCT 320 Operation 9. Click on the peak you will be monitoring for the alignment. This will display the data cursor, which you can position at the top of the peak. Since the data cursor spans the ROIs (graphs), you can use the data cursor as your vertical reference. 10.

  • Page 35: Winspec

    ® IsoPlane SCT 320 Manual Version 1.B 3.5 WinSpec Start WinSpec after making sure the detector and IsoPlane are connected to the computer and are turned on. WinSpec should find the detector and present a dialog for selecting the detector for your experiment.
  • Page 36 Chapter 3 SCT 320 Operation 2. On the Define Spectrograph dialog (Figure 3-6), click on the Install/Remove Spectrograph button. 3. On the Install/Remove Spectrograph dialog, scroll down the list of supported spectrographs, click on Acton SCT320, click on the Install Selected Spectrograph button, and then click on OK to return to the Define Spectrograph dialog.

  • Page 37: Perform Alignment

    After you have aligned the optics the first time, you may want to repeat the process to fine tune the alignment. 1. Mount a light source such as a Princeton Instruments Hg and Ne/Ar Dual Switchable light source in front of the entrance slit.
  • Page 38 Chapter 3 SCT 320 Operation 3. Set the slit to 10 µm at a minimum. If necessary, adjust the Exposure Time to maintain optimum (near full-scale) signal intensity. 4. Wait until the detector locks at its default temperature. If the detector is LN-cooled, it should have been filled after the detector was powered ON.
  • Page 39 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 40: Appendix A Using The Monochromator Control Software

    A.1 Introduction As has been previously mentioned in this manual, the Acton IsoPlane spectrograph can be controlled using Princeton Instruments’ LightField, WinSpec, or SpectraSense software. It can also controlled from a computer using the supplied Monochromator Control software via the RS-232 or USB interface.

  • Page 41: Spectrograph Wavelength Movement Commands

    ® IsoPlane SCT 320 Manual Version 1.B Parameters, if needed, precede the command and are separated from the command by at least one space (e.g., 546.07 GOTO). For RS-232 operation, the port set-up is 9600 baud, 8 data bits, 1 stop bit and no parity. A convenient tool for trying out this mode of operation is the program HyperTerminal supplied with the Windows operating system.

  • Page 42: Grating Control Commands

    Appendix A Using the Monochromator Control Software A.4.2 Grating Control Commands Places specified grating in position to the wavelength of the wavelength GRATING on the present grating. Up to nine (9) gratings are allowed on three (3) turrets. This command takes a grating number from 1 - 9. IMPORTANT NOTE: This command assumes that the correct turret is specified by the TURRET command.

  • Page 43: Slit Width Control Commands (For Motorized Slits Only)

    ® IsoPlane SCT 320 Manual Version 1.B A.4.3 Slit Width Control Commands (for Motorized Slits only) Designates side exit slit to receive slit control commands. SIDE-EXIT-SLIT Designates side entrance slit to receive slit control commands. SIDE-ENT-SLIT Sets the slit width for the designated slit in the range of 10 to 3000 MICRONS microns to 1 micron resolution.

  • Page 44: Appendix B Spectrograph To Computer Cable Connection

    Appendix B Spectrograph to Computer Cable Connection Figure B-1. RS-232 Cable Wiring Figure B-2. IsoPlane Cable Connectors Filter driver connection for Acton FA-2448 Filter Wheel. FILTER SHT TTL connection for TTL control of shutter. SHT TTL DSP connection to connect two spectrographs as doubles. Com light flashes when communicating with the computer.
  • Page 45 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 46: Appendix C Accessories Listing

