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Bruker BioSpin CryoProbe RF CRP RF UNIT Technical Manual

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CryoProbe RF
ELECTRONICS
Technical Manual
003
Version
Bruker BioSpin

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Summary of Contents for Bruker BioSpin CryoProbe RF CRP RF UNIT

  • Page 1 CryoProbe RF ELECTRONICS Technical Manual Version Bruker BioSpin...
  • Page 2 The information in this manual may be altered without notice. Bruker BioSpin accepts no responsibility for actions taken as a result of use of this manual. Bruker BioSpin accepts no liability for any mistakes contained in the manual, leading to coinciden- tal damage, whether during installation or operation of the in- strument.

  • Page 3: Table Of Contents

    RF UNIT 1H13C2H15N Technical Data ....21 General ................21 Power Consumption ............21 Transmit-/Receive Bias Currents ........22 Service Information ..........23 General ................23 Basic System Checks ............23 Block Diagrams (HPPR and HPPR/2 family) ...... 24 Technical Manual Index 003 Bruker BioSpin 3 (33)
  • Page 4 Contents Figures ..............29 Tables ..............31 4(33) Bruker BioSpin Technical Manual Index 003...

  • Page 5: General Description

    HPPR CRP MODULEs respectively HPPR/2 MODULEs - Improved spectral purity of the rf pulses by using the built-in filters of the HPPR CRP MODULEs (HPPR/2 MODULEs) - Probe tuning of all nuclei - PICS (Probe Identification System) Technical Manual Index 003 Bruker BioSpin 5 (33)

  • Page 6: Crp Rf Unit Vs Hppr Crp (Hppr/2) Module

    - is used for probe tuning and matching - selects the received signal FT-REC - has full functionality for conventional probes • CRP RF UNIT: - contains transmit/receive switches - contains cryocooled preamplifiers - filters received signal - PICS 6 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 7: Rf Wiring For A Cp Dul C/H-D Or Cp Dui H/C-D (Hppr Crp)

    / to X-BB19F 2HS MODULE or 13C CRP MODULE (plugged at the SELECTOR manually) 1H RF IN 2H RF IN Connect the HPPR CRP FILTER SET 1H13C2H to the ‚XBB RF-IN‘ BNC-cable jack CP DUL C/H-D Technical Manual Index 003 Bruker BioSpin 7 (33)

  • Page 8: Rf Wiring For A Cp Dul C/H-D Or Cp Dui H/C-D (Hppr/2 Family)

    RF IN). Figure 1.2. RF wiring for a CP DUL C/H-D or DUI H/C-D (HPPR/2 family) Connect the HPPR CRP FILTER SET 1H13C2H to the ‚13C RF-IN‘ BNC-cable jack CP DUL C/H-D 8 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 9: Rf Wiring For A Cp Txi H-C/N-D (Hppr Crp)

    CONFIGURATION OF X-BB THE SELECTOR PREAMPLIFIER - SELECTOR from / to X-BB19F 2HS MODULE or 13C CRP MODULE (plugged at the SELECTOR manually) 1H RF IN 2H RF IN CP TXI H-C/N-D Technical Manual Index 003 Bruker BioSpin 9 (33)

  • Page 10: Rf Wiring For A Cp Txi H-C/N-D (Hppr/2 Family)

    1. The HPPR/2 XBB19F 2HS MODULE is used ONLY for operation with a con- ventional probe. 2. In general, no external filters are required between the HPPR/2 MODULEs and the CryoProbe. Figure 1.4. RF wiring for a CP TXI H-C/N-D (HPPR/2 family) CP TXI H-C/N-D 10 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 11: Rf Wiring For A Conventional Probe (Hppr Crp)

    TUNING - SPLITTER CONFIGURATION OF X-BB THE SELECTOR PREAMPLIFIER - SELECTOR from / to X-BB19F 2HS MODULE or 13C CRP MODULE (plugged at the SELECTOR manually) 13C PASS 2H STOP 15N PASS 2H STOP Technical Manual Index 003 Bruker BioSpin 11 (33)

  • Page 12: Rf Wiring In Case Of Existing Standard Hppr Modules

    Combination with HPHP 19F/1H/3H & X-BB MODULEs 1.9.4 Installation: • Power the HPHP 19F/1H/3H and X-BB HP MODULE by the ribbon cables leading from the HPPR CRP COVER MODULE to every single HPPR MOD- ULE. 12 (33) Bruker BioSpin Technical Manual Index 003...
  • Page 13 • Connect the rf cables of HPHP 19F/1H/3H MODULE to the 19F-connectors of the HPPR SELECTOR/TUNING-SPLITTER. • Connect the rf cables of HPHP X-BB MODULE to the UB-connectors of the HPPR SELECTOR/TUNING-SPLITTER. Technical Manual Index 003 Bruker BioSpin 13 (33)
  • Page 14 General Description 14 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 15: Operation

    The internal CryoProbe preamplifier may be bypassed for debugging purpose as follows: • xwinnmr -e UniTool hppr • [P]reamplifier module • [5] 1H, [7] 2H or [8] 13C • [S]et Force-State • [0] off, [4] cold, [8] bypass • [Q], [Q], ... Technical Manual Index 003 Bruker BioSpin 15 (33)

  • Page 16: Cryoprobe Operation With Hppr Crp Assembly

    XWIN-NMR selection of observe and decoupling nuclei (HPPR CRP only) 2.2.2 The observing nucleus can be selected in XWIN-NMR by the command ‚edasp’ and by selecting the corresponding F1 nucleus. The decoupling nuclei should be 16 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 17: Hppr Crp Cover Rf Selection Control

