Summary of Contents for Barnstead International NANOpure DIamond 1192 Series
- Page 1 NANOpure DIamond ® ™ ultrapure water system Operation Manual Series 1192 Model No. Voltage D11921 100V - 240V LT1192X1 • 8/27/03...
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Page 2: Table Of Contents
Table of Contents Safety Information ......................................3 Alert Signals......................................3 Warnings ........................................3 Introduction ........................................5 General Usage......................................5 General Specifications ....................................6 Environmental Conditions ..................................7 Declaration of Conformity ..................................7 Unpacking ........................................8 Installation ........................................9 Choosing a Site ......................................9 Ultrafilter Installation ....................................10 Other Accessories ....................................11 Bench Mounting ....................................12 Wall Mounting ......................................12 Installing the Control Panel in a Remote Location ..........................13 Water Connections ....................................14... -
Page 3: Safety Information
Safety Information Your Barnstead NANOpure DIamond UF ultrapure water Alert Signals system has been designed with function, reliability, and safety in mind. It is your responsibility to install it in con- formance with local electrical codes. This manual con- tains important safety information. You must carefully read Warning Warnings alert you to a possibility of and understand the contents of this manual prior to the... - Page 4 AFETY NFORMATION clothing or skin. Ensure all piping connections are tight to avoid chemical leakage. Ensure adequate ventilation. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. Depressurize system prior to removing the cartridge pack. Refer servicing to qualified personnel.
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Page 5: Introduction
Introduction Congratulations on your purchase of a Barnstead NANOpure DIamond Life Science (UV/UF) ultrapure water system. This water purification system is designed to provide pyrogen-free, low TOC, high resistivity, reagent grade water that exceeds ASTM Type I, CAP and NCCLS Type I standards. -
Page 6: General Specifications
General Specifications Dimensions and Clearance Requirements Dimensions 13.5” W x 19.5” H x 17.0” D (34.3 x 49.5 x 43.2 cm) Clearances Sides - 9” (22.9 cm) minimum for servicing. Above - 3” (7.6 cm) minimum for removal of the top cover. Front - 4.75”... -
Page 7: Environmental Conditions
Storage: -25°C to 65°C; 10% to 85% relative humidity. Declaration of Conformity Barnstead International hereby declares under its sole responsibility that this product conforms with the technical requirements of the following standards: EMC: EN 61000-3-2 Limits for Harmonic Current Emissions... -
Page 8: Unpacking
Unpacking Remove the unit from its shipping container. Remove all contents carefully. Ensure that the ultrafilter, feed and drain tubing, sanitization cartridge, wall bracket, accessory parts bag and power cords (see list below) are re- moved from the packaging materials before discarding. -
Page 9: Installation
Installation Choosing a Site Caution The NANOpure DIamond UF features a removable con- Wall composition, condition and trol panel display which allows the system to be mounted construction as well as fastener type almost anywhere within the laboratory. Use the wall must be considered when mounting bracket for wall mounted systems as a template to drill this unit. -
Page 10: Ultrafilter Installation
NSTALLATION Ultrafilter Installation Remove the ultrafilter from its protective bag. Install the ultrafilter as follows: Note Open the front (right side) door and the right Do not install the ultrafilter until the side door. NANOpure DIamond UF is ready for use. -
Page 11: Other Accessories
NSTALLATION Other Accessories Optional accessories for this unit include a float switch, low pressure switch, N.I.S.T. Traceable Calibration Module, remote dispenser, and printer. Installation proce- dures for these accessories are explained in later sections of this manual. -
Page 12: Bench Mounting
NSTALLATION Bench Mounting Place the NANOpure DIamond UF on a bench top that is accessible to pretreated water, elec- tricity and an atmospherically vented drain. Wall Mounting Caution Install the NANOpure DIamond UF on a wall in a conven- Wall composition, condition and con- ient location that is accessible to water, an atmospherical- struction, as well as fastener type, ly vented drain and electricity. -
Page 13: Installing The Control Panel In A Remote Location
NSTALLATION Installing the Control Panel in a Note The removable control panel was not Remote Location designed to be repeatedly removed For your convenience, the control panel can be removed from the unit, therefore, you may from the unit and mounted at a convenient location within experience difficulty when attempting 10 ft. -
Page 14: Water Connections
NSTALLATION Water Connections Caution Do not connect feed water until direct- Feed Water Connection ed to do so during “Initial Sanitization.” Locate the length of 3/8” (.95 cm) O.D. tubing pro- vided with the unit with a quick disconnect insert on one end and a 3/8”... - Page 15 NSTALLATION Wet the tube end with water and insert tube straight into fitting until it bottoms out on interior shoulder and insertion mark is no longer visible. To remove tubing, push collet toward fitting body and pull on tubing. To reuse fitting, begin assem- bly at step one.