    Appendix C Accessories Listing Slit Assembly Bilaterally adjustable ENTRANCE slit assembly for IsoPlane monochromator SP-716-1 or spectrograph. Micrometer adjustable widths from 10 µm to 3 mm. Supplied with interchangeable 4.0 mm and 14.0 mm high baffles. Triple Grating Turret Interchangeable triple grating turret for the IsoPlane. Requires gratings. 300-483 Optional second and third turrets.
  • Page 47 MicroSpec spectroscopy with a single system. Attaches to a UDP port on an inverted microscope and couples to the IsoPlane SCT 320. For more information, refer to the MicroSpec data sheet on the Princeton Instruments website. Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 48 Appendix C Accessories Listing Filter Wheels and Order Sorting Filter Assemblies Six Position Filter Wheel Assembly. Manual sample indexing, holds up to six FA-2448 samples, each 1.0” diameter; automated via SP Control Cable. Can be used with the IsoPlane. Requires FA-2448-F Filter Set or customer-supplied filters of 25 mm (1 inch) diameter and 5 mm or less in thickness.
  • Page 49 CC-499-2 connectors. USB cable, 6 feet (1.82 meters) long, type A to B connectors. 3650-USB-06 If the above cables are not compatible with your system, contact Princeton Instruments for a custom cable. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 50: Appendix D Gratings For Isoplane

    Acton, MA 01720 U.S.A. FAX: 978-263-5086 Orders accepted subject to current pricing. All orders FOB Princeton Instruments-Acton or shipping charges & insurance added separately. All orders subject to new customer approval. ™ • IsoPlane is a trademark of Roper Scientific, Inc. •...
  • Page 51 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 52: Appendix E Outline Drawings

    Appendix E Outline Drawings Figure E-1. IsoPlane: 320 with Manual Slit Assembly Outline Drawing Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 53 ® IsoPlane SCT 320 Manual Version 1.B Figure E-2. IsoPlane: 320 with Motorized Slit Assembly Outline Drawing Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 54: Appendix F Standard Slit Assembly Drawing

    Appendix F Standard Slit Assembly Drawing Figure F-1. Standard Slit Assembly Drawing Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 55 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 56: Appendix G Declaration Of Conformity

    Appendix G Declaration of Conformity DECLARATION OF CONFORMITY We, the undersigned Manufacturer: Princeton Instruments Address, City: 15 Discovery Way, Acton, MA 01720 Country: USA Certify and declare under our sole responsibility that the following apparatus: IsoPlane SCT-320 with Power Supply Conforms to the emissions requirements of EN61326-1:2006;...
  • Page 57 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 58: Appendix H Certification And Warranty

    Appendix H Certification and Warranty Certification Princeton Instruments certifies that this instrument was thoroughly tested and found to meet the specifications furnished by Princeton Instruments when it was shipped from the factory. Warranty Princeton Instruments instruments and accessories are warranted for a period of one full year from date of delivery to be free from defects in material and to conform to the specifications furnished by Princeton Instruments.
  • Page 59 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.

  • Page 60: Index

    Index Monochromator Control application software ....39 Motorized slit ..............22 Accessories Mounting a detector listing of............... 45 array ................16 MicroSpec ..............46 PyLoN without shutter ..........16 mounting to slit assembly ..........11 single point ..............20 Additional commands ............42 SPEC-10 LN without shutter ........
  • Page 61 ® IsoPlane SCT 320 Manual Version 1.B This page intentionally left blank. Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 62 Contact Princeton Instruments for additional information. www.princetoninstruments.com | info@princetoninstruments.com USA TOLL-FREE +1.877.474.2286 | USA +1.609.587.9797 Download from Www.Somanuals.com. All Manuals Search And Download.
  • Page 63 Free Manuals Download Website h p://myh66.com h p://usermanuals.us h p://www.somanuals.com h p://www.4manuals.cc h p://www.manual-lib.com h p://www.404manual.com h p://www.luxmanual.com h p://aubethermostatmanual.com Golf course search by state h p://golfingnear.com Email search by domain h p://emailbydomain.com Auto manuals search h p://auto.somanuals.com TV manuals search h p://tv.somanuals.com...

Table of Contents