    SEMBLY provided that NOT MORE THAN 300 W is used for the HPPR 13C CRP or HPPR 15N CRP MODULE. Otherwise you have to check whether your possi- ble already existing HPPR XBB19F 2HS MODULE is able to handle 400 to 500W. Technical Manual Index 003 Bruker BioSpin 17 (33)
  • Page 18 - wobbling of observe channels (e.g. 1H, 13C, 15N), 2H lock operation. Note: After tuning and matching of a CryoProbe, the RF path routing must be re- set by the ‘crpon‘ command. 18 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 19: Rf Unit 1H13C2H Technical Data

    GND PIN 3 GND PIN 9 GND PIN 4 +15V (POWER Connector (LEMO), Pin 5) + 200 mA +15V PIN 5 -15V (POWER Connector (LEMO), Pin 6) - 50 mA -15V PIN 6 Technical Manual Index 003 Bruker BioSpin 19 (33)

  • Page 20: Transmit-/Receive Bias Currents

    ~ 25mA for ECL 00.05 and higher 500: Z003472 750: Z003475 500: Z003300 500: Z003897 600: Z003473 800: Z003476 600: Z003301 600: Z003898 800: Z003904 700: Z003474 900: Z003477 700: Z003914 900: Z100112. 20 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 21: Rf Unit 1H13C2H15N Technical Data

    GND PIN 3 GND PIN 9 GND PIN 4 +15V (POWER Connector (LEMO), Pin 5) + 200 mA +15V PIN 5 -15V (POWER Connector (LEMO), Pin 6) - 50 mA -15V PIN 6 Technical Manual Index 003 Bruker BioSpin 21 (33)

  • Page 22: Transmit-/Receive Bias Currents

    ~ 25mA for ECL 00.05 and higher 500: Z003472 750: Z003475 500: Z003300 500: Z003897 600: Z003473 800: Z003476 600: Z003301 600: Z003898 800: Z003904 700: Z003474 900: Z003477 700: Z003914 900: Z100112. 22 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 23: Service Information

    ING mode you get a traceable sweeped signal). With help of the oscilloscope, the following block diagram and a HPPR Technical Manual you can trace the tuning rf signal and all necessary trigger pulses at the HPPR and CryoProbe interface connectors. Technical Manual Index 003 Bruker BioSpin 23 (33)

  • Page 24: Block Diagrams (Hppr And Hppr/2 Family)

    Power Supply (BNC) 1H RF-OUT (BNC) 2H RF-OUT (BNC) 13C RF-OUT ± 5V COIL - SYSTEM (SMB) 13C COIL 2H COIL 1H COIL HPPR CRP FILTER SET 1H13C2H (BNC) (SMA) (SMA) (SMA) 24 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 25: Figure 5.2. Block Diagram Cp Dul C/H-D Or Cp Dui H/C-D (Hppr/2 Family)

    (±15V / SDA / SCL) Power Supply (BNC) 1H RF-OUT (BNC) 2H RF-OUT 13C RF-OUT (BNC) COIL - SYSTEM 13C COIL 1H COIL 2H COIL (BNC) POWER CABLE / I2C (±15V / SDA / SCL) Technical Manual Index 003 Bruker BioSpin 25 (33)

  • Page 26: Figure 5.3. Block Diagram Cp Txi H-C/N-D (Hppr Crp)

    (±15V / SDA / SCL) (BNC) (BNC) (BNC) Power Supply 1H RF-OUT 2H RF-OUT ± 5V COIL - SYSTEM (SMB) 1H COIL 2H COIL 13C COIL 15N COIL (BNC) (SMA) (SMA) (SMA) (SMA) 26 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 27: Figure 5.4. Block Diagram Cp Txi H-C/N-D (Hppr/2 Family)

    (±15V / SDA / SCL) Power Supply 1H RF-OUT 2H RF-OUT COIL - SYSTEM 1H COIL 2H COIL 13C COIL 15N COIL (BNC) POWER CABLE / I2C (±15V / SDA / SCL) Technical Manual Index 003 Bruker BioSpin 27 (33)
  • Page 28 Service Information 28 (33) Bruker BioSpin Technical Manual Index 003...

  • Page 29: Figures

    Block Diagram CP DUL C/H-D or CP DUI H/C-D (HPPR/2 family) ..............25 Figure 5.3. Block Diagram CP TXI H-C/N-D (HPPR CRP) ..... 26 Figure 5.4. Block Diagram CP TXI H-C/N-D (HPPR/2 family) ....27 Figures Tables Technical Manual Index 003 Bruker BioSpin 29 (33)
  • Page 30 Figures 30 (33) Bruker BioSpin Technical Manual Index 003...
  • Page 31 Table 4.1. Power Consumption ............21 Table 4.2. Cryoprobe T/R-switch bias current for the HPPR CRP ..22 Table 4.3. Cryoprobe T/R-switch bias current for the HPPR/2 family 22 Service Information Figures Tables Technical Manual Index 003 Bruker BioSpin 31 (33)
  • Page 32 Tables 32 (33) Bruker BioSpin Technical Manual Index 003...
  • Page 33 Lastpage Technical Manual Index 003 Bruker BioSpin 33 (33)

This manual is also suitable for:

Cryoprobe rf hppr crpCryoprobe rf hppr/2

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