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Page 16: Controls
Controls Main Power Switch The main power switch on the NANOpure DIamond UF is located on the lower back right side of the unit (as you face the front of the unit), directly above the power cord receptacle. Note Control Panel The removable control panel was not The NANOpure DIamond UF is controlled through a panel designed to be repeatedly removed... -
Page 17: Switches
ONTROLS Switches When the main power switch (on the lower back right side of the unit as you face the unit) is ON, the switches on the control panel function as follows: START/STOP allows you to alternate the unit between the normal (recirculation) mode;... -
Page 18: Initial Operation
Initial Operation Cartridge packs will come bagged with four manifold connection caps. Part Application DIamond Kit Organic Free R/O & Distilled Feed D50280 Ultra-Low Organics, Type 1 Water, Reverse Osmosis or Distilled Warning Water Feed Allow cartridge pack to warm to room temperature before installation. -
Page 19: Initial Rinse
NITIAL PERATION Initial Rinse Attach the feed water line to the unit by snapping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit. Attach an atmospheric drain line [1/4” (.64 cm)] tubing by pushing into the quick connect fitting on the lower left back of unit. - Page 20 NITIAL PERATION System Sanitization Procedure Warning Your NANOpure DIamond UF has been shipped with a Avoid splashing disinfecting solution cleaning syringe (Cat. No. CMX25). When the system is on clothing or skin. new or whenever a new cartridge pack is installed, the system should be sanitized (cleaned).
- Page 21 NITIAL PERATION and press ENTER. Display will now read, “Unit Sanitizing.” 14. Unit may now be left unattended until display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculation mode.
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Page 22: Normal Operation
Normal Operation Turn the system power ON by depressing the main power switch to the “I” position. The system greeting display indicates the type of unit you own. This greeting is “UF.” Note On initial start-up, the purity meter The system electronics will initialize and check may display “...MΩ-cm or uS/cm.”... -
Page 23: User Settings
User Settings Adjusting Display Brightness From the (Idle) mode, when the display reads, “NANOpure Diamond (Idle) xx:xx:xx xx/xx/xx,” press the UP or DOWN arrow until display reads, “Advanced Menu?” Press ENTER. Press ENTER to proceed through the options until “Set Display Brightness” is displayed. Press the UP or DOWN arrow to choose “Yes.”... -
Page 24: Setting The Cell Constant
ETTINGS Press ENTER. Press ENTER when the unit displays “Printer Attached?” When prompted with “Date Format” press the UP or DOWN arrow to show the date format desired. Press ENTER to select the desired for- mat and continue. When prompted with “Set Date,” press the UP or DOWN arrow to choose “Yes,”... - Page 25 ETTINGS Unlatch and open the right side door. Find and copy down the two cell constants attached to the gray cable, leaving the electron- ics board mounted on the inside of the right side door. Close and latch the right side door. Reconnect the power cord and turn unit ON.
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Page 26: Use Of Standby Mode
ETTINGS Use of Standby Mode Note At the end of the work day, place the NANOpure When in Standby mode, press DIamond UF in Standby mode for the night. To place the START/STOP to continue normal unit in Standby mode: operation. -
Page 27: Resetting The Sanitization Timer
ETTINGS Press ENTER. Press BACK to return to the (Idle) mode. The second line of the display will show a “Below Set point” message once every 8 to 10 seconds when the measurement is below the set point. (The set point indica- tion is set at the factory at 10 MΩ-cm.) Resetting the Sanitization Timer From the (Idle) mode, when the display reads,... -
Page 28: Setting Volumetric Dispensing
ETTINGS Setting Volumetric Dispensing Note Volumetric dispensing is based upon From the normal recirculating mode, when the total fluid volume entering the display is showing purity, press the UP or NANOpure DIamond UF. Point of DOWN arrow until the display reads, “Auto draw-off accuracy will be compromised Dispense Menu?”... -
Page 29: Setting Timed Dispensing
ETTINGS Setting Timed Dispensing From the normal recirculating mode, when the dis- play is showing purity, press the UP or DOWN arrow until the display reads, “Auto Dispense Menu?” Press ENTER. Display will read, “Dispense Method.” Press the UP or DOWN arrow to select TIME. Press ENTER. -
Page 30: Temperature Compensation
ETTINGS Press the UP or DOWN arrow to select “MΩ-cm” or “uS/cm” Press ENTER. Press BACK to return to the normal recirculating mode. Temperature Compensation Note (Factory set to “ON.”) Purity displayed will have an asterisk From the normal recirculating mode, when the (*) the the left of the reading (* xx.x display is showing purity, press the Up or MΩ-cm or * x.xx uS/cm) to inform the... -
Page 31: Installing Float Or Pressure Switch
Installing Float or Pressure Switch Accessories D8964 (float switch) and D2706 (pressure switch) are designed to protect the NANOpure DIamond UF pump by alerting the system of an inadequate feed water condition so that the pump can be shut down. If an inadequate feed water condition exists and the pump is shut down due to this condition, the display will read “Check Inlet.”... -
Page 32: N.i.s.t Calibration Module
N.I.S.T Calibration Module Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module If you purchased the optional N.I.S.T. calibration module (Catalog No. E896X5) you can perform a calibration of the NANOpure DIamond purity sensing electronics traceable to N.I.S.T. standards. Disconnect power cord from the unit. -
Page 33: Remote Dispenser
N.I.S.T. C ALIBRATION ODULE 11. Press BACK to return to the (Idle) mode. 12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door. -
Page 34: Computer/Printer Setup
Computer/Printer Setup Connecting NANOpure DIamond to Computer and Communicating Though the RS-232 Port Using Hyperterminal or Procomm Hyperterminal RS-232 Capture Instructions Connect the 9 pin serial cable (part no. WHX18) from the NANOpure DIamond RS-232 port to COM2: port or (COM1: port) on back of computer. - Page 35 OMPUTER RINTER ETUP capture text. Accepting default will put the file which you name in the c:/windows directory called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. 12. When you are finished storing data from the NANOpure DIamond, save your file.
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Page 36: Connecting And Starting The Printer
OMPUTER RINTER ETUP 12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the NANOpure DIamond. -
Page 37: Printer Setup
OMPUTER RINTER ETUP During normal Recirculation mode, a purity and temperature reading will be printed once every Note 12 minutes. A colored stripe along the edge of the paper indicates that you are approach- ing the end of the tape. When the stripe appears, approximately 23 inch- Printer Setup es ( 58.4 cm) of paper remains,... -
Page 38: Maintenance And Servicing
Maintenance and Servicing General Cleaning Instructions Warning Disconnect electrical service to the unit. Wipe exterior • Avoid splashing mild detergent surfaces with lightly dampened cloth containing mild soap or weak acid on clothing or solution. skin • Ensure all piping connections are tight to avoid chemical Cell Cleaning leakage... -
Page 39: System Sanitization
AINTENANCE AND ERVICING System Sanitization Note After sanitization is complete (approximately 3.5 hours), The sanitization timer will display after place the unit into its normal (recirculation) mode to allow six months, reminding you to sanitize the system to recirculate overnight after cleaning. the unit. -
Page 40: System Depressurization
AINTENANCE AND ERVICING 14. Unit may now be left unattended until the display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete and the user presses “ENTER” the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode. -
Page 41: Cartridge Pack Replacement
Warning installed. The simple-to-use cleaning syringe is available Allow cartridge pack to warm to room from Barnstead International (Catalog Number CMX25). temperature before installation. This is used to effect a complete sanitization. Remove the feed water line by depressing the stainless steel thumb pad. -
Page 42: 0.2 Micron Filter Replacement
AINTENANCE AND ERVICING Caution Do not overtighten the 0.2 micron filter or use excessive force in seating it. The filter can be damaged by over- tightening or excessive force. 0.2 Micron Filter Replacement Replace the 0.2 micron final filter whenever any of the fol- Note lowing conditions occur: every 30 days, the product water If a newly installed 0.2 micron filter... - Page 43 AINTENANCE AND ERVICING Pull the ultrafilter out of the unit and turn it to the left side. (This will make it easier to disconnect the bottom fitting.) Using the tool supplied with the ultrafilter, simul- taneously push and hold the collet on the ultrafil- ter down while pulling the bottom fitting out of the connector.
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Page 44: Fuse Replacement
AINTENANCE AND ERVICING Fuse Replacement Turn off the NANOpure DIamond UF and dis- connect it from the power supply by removing the power cord directly below the main power switch on right side of unit. Locate the fuse drawer above the power cord receptacle. Pull out the fuse drawer located in the power entry module. -
Page 45: Troubleshooting
Troubleshooting Problem Possible Causes Solutions NANOpure DIamond completely No electrical power to NANOpure Ensure NANOpure DIamond power inactive (pump and display DIamond. cord is connected to a live power not operating.) source and completely plugged into electrical outlet as well as power entry module on the unit. - Page 46 ROUBLESHOOTING Poor quality feed water. If a Barnstead ROpure is the feed water source, check that the membrane is functioning properly. If a Barnstead Still is the feed water source, ensure that the distillate temperature to the NANOpure DIamond does not exceed 40°C (104°F).
- Page 47 ROUBLESHOOTING New cartridge pack: o-ring missing Disconnect inlet water and from post (each of the 4 posts depressurize system. Next, disconnect must contain an o-ring.) the manifold and verify/replace missing o-ring. Reinstall cartridge pack as indicated in “Cartridge Pack Replacement.”...
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Page 48: Replacement Parts
(filters, resin cartridges, etc.) and other items of limited life (indicator lights, fuses, etc.) that you can expect to replace on a more or less random basis. Where practical, Barnstead International recommends the frequency of replacement, or provides information on life expectancy from which you may calculate a replacement interval compatible with your usage pattern. - Page 49 EPLACEMENT ARTS Safety Stock For critical applications where performance with minimum downtime is required, Barnstead International recommends that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections. Description Catalog No. Recommended Quantity...
- Page 50 Flow Chart power switch turned on Barnstead / Thermolyne Vx.xx Style English Unit Initialization & Meter Calibration Check NANOpure DIamond (Idle) xx: xx: xx xx/ xx/ xx standby start_stop back key up or down enter key key pressed key pressed pressed keys pressed pressed...
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Page 51: Wiring Diagram
Wiring Diagram POWER ENTRY MODULE SWITCH & FUSES: 120V: (2) FSX47 230V: (2) FSX54 NEUTRAL CHASSIS GND CHASSIS LINE REMOTE DISPLAY CONNECTOR (SPG) MODEL #s D11911 & D11931 ONLY DIAGRAM COMPONENT LIST MODEL NO. AND OUR PART NO.(s) REF. DESCRIPTION D11901 D11901 D11911... -
Page 52: Ordering Procedures
All parts listed herein may be ordered from the Barnstead International dealer from whom you purchased this unit or can be obtained promptly from the factory. When service or replacement parts are needed we ask that you check first with your dealer. - Page 56 SALE, USE OR PERFORMANCE OF ANY PRODUCTS, WHETHER SUCH CLAIM IS BASED ON CON- TRACT, TORT (INCLUDING NEGLIGENCE), ANY THEORY OF STRICT LIABILITY OR REGULATORY ACTION. The name of the authorized Barnstead International dealer nearest you may be obtained by calling 1-800-446-6060 (563-556-2241) or writing to: 2555 Kerper Boulevard P.O.